#============================================================================= data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 14 _journal_issue 4 _journal_year 2023 _journal_page_first 428 _journal_page_last 437 #============================================================================= data_shelx _audit_creation_date 2023-08-31 # end Validation Reply Form _audit_creation_method ; Olex2 1.3-beta (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _shelx_SHELXL_version_number '2018/3' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C14 H11 Cu N3 O5, H2 O' _chemical_formula_sum 'C14 H13 Cu N3 O6' _chemical_formula_weight 382.81 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2yn' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 8.7355(11) _cell_length_b 17.646(2) _cell_length_c 9.8036(12) _cell_angle_alpha 90 _cell_angle_beta 98.506(6) _cell_angle_gamma 90 _cell_volume 1494.6(3) _cell_formula_units_Z 4 _cell_measurement_reflns_used 4989 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 24.991 _cell_measurement_theta_min 2.308 _shelx_estimated_absorpt_T_max ? _shelx_estimated_absorpt_T_min ? _exptl_absorpt_coefficient_mu 1.500 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.586 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details '(SADABS; Bruker, 2000)' _exptl_absorpt_special_details ? _exptl_crystal_colour blue _exptl_crystal_colour_primary blue _exptl_crystal_density_diffrn 1.701 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description rod _exptl_crystal_F_000 780 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.16 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0316 _diffrn_reflns_av_unetI/netI 0.0718 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 5120 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 24.991 _diffrn_reflns_theta_max 24.991 _diffrn_reflns_theta_min 2.308 _diffrn_ambient_temperature 296(2) _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source 'fine-focus sealed tube' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 1352 _reflns_number_total 1953 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX-II CCD' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _refine_diff_density_max 0.362 _refine_diff_density_min -0.300 _refine_diff_density_rms 0.088 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.929 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 223 _refine_ls_number_reflns 1953 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0585 _refine_ls_R_factor_gt 0.0380 _refine_ls_restrained_S_all 0.928 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0485P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0932 _refine_ls_wR_factor_ref 0.0972 _refine_special_details ? _olex2_refinement_description ; 