European Journal of Chemistry 2017, 8(1), 18-19. doi:10.5155/eurjchem.8.1.18-19.1510

Synthesis and characterization of 1,3-bis(2-fluorophenyl)-5-pentyl-1,3,5-triazinane


Amel Ferhati (1,*) , Achene Bouchemma (2) , Mustapha Bouhenguel (3) , Leila Lefrada (4) , Assia Sid (5)

(1) Laboratory of Applied Chemistry and Materials Technology, Faculty of Exact Sciences and Natural Sciences and life, Department of Material Sciences, Larbi Ben M’hidi University, Oum El Bouaghi, 04000, Algeria
(2) Laboratory of Applied Chemistry and Materials Technology, Faculty of Exact Sciences and Natural Sciences and life, Department of Material Sciences, Larbi Ben M’hidi University, Oum El Bouaghi, 04000, Algeria
(3) Laboratory of Applied Chemistry and Materials Technology, Faculty of Exact Sciences and Natural Sciences and life, Department of Material Sciences, Larbi Ben M’hidi University, Oum El Bouaghi, 04000, Algeria
(4) Laboratory of Applied Chemistry and Materials Technology, Faculty of Exact Sciences and Natural Sciences and life, Department of Material Sciences, Larbi Ben M’hidi University, Oum El Bouaghi, 04000, Algeria
(5) Laboratory of Applied Chemistry and Materials Technology, Faculty of Exact Sciences and Natural Sciences and life, Department of Material Sciences, Larbi Ben M’hidi University, Oum El Bouaghi, 04000, Algeria
(*) Corresponding Author

Received: 14 Nov 2016, Accepted: 14 Jan 2017, Published: 31 Mar 2017

Abstract


A new triazinane derivative was obtained by condensation reaction of pentylamine, 2-fluoroaniline and formaldehyde (formalin) in basic solution to yield 1,3-bis(2-fluorophenyl)-5-pentyl-1,3,5-triazinane. The structure of the synthesized compound was characterized by spectroscopic methods: FT-IR, UV-Vis, 13C, 19F and 1H NMR.


Keywords


Triazinane; Pentylamine; Formaldehyde; 2-Fluoroaniline; IR spectroscopy; Heterocyclic nitrogen compound

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DOI: 10.5155/eurjchem.8.1.18-19.1510

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Citations

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[1]. Leila Lefrada, Randolf Köhn, Souhila Malki, Wissam Mazouz, Ahcene Bouchemma, Meriem Hadjem
Synthesis and antimicrobial activity of 1,3-bis-butyl-5-(4-iodophenyl)-1,3,5-triazacyclohexane
European Journal of Chemistry  8(1), 82, 2017
DOI: 10.5155/eurjchem.8.1.82-84.1537
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References

[1]. Randolf, D. K.; Matthias, H.; Shahram, M.; Dieter, L. Chem. Commun. 2000, 19, 1927-1928.

[2]. Mahmoud, C.; Amel, M.; Duygu, B.; Ahcen, B.; Cemal, P. J. Mol. Struc. 2017, 1129, 152-159.
https://doi.org/10.1016/j.molstruc.2016.09.060

[3]. Bouchemma, A.; Peter, H. M.; George, A. S. J. Chem. Soc. Perkin Trans. II 1989, 6, 583-587.

[4]. Dilara, O.; Nihat, K. J. Taiwan Inst. Chem. Eng. 2015, 50, 306-313.

[5]. Saida, L.; Abdelhamid, M.; Gabriele, K. K.; Randolf, D. K.; Frank, S. Polyhedron 2010, 29, 1399-1404.
https://doi.org/10.1016/j.poly.2010.01.008

[6]. Guide, S. PhD Thesis, Synthesis and coordination chemistry of triazacyclohexane and orthoamides, Technischen Universitat, Berlin, 1999.

[7]. Lefrada, L.; Bouchemma, A.; Bouacida, S.; Claiser, N.; Souhassou, M. Acta Crystallogr. E 2007, 70(9), o1061-o1062.
https://doi.org/10.1107/S1600536814019060

[8]. Chebbah, M.; Bouchemma, A.; Bouacida, S.; Lefrada, L.; Bouhenguel, M. Acta Crystallogr. E 2007, 69(6), o976-o976.
https://doi.org/10.1107/S1600536813013743

[9]. Lefrada, L.; Bouchemma, A.; Bouhenguel, M.; Ferhati, A.; Chebbah, M. Eur. J. Chem. 2012, 3(4), 404-405.
https://doi.org/10.5155/eurjchem.3.4.404-405.657

[10]. Malki, S.; Lefrada, L.; Bouchemma, A.; Bouhenguel, M.; Chebbah, M.; Sid, A. Eur. J. Chem. 2016, 7(1), 137-138.
https://doi.org/10.5155/eurjchem.7.1.137-138.1337

[11]. Lefrada, L.; Köhn, R.; Malki, S.; Mazouz, W.; Bouchemma, A.; Hadjem, M. Eur. J. Chem. 2017, 8(1), 82-84.
https://doi.org/10.5155/eurjchem.8.1.82-84.1537


How to cite


Ferhati, A.; Bouchemma, A.; Bouhenguel, M.; Lefrada, L.; Sid, A. Eur. J. Chem. 2017, 8(1), 18-19. doi:10.5155/eurjchem.8.1.18-19.1510
Ferhati, A.; Bouchemma, A.; Bouhenguel, M.; Lefrada, L.; Sid, A. Synthesis and characterization of 1,3-bis(2-fluorophenyl)-5-pentyl-1,3,5-triazinane. Eur. J. Chem. 2017, 8(1), 18-19. doi:10.5155/eurjchem.8.1.18-19.1510
Ferhati, A., Bouchemma, A., Bouhenguel, M., Lefrada, L., & Sid, A. (2017). Synthesis and characterization of 1,3-bis(2-fluorophenyl)-5-pentyl-1,3,5-triazinane. European Journal of Chemistry, 8(1), 18-19. doi:10.5155/eurjchem.8.1.18-19.1510
Ferhati, Amel, Achene Bouchemma, Mustapha Bouhenguel, Leila Lefrada, & Assia Sid. "Synthesis and characterization of 1,3-bis(2-fluorophenyl)-5-pentyl-1,3,5-triazinane." European Journal of Chemistry [Online], 8.1 (2017): 18-19. Web. 21 Oct. 2019
Ferhati, Amel, Bouchemma, Achene, Bouhenguel, Mustapha, Lefrada, Leila, AND Sid, Assia. "Synthesis and characterization of 1,3-bis(2-fluorophenyl)-5-pentyl-1,3,5-triazinane" European Journal of Chemistry [Online], Volume 8 Number 1 (31 March 2017)

DOI Link: https://doi.org/10.5155/eurjchem.8.1.18-19.1510

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