European Journal of Chemistry 2014, 5(3), 394-396. doi:10.5155/eurjchem.5.3.394-396.1043

Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide


Riya Datta (1,*) , Ramya Vittalacharya (2) , Bubbly Shivappa Gudennavar (3)

(1) Department of Chemistry, Christ University, Bangalore-560029, India
(2) Department of Chemistry, Christ University, Bangalore-560029, India
(3) Department of Physics, Christ University, Bangalore-560029, India
(*) Corresponding Author

Received: 06 Mar 2014, Accepted: 07 Mar 2014, Published: 30 Sep 2014

Abstract


A new compound, N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide was synthesized. Elemental analysis, IR spectrum, 1H NMR and X-ray crystal structure studies were carried out to determine the compositions and molecular structure of the compound. It crystallizes in the orthorhombic space group Pbca with unit cell parameters a = 11.3142(4) Å, b = 7.5526(2) Å and c = 22.9030(9) Å. The crystal structure studies reveal intermolecular N-H···O hydrogen bonding interactions in the solid state.


Keywords


IR; NMR; Furfural; Crystal structure; Acylhydrazone; p-Chlorobenzhydrazide

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DOI: 10.5155/eurjchem.5.3.394-396.1043

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How to cite


Datta, R.; Vittalacharya, R.; Gudennavar, B. Eur. J. Chem. 2014, 5(3), 394-396. doi:10.5155/eurjchem.5.3.394-396.1043
Datta, R.; Vittalacharya, R.; Gudennavar, B. Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide. Eur. J. Chem. 2014, 5(3), 394-396. doi:10.5155/eurjchem.5.3.394-396.1043
Datta, R., Vittalacharya, R., & Gudennavar, B. (2014). Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide. European Journal of Chemistry, 5(3), 394-396. doi:10.5155/eurjchem.5.3.394-396.1043
Datta, Riya, Ramya Vittalacharya, & Bubbly Shivappa Gudennavar. "Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide." European Journal of Chemistry [Online], 5.3 (2014): 394-396. Web. 26 Aug. 2019
Datta, Riya, Vittalacharya, Ramya, AND Gudennavar, Bubbly. "Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide" European Journal of Chemistry [Online], Volume 5 Number 3 (30 September 2014)

DOI Link: https://doi.org/10.5155/eurjchem.5.3.394-396.1043

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