1. Restrained distances Cu1-H5A \\sim Cu1-H5B with sigma of 0.02 2.a Free rotating group: O6(H6A,H6B), O5(H5A,H5B) 2.b Aromatic/amide H refined with riding coordinates: C3(H3), N1(H1), C12(H12), C4(H4), C1(H1A), C10(H10), C11(H11), C7(H7), C2(H2) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary ? _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O6 O 0.5600(8) 0.4808(3) 0.3648(11) 0.157(3) Uani 1 1 d G . . . . H6A H 0.542860 0.434329 0.345283 0.235 Uiso 1 1 d G U . . . H6B H 0.651855 0.481607 0.407923 0.235 Uiso 1 1 d G U . . . Cu1 Cu 0.72122(6) 0.15717(3) 0.41343(6) 0.0321(2) Uani 1 1 d D . . . . O1 O 0.6451(3) 0.26510(16) 0.3925(3) 0.0358(8) Uani 1 1 d . . . . . N2 N 0.9417(4) 0.17349(19) 0.4676(4) 0.0336(9) Uani 1 1 d . . . . . O4 O 0.4394(4) 0.33277(15) 0.3073(3) 0.0369(8) Uani 1 1 d . . . . . N3 N 0.5137(4) 0.13874(18) 0.3293(4) 0.0276(8) Uani 1 1 d . . . . . C3 C 1.2529(6) 0.3464(3) 0.5688(6) 0.0471(13) Uani 1 1 d . . . . . H3 H 1.327554 0.383483 0.593187 0.057 Uiso 1 1 calc R U . . . C8 C 0.5998(5) 0.0125(2) 0.3408(5) 0.0329(11) Uani 1 1 d . . . . . N1 N 1.1722(4) 0.1421(2) 0.5680(4) 0.0365(9) Uani 1 1 d . . . . . H1 H 1.248369 0.114095 0.603508 0.044 Uiso 1 1 calc R U . . . C9 C 0.4674(5) 0.0676(2) 0.3029(5) 0.0300(10) Uani 1 1 d . . . . . O3 O 0.5752(4) -0.05553(16) 0.3267(4) 0.0457(9) Uani 1 1 d . . . . . O2 O 0.7296(4) 0.04239(16) 0.3844(4) 0.0466(9) Uani 1 1 d . . . . . O5 O 0.6712(4) 0.14405(18) 0.6301(3) 0.0490(9) Uani 1 1 d G . . . . H5A H 0.607352 0.112676 0.655758 0.074 Uiso 1 1 d DG U . . . H5B H 0.736539 0.151905 0.701992 0.074 Uiso 1 1 d DG U . . . C14 C 0.5060(5) 0.2727(2) 0.3354(4) 0.0296(10) Uani 1 1 d . . . . . C12 C 0.2703(5) 0.1867(3) 0.2363(5) 0.0390(12) Uani 1 1 d . . . . . H12 H 0.203785 0.227468 0.213859 0.047 Uiso 1 1 calc R U . . . C4 C 1.2895(6) 0.2735(3) 0.5975(5) 0.0435(12) Uani 1 1 d . . . . . H4 H 1.386905 0.259654 0.642218 0.052 Uiso 1 1 calc R U . . . C6 C 1.0285(5) 0.2398(2) 0.4929(4) 0.0302(10) Uani 1 1 d . . . . . C1 C 0.9903(6) 0.3155(3) 0.4630(5) 0.0378(11) Uani 1 1 d . . . . . H1A H 0.892941 0.329577 0.418705 0.045 Uiso 1 1 calc R U . . . C10 C 0.3193(5) 0.0531(2) 0.2431(5) 0.0394(12) Uani 1 1 d . . . . . H10 H 0.285312 0.003703 0.225162 0.047 Uiso 1 1 calc R U . . . C11 C 0.2210(5) 0.1138(2) 0.2097(5) 0.0443(13) Uani 1 1 d . . . . . H11 H 0.119666 0.105035 0.168519 0.053 Uiso 1 1 calc R U . . . C7 C 1.0339(5) 0.1177(2) 0.5150(4) 0.0303(10) Uani 1 1 d . . . . . H7 H 1.004871 0.066952 0.511580 0.036 Uiso 1 1 calc R U . . . C13 C 0.4210(5) 0.1981(2) 0.2973(4) 0.0268(10) Uani 1 1 d . . . . . C2 C 1.1051(6) 0.3683(3) 0.5030(5) 0.0433(12) Uani 1 1 d . . . . . H2 H 1.084344 0.419365 0.486115 0.052 Uiso 1 1 calc R U . . . C5 C 1.1746(5) 0.2193(2) 0.5572(5) 0.0334(11) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O6 0.143(6) 0.049(3) 0.266(9) -0.016(4) -0.013(6) -0.024(3) Cu1 0.0213(3) 0.0258(3) 0.0453(4) 0.0003(2) -0.0080(3) -0.0001(2) O1 0.0293(18) 0.0265(16) 0.048(2) 0.0009(14) -0.0055(17) -0.0022(13) N2 0.026(2) 0.028(2) 0.043(2) -0.0007(16) -0.006(2) -0.0017(16) O4 0.0357(19) 0.0251(17) 0.0466(19) -0.0008(13) -0.0046(18) 0.0076(14) N3 0.0238(19) 0.028(2) 0.0286(19) -0.0023(15) -0.0057(18) -0.0004(16) C3 0.038(3) 0.049(3) 0.055(3) -0.006(2) 0.011(3) -0.019(2) C8 0.024(2) 0.028(3) 0.045(3) 0.0062(19) 0.001(2) -0.0008(19) N1 0.024(2) 0.037(2) 0.047(2) 0.0018(17) -0.003(2) 0.0050(17) C9 0.030(3) 0.023(2) 0.037(3) 0.0010(18) 0.000(2) 0.0028(18) O3 0.0294(17) 0.0211(18) 0.082(3) 0.0010(15) -0.006(2) -0.0020(13) O2 0.0256(17) 0.0289(17) 0.079(3) 0.0000(16) -0.014(2) 0.0007(13) O5 0.047(2) 0.052(2) 0.044(2) 0.0073(16) -0.0066(19) -0.0251(17) C14 0.032(3) 0.027(2) 0.030(2) -0.0035(19) 0.004(2) 0.000(2) C12 0.028(3) 0.034(3) 0.052(3) 0.004(2) -0.003(3) 0.006(2) C4 0.025(3) 0.058(4) 0.046(3) -0.003(2) 0.001(2) -0.013(2) C6 0.027(2) 0.031(2) 0.033(2) -0.0003(19) 0.007(2) -0.0069(19) C1 0.032(3) 0.040(3) 0.039(3) 0.006(2) -0.001(2) 0.001(2) C10 0.028(3) 0.024(2) 0.061(3) 0.000(2) -0.009(3) -0.0009(19) C11 0.021(2) 0.041(3) 0.066(3) -0.002(2) -0.009(3) -0.002(2) C7 0.026(2) 0.024(2) 0.039(3) 0.0011(19) -0.001(2) 0.003(2) C13 0.023(2) 0.026(2) 0.030(2) 0.0018(17) -0.001(2) 0.0032(19) C2 0.047(3) 0.033(3) 0.051(3) 0.000(2) 0.011(3) -0.008(2) C5 0.024(2) 0.040(3) 0.036(3) 0.000(2) 0.005(2) 0.000(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O6 H6A 0.8499 . ? O6 H6B 0.8500 . ? Cu1 O1 2.018(3) . ? Cu1 N2 1.942(4) . ? Cu1 N3 1.905(4) . ? Cu1 O2 2.048(3) . ? Cu1 O5 2.243(3) . ? O1 C14 1.267(5) . ? N2 C6 1.396(5) . ? N2 C7 1.313(5) . ? O4 C14 1.221(5) . ? N3 C9 1.334(5) . ? N3 C13 1.333(5) . ? C3 H3 0.9300 . ? C3 C4 1.345(7) . ? C3 C2 1.410(7) . ? C8 C9 1.514(6) . ? C8 O3 1.224(5) . ? C8 O2 1.266(5) . ? N1 H1 0.8600 . ? N1 C7 1.314(5) . ? N1 C5 1.367(5) . ? C9 C10 1.363(6) . ? O5 H5A 0.8501 . ? O5 H5B 0.8500 . ? C14 C13 1.530(6) . ? C12 H12 0.9300 . ? C12 C11 1.369(6) . ? C12 C13 1.378(6) . ? C4 H4 0.9300 . ? C4 C5 1.400(6) . ? C6 C1 1.397(6) . ? C6 C5 1.386(6) . ? C1 H1A 0.9300 . ? C1 C2 1.382(7) . ? C10 H10 0.9300 . ? C10 C11 1.381(6) . ? C11 H11 0.9300 . ? C7 H7 0.9300 . ? C2 H2 0.9300 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag H6A O6 H6B 104.5 . . ? O1 Cu1 O2 159.60(12) . . ? O1 Cu1 O5 94.94(13) . . ? N2 Cu1 O1 100.75(13) . . ? N2 Cu1 O2 97.50(13) . . ? N2 Cu1 O5 94.62(15) . . ? N3 Cu1 O1 80.72(13) . . ? N3 Cu1 N2 170.16(16) . . ? N3 Cu1 O2 79.76(13) . . ? N3 Cu1 O5 94.95(14) . . ? O2 Cu1 O5 92.60(13) . . ? C14 O1 Cu1 115.1(3) . . ? C6 N2 Cu1 131.6(3) . . ? C7 N2 Cu1 121.2(3) . . ? C7 N2 C6 106.0(4) . . ? C9 N3 Cu1 119.2(3) . . ? C13 N3 Cu1 118.3(3) . . ? C13 N3 C9 122.6(4) . . ? C4 C3 H3 119.0 . . ? C4 C3 C2 122.1(5) . . ? C2 C3 H3 119.0 . . ? O3 C8 C9 119.1(4) . . ? O3 C8 O2 125.5(4) . . ? O2 C8 C9 115.4(4) . . ? C7 N1 H1 125.7 . . ? C7 N1 C5 108.6(3) . . ? C5 N1 H1 125.7 . . ? N3 C9 C8 110.9(4) . . ? N3 C9 C10 120.1(4) . . ? C10 C9 C8 128.9(4) . . ? C8 O2 Cu1 114.2(3) . . ? Cu1 O5 H5A 125.1 . . ? Cu1 O5 H5B 124.6 . . ? H5A O5 H5B 104.5 . . ? O1 C14 C13 114.6(4) . . ? O4 C14 O1 125.8(4) . . ? O4 C14 C13 119.6(4) . . ? C11 C12 H12 120.9 . . ? C11 C12 C13 118.2(4) . . ? C13 C12 H12 120.9 . . ? C3 C4 H4 121.4 . . ? C3 C4 C5 117.1(5) . . ? C5 C4 H4 121.4 . . ? N2 C6 C1 131.1(4) . . ? C5 C6 N2 107.5(4) . . ? C5 C6 C1 121.4(4) . . ? C6 C1 H1A 121.8 . . ? C2 C1 C6 116.4(5) . . ? C2 C1 H1A 121.8 . . ? C9 C10 H10 120.8 . . ? C9 C10 C11 118.3(4) . . ? C11 C10 H10 120.8 . . ? C12 C11 C10 121.1(5) . . ? C12 C11 H11 119.5 . . ? C10 C11 H11 119.5 . . ? N2 C7 N1 112.0(4) . . ? N2 C7 H7 124.0 . . ? N1 C7 H7 124.0 . . ? N3 C13 C14 111.3(4) . . ? N3 C13 C12 119.7(4) . . ? C12 C13 C14 129.0(4) . . ? C3 C2 H2 119.3 . . ? C1 C2 C3 121.5(5) . . ? C1 C2 H2 119.3 . . ? N1 C5 C4 132.7(4) . . ? N1 C5 C6 105.8(4) . . ? C6 C5 C4 121.6(4) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cu1 O1 C14 O4 -176.5(4) . . . . ? Cu1 O1 C14 C13 1.8(4) . . . . ? Cu1 N2 C6 C1 -13.7(7) . . . . ? Cu1 N2 C6 C5 167.0(3) . . . . ? Cu1 N2 C7 N1 -169.0(3) . . . . ? Cu1 N3 C9 C8 -3.1(5) . . . . ? Cu1 N3 C9 C10 179.8(3) . . . . ? Cu1 N3 C13 C14 0.7(5) . . . . ? Cu1 N3 C13 C12 180.0(3) . . . . ? O1 C14 C13 N3 -1.6(5) . . . . ? O1 C14 C13 C12 179.1(4) . . . . ? N2 C6 C1 C2 179.9(4) . . . . ? N2 C6 C5 N1 0.4(5) . . . . ? N2 C6 C5 C4 -179.4(4) . . . . ? O4 C14 C13 N3 176.8(4) . . . . ? O4 C14 C13 C12 -2.5(7) . . . . ? N3 C9 C10 C11 0.8(7) . . . . ? C3 C4 C5 N1 179.1(5) . . . . ? C3 C4 C5 C6 -1.2(7) . . . . ? C8 C9 C10 C11 -175.7(5) . . . . ? C9 N3 C13 C14 -178.3(4) . . . . ? C9 N3 C13 C12 1.0(6) . . . . ? C9 C8 O2 Cu1 6.7(5) . . . . ? C9 C10 C11 C12 -0.2(8) . . . . ? O3 C8 C9 N3 177.8(4) . . . . ? O3 C8 C9 C10 -5.5(8) . . . . ? O3 C8 O2 Cu1 -173.8(4) . . . . ? O2 C8 C9 N3 -2.7(6) . . . . ? O2 C8 C9 C10 174.0(5) . . . . ? C4 C3 C2 C1 -0.8(8) . . . . ? C6 N2 C7 N1 -0.2(5) . . . . ? C6 C1 C2 C3 0.7(7) . . . . ? C1 C6 C5 N1 -179.0(4) . . . . ? C1 C6 C5 C4 1.2(7) . . . . ? C11 C12 C13 N3 -0.5(6) . . . . ? C11 C12 C13 C14 178.7(5) . . . . ? C7 N2 C6 C1 179.2(5) . . . . ? C7 N2 C6 C5 -0.1(5) . . . . ? C7 N1 C5 C4 179.2(5) . . . . ? C7 N1 C5 C6 -0.5(5) . . . . ? C13 N3 C9 C8 175.9(4) . . . . ? C13 N3 C9 C10 -1.2(7) . . . . ? C13 C12 C11 C10 0.1(7) . . . . ? C2 C3 C4 C5 1.0(8) . . . . ? C5 N1 C7 N2 0.5(5) . . . . ? C5 C6 C1 C2 -0.9(7) . . . . ? _shelx_res_file ; TITL shelxt_a.res in P2(1)/n shelx.res created by SHELXL-2018/3 at 08:49:04 on 05-Aug-2023 CELL 0.71073 8.7355 17.6464 9.8036 90.000 98.506 90.000 ZERR 4.00 0.0011 0.0022 0.0012 0.000 0.006 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H N O CU UNIT 56 52 12 24 4 MERG 2 OMIT -1.00 50.00 SADI Cu1 H5a Cu1 H5b MORE -1 FMAP 2 PLAN 5 ACTA BOND $H CONF L.S. 10 TEMP 23.00 WGHT 0.048500 FVAR 0.23148 AFIX 6 O6 4 0.559974 0.480774 0.364845 11.00000 0.14290 0.04892 = 0.26576 -0.01632 -0.01317 -0.02404 H6A 2 0.542860 0.434329 0.345283 11.00000 -1.50000 H6B 2 0.651855 0.481607 0.407923 11.00000 -1.50000 AFIX 0 CU1 5 0.721220 0.157168 0.413427 11.00000 0.02128 0.02578 = 0.04530 0.00030 -0.00796 -0.00009 O1 4 0.645052 0.265099 0.392528 11.00000 0.02926 0.02653 = 0.04824 0.00092 -0.00547 -0.00216 N2 3 0.941650 0.173492 0.467587 11.00000 0.02629 0.02786 = 0.04317 -0.00072 -0.00625 -0.00167 O4 4 0.439376 0.332773 0.307252 11.00000 0.03573 0.02511 = 0.04659 -0.00077 -0.00458 0.00761 N3 3 0.513743 0.138744 0.329328 11.00000 0.02380 0.02761 = 0.02862 -0.00234 -0.00572 -0.00038 C3 1 1.252945 0.346359 0.568833 11.00000 0.03846 0.04918 = 0.05506 -0.00617 0.01145 -0.01933 AFIX 43 H3 2 1.327554 0.383483 0.593187 11.00000 -1.20000 AFIX 0 C8 1 0.599793 0.012530 0.340800 11.00000 0.02384 0.02830 = 0.04529 0.00624 0.00118 -0.00081 N1 3 1.172153 0.142067 0.567984 11.00000 0.02354 0.03670 = 0.04669 0.00184 -0.00330 0.00502 AFIX 43 H1 2 1.248369 0.114095 0.603508 11.00000 -1.20000 AFIX 0 C9 1 0.467378 0.067555 0.302895 11.00000 0.02955 0.02254 = 0.03658 0.00100 0.00043 0.00276 O3 4 0.575185 -0.055528 0.326732 11.00000 0.02936 0.02114 = 0.08216 0.00103 -0.00626 -0.00198 O2 4 0.729551 0.042394 0.384415 11.00000 0.02557 0.02891 = 0.07884 -0.00002 -0.01371 0.00071 AFIX 6 O5 4 0.671221 0.144054 0.630100 11.00000 0.04663 0.05239 = 0.04401 0.00731 -0.00665 -0.02509 H5A 2 0.607352 0.112676 0.655758 11.00000 -1.50000 H5B 2 0.736539 0.151905 0.701992 11.00000 -1.50000 AFIX 0 C14 1 0.505999 0.272696 0.335443 11.00000 0.03177 0.02677 = 0.02995 -0.00351 0.00356 0.00006 C12 1 0.270281 0.186729 0.236327 11.00000 0.02802 0.03436 = 0.05189 0.00444 -0.00284 0.00563 AFIX 43 H12 2 0.203785 0.227468 0.213859 11.00000 -1.20000 AFIX 0 C4 1 1.289513 0.273463 0.597523 11.00000 0.02488 0.05780 = 0.04650 -0.00270 0.00131 -0.01261 AFIX 43 H4 2 1.386905 0.259654 0.642218 11.00000 -1.20000 AFIX 0 C6 1 1.028506 0.239788 0.492878 11.00000 0.02663 0.03131 = 0.03339 -0.00028 0.00726 -0.00692 C1 1 0.990305 0.315475 0.463044 11.00000 0.03235 0.04006 = 0.03898 0.00603 -0.00115 0.00139 AFIX 43 H1A 2 0.892941 0.329577 0.418705 11.00000 -1.20000 AFIX 0 C10 1 0.319312 0.053147 0.243077 11.00000 0.02846 0.02357 = 0.06150 0.00037 -0.00922 -0.00086 AFIX 43 H10 2 0.285312 0.003703 0.225162 11.00000 -1.20000 AFIX 0 C11 1 0.220988 0.113834 0.209719 11.00000 0.02107 0.04095 = 0.06612 -0.00166 -0.00878 -0.00225 AFIX 43 H11 2 0.119666 0.105035 0.168519 11.00000 -1.20000 AFIX 0 C7 1 1.033913 0.117699 0.515035 11.00000 0.02630 0.02377 = 0.03908 0.00109 -0.00081 0.00261 AFIX 43 H7 2 1.004871 0.066952 0.511580 11.00000 -1.20000 AFIX 0 C13 1 0.421048 0.198124 0.297287 11.00000 0.02335 0.02599 = 0.02957 0.00177 -0.00123 0.00316 C2 1 1.105108 0.368256 0.503020 11.00000 0.04689 0.03331 = 0.05083 0.00023 0.01105 -0.00756 AFIX 43 H2 2 1.084344 0.419365 0.486115 11.00000 -1.20000 AFIX 0 C5 1 1.174625 0.219257 0.557195 11.00000 0.02426 0.03983 = 0.03610 -0.00047 0.00474 -0.00009 HKLF 4 REM shelxt_a.res in P2(1)/n REM wR2 = 0.0972, GooF = S = 0.929, Restrained GooF = 0.928 for all data REM R1 = 0.0380 for 1352 Fo > 4sig(Fo) and 0.0585 for all 1953 data REM 223 parameters refined using 1 restraints END WGHT 0.0485 0.0000 REM Highest difference peak 0.362, deepest hole -0.300, 1-sigma level 0.088 Q1 1 0.6519 0.4592 0.3841 11.00000 0.05 0.36 Q2 1 0.5029 0.4966 0.4431 11.00000 0.05 0.31 Q3 1 0.9533 0.4070 0.3517 11.00000 0.05 0.28 Q4 1 0.7315 0.4374 0.2899 11.00000 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1 10.10 3.10 -10 4 1 13.60 3.60 11 4 -2 1.20 3.20 11 4 2 -1.10 3.80 10 4 2 13.30 4.50 9 4 -2 14.90 3.30 9 4 -2 20.30 4.40 9 4 2 21.20 4.40 9 4 2 18.90 3.10 9 4 2 17.00 4.40 8 4 -2 22.20 3.90 8 4 -2 20.20 3.50 8 4 2 26.80 5.20 8 4 2 23.30 3.00 8 4 2 23.50 3.10 4 4 -2 13.80 2.00 4 4 -2 14.20 2.10 4 4 2 11.50 1.60 4 4 2 10.80 2.20 4 4 2 10.70 1.40 -2 -4 -2 348.47 13.20 -2 -4 -2 362.76 13.60 2 4 2 360.66 13.50 2 4 2 347.07 14.40 0 -4 -2 140.49 7.00 0 -4 -2 130.59 5.90 0 -4 2 127.09 5.50 0 -4 2 128.59 5.40 0 4 2 127.49 5.90 -1 4 2 18.60 3.00 -2 4 -2 355.46 14.10 2 -4 2 346.27 13.10 3 -4 -2 216.78 9.50 -3 4 2 217.68 9.60 -4 4 -2 11.30 2.40 4 -4 -2 9.80 2.30 -4 4 2 13.60 2.40 5 -4 -2 116.19 6.40 -5 4 2 112.39 6.50 -7 4 2 148.29 8.20 -8 4 2 24.80 4.10 -9 4 2 16.80 3.70 -10 4 2 7.40 3.50 -11 4 2 -0.50 2.80 11 4 3 2.10 4.40 10 4 3 -0.20 3.60 9 4 3 -0.40 3.20 8 4 -3 1.90 2.00 8 4 3 -0.90 2.80 8 4 3 -1.20 1.30 8 4 3 -0.80 1.30 7 4 3 4.30 1.50 7 4 3 3.10 2.70 7 4 3 4.40 1.20 5 4 3 53.69 3.20 5 4 3 51.39 2.80 5 4 3 51.79 5.10 3 4 -3 125.49 5.80 -3 -4 -3 117.59 5.30 -3 -4 -3 115.99 4.90 3 4 3 116.49 6.70 -3 -4 3 123.69 5.90 1 4 -3 114.99 5.20 1 4 -3 117.29 5.50 -1 -4 3 121.89 5.40 0 -4 -3 133.39 6.20 0 4 -3 129.29 5.70 0 4 -3 131.19 5.50 0 4 3 132.69 6.30 0 -4 3 129.59 5.60 -1 4 -3 38.80 2.20 1 -4 3 40.50 2.20 1 -4 3 38.00 2.20 2 -4 -3 194.88 8.80 -2 4 3 192.58 8.80 -3 4 -3 118.29 6.30 3 -4 -3 124.99 6.40 -3 4 3 118.89 6.40 3 -4 3 116.19 4.90 -5 4 -3 53.49 4.20 -6 4 3 67.59 5.60 -7 4 3 11.00 3.10 -8 4 3 1.20 2.50 -9 4 3 -0.40 2.70 -10 4 3 0.40 3.00 -11 4 3 -0.70 3.10 10 4 4 5.00 4.60 9 4 4 20.60 5.20 8 4 -4 46.00 5.10 8 4 4 27.80 6.40 7 4 4 29.10 2.50 7 4 4 27.00 5.60 6 4 4 15.30 3.60 -2 -4 -4 109.79 5.00 -2 -4 -4 112.39 4.50 -2 -4 -4 113.69 5.60 2 4 4 112.39 6.50 -1 -4 -4 92.89 5.00 1 4 4 87.09 4.80 1 4 4 88.69 5.50 0 4 -4 2.50 0.80 0 -4 -4 3.70 1.40 0 4 -4 2.60 0.80 0 4 4 1.90 1.50 0 -4 4 2.90 0.80 0 4 4 3.10 1.40 3 -4 -4 -0.80 1.20 -3 4 4 -0.50 1.50 -6 4 4 38.00 4.70 -7 4 4 0.40 2.30 -8 4 4 43.70 5.70 -9 4 4 24.80 5.20 -10 4 4 3.20 3.20 -11 4 4 7.10 4.60 10 4 5 -1.30 4.20 9 4 5 8.20 4.60 8 4 5 10.30 4.30 7 4 -5 27.60 4.20 7 4 5 22.90 4.80 5 4 -5 10.50 2.30 -3 -4 -5 4.30 1.10 3 4 -5 8.70 2.40 -3 -4 -5 4.80 1.70 3 4 -5 7.90 1.70 3 4 5 3.70 2.20 1 4 -5 110.59 5.60 -1 -4 -5 123.89 6.30 -1 -4 5 113.39 5.80 1 4 5 124.59 6.20 1 4 5 122.49 7.10 0 -4 -5 26.60 3.10 0 4 -5 32.80 2.50 0 4 -5 33.50 2.30 0 4 5 28.30 3.30 0 4 5 27.50 3.60 0 -4 5 28.50 2.50 1 -4 -5 115.79 6.60 -1 4 -5 125.49 5.40 -1 4 5 111.99 6.70 1 -4 5 127.59 5.50 2 -4 -5 66.39 5.00 -2 4 5 67.29 5.20 3 -4 5 3.80 0.80 -3 4 5 6.40 2.30 -5 4 5 10.40 2.80 -7 4 5 29.00 4.90 -8 4 5 47.00 6.00 -9 4 5 9.10 3.60 -10 4 5 4.30 3.50 9 4 6 -1.10 4.10 8 4 6 -0.50 3.70 7 4 -6 14.30 3.70 5 4 -6 2.90 1.70 5 4 6 6.70 3.30 -4 -4 -6 46.20 3.70 -3 -4 -6 152.78 7.80 -3 -4 -6 155.08 6.50 3 4 6 153.28 9.40 -2 -4 -6 89.59 4.40 -2 -4 -6 90.09 5.70 2 4 6 95.99 6.70 -1 -4 -6 35.50 3.70 1 4 -6 35.20 3.00 1 4 6 37.20 4.40 0 -4 -6 34.00 3.60 0 4 -6 32.90 2.80 0 4 -6 35.30 2.50 0 4 6 31.90 4.20 0 4 6 26.90 3.70 0 -4 6 31.00 2.70 -1 4 -6 37.00 2.60 1 -4 -6 40.20 4.00 -1 4 6 39.80 4.30 1 -4 6 36.30 2.70 -4 4 6 6.70 2.70 -5 4 6 3.70 2.70 -7 4 6 14.80 3.80 -8 4 6 1.50 3.00 -9 4 6 0.90 3.30 -10 4 6 1.40 3.60 9 4 7 5.40 5.20 8 4 7 21.80 5.90 7 4 7 43.40 7.90 6 4 -7 27.00 4.30 6 4 7 32.00 6.70 5 4 7 15.10 4.10 -3 -4 -7 20.90 2.00 -3 -4 -7 26.30 3.60 3 4 7 23.70 5.00 -1 -4 -7 16.20 3.20 1 4 7 13.40 3.20 0 4 -7 12.30 2.20 0 4 -7 13.30 2.00 0 -4 -7 17.80 3.40 0 4 7 12.80 3.10 -3 4 7 1.10 2.50 -4 4 7 0.70 2.30 -5 4 7 0.40 2.60 -6 4 -7 28.30 4.90 -6 4 7 24.90 5.10 -7 4 7 2.20 3.20 -8 4 7 0.40 3.20 -9 4 7 17.30 5.10 8 4 8 3.10 4.60 7 4 8 5.10 4.40 6 4 8 6.80 4.20 4 4 -8 10.40 2.50 4 4 8 7.60 3.70 3 4 -8 17.10 2.70 -3 -4 8 23.80 3.50 2 4 -8 8.50 2.00 2 4 8 0.00 2.30 -1 -4 -8 1.40 2.20 -1 -4 -8 -0.10 1.00 1 4 8 2.30 2.60 0 -4 -8 15.90 3.50 0 4 -8 13.30 2.20 0 4 -8 10.20 2.00 0 4 8 12.00 3.40 -1 4 -8 0.60 1.30 -3 4 8 24.10 4.70 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0 71.09 3.50 1 5 0 67.99 3.70 0 -5 0 1.20 0.60 0 -5 0 1.10 0.80 0 5 0 0.90 0.80 1 -5 0 69.09 3.90 -1 5 0 72.29 4.00 -2 5 0 108.79 5.50 2 -5 0 110.59 5.50 3 -5 0 13.20 2.10 -3 5 0 11.00 2.10 -4 5 0 287.07 12.30 4 -5 0 291.97 12.20 -5 5 0 1.80 1.80 5 -5 0 4.30 1.70 -6 5 0 131.09 7.20 -7 5 0 12.90 2.90 -8 5 0 62.19 5.20 -9 5 0 17.80 4.00 11 5 -1 0.90 2.90 10 5 -1 -1.00 2.40 10 5 1 -1.20 3.10 10 5 1 0.20 2.50 8 5 -1 4.30 2.30 8 5 -1 4.90 2.30 8 5 -1 7.20 2.10 8 5 1 1.30 1.70 8 5 1 0.40 1.50 8 5 1 0.20 2.40 7 5 -1 35.50 4.20 7 5 -1 40.50 3.90 7 5 -1 40.30 4.10 6 5 -1 16.80 2.70 6 5 -1 15.70 2.80 6 5 -1 12.40 2.40 5 5 1 60.49 4.00 5 5 1 64.49 3.70 5 5 1 61.79 4.80 -4 -5 -1 6.50 1.30 4 5 1 6.00 1.40 4 5 1 7.50 1.90 4 5 1 4.90 1.10 -2 -5 -1 95.29 4.50 -1 -5 -1 116.39 5.40 -1 -5 -1 115.39 5.60 1 5 -1 132.99 5.90 1 5 -1 136.99 5.40 1 5 -1 138.69 5.70 -1 -5 -1 122.19 6.70 -1 -5 1 136.69 5.50 1 5 1 113.99 5.40 -1 -5 1 142.89 5.80 1 5 1 109.89 5.50 0 5 -1 4.30 0.90 0 -5 -1 6.00 1.20 0 5 1 5.40 1.20 0 -5 1 5.30 1.20 0 -5 1 5.40 1.00 1 -5 -1 132.59 5.80 -1 5 -1 112.59 5.70 -1 5 1 129.29 5.90 1 -5 1 115.39 5.20 1 -5 1 116.89 5.80 4 -5 -1 18.30 2.60 -4 5 1 17.80 2.80 5 -5 -1 117.49 6.30 -5 5 1 108.69 6.40 -6 5 1 13.90 3.20 -7 5 1 33.40 4.20 -8 5 -1 1.30 2.10 -8 5 1 4.30 2.60 -9 5 1 2.70 2.70 -10 5 1 -0.50 2.70 -11 5 1 0.50 2.90 11 5 -2 -0.20 4.50 9 5 -2 -0.60 2.10 9 5 2 0.70 1.80 9 5 2 -0.20 3.10 7 5 2 5.40 2.80 7 5 2 7.40 1.80 7 5 2 7.60 1.60 6 5 2 92.09 6.70 6 5 2 98.19 5.30 6 5 2 93.19 4.80 5 5 2 23.70 3.80 5 5 2 25.00 2.50 5 5 2 26.80 2.20 -2 -5 -2 11.30 1.20 2 5 -2 9.20 1.40 2 5 -2 9.70 1.50 -2 -5 -2 11.30 1.40 2 5 2 11.60 1.50 2 5 2 11.20 1.40 -2 -5 2 8.20 1.40 2 5 2 12.20 2.20 0 5 -2 23.90 1.80 0 -5 -2 23.10 2.10 0 -5 2 24.70 1.70 0 5 2 24.40 2.20 0 -5 2 23.90 1.90 -2 5 -2 10.80 2.00 2 -5 -2 9.40 1.70 -2 5 2 8.20 1.80 2 -5 2 10.70 1.20 3 -5 -2 149.19 7.20 -3 5 2 144.69 7.30 5 -5 -2 7.20 2.80 -5 5 2 4.60 2.10 -6 5 2 31.70 4.10 -7 5 2 17.50 3.80 -8 5 2 59.59 5.60 -9 5 2 0.90 2.60 -10 5 2 20.10 4.30 -11 5 2 -0.50 3.00 11 5 3 1.30 4.30 10 5 3 2.10 3.90 9 5 3 33.60 6.70 8 5 3 18.50 2.90 8 5 3 19.40 4.40 7 5 -3 70.59 5.70 7 5 3 85.49 4.40 7 5 3 87.99 4.90 7 5 3 87.19 7.30 6 5 3 21.40 2.00 6 5 3 21.00 2.40 6 5 3 18.50 4.30 5 5 -3 155.08 8.40 5 5 -3 168.28 7.60 5 5 3 129.39 6.50 5 5 3 125.99 8.30 4 5 -3 7.50 1.50 4 5 3 4.70 1.20 4 5 3 4.80 2.10 -3 -5 -3 83.19 4.20 -3 -5 -3 81.19 3.80 3 5 3 81.09 5.50 2 5 -3 12.60 1.70 -2 -5 -3 7.80 1.70 2 5 -3 12.90 1.90 -2 -5 -3 9.90 1.40 -2 -5 -3 10.50 1.10 2 5 3 10.70 1.70 -2 -5 3 13.40 1.80 2 5 3 11.20 2.50 0 5 -3 33.10 2.30 0 -5 -3 34.50 2.80 0 -5 3 33.90 2.20 0 5 3 31.30 2.80 2 -5 -3 10.70 2.10 -2 5 3 10.90 2.30 2 -5 3 9.50 1.20 3 -5 -3 42.80 3.70 -3 5 3 40.80 3.80 -4 5 -3 3.90 1.80 4 -5 -3 10.40 2.40 4 -5 3 5.80 1.10 -4 5 3 7.50 2.10 -5 5 -3 125.49 7.50 -5 5 3 160.48 8.20 -7 5 3 69.09 6.00 -8 5 3 6.90 3.10 -9 5 3 44.80 5.60 -10 5 3 7.30 3.70 -11 5 3 7.20 3.80 10 5 4 17.80 5.60 9 5 4 2.00 3.70 8 5 -4 12.00 3.40 8 5 4 2.80 3.60 7 5 -4 2.20 1.80 7 5 4 0.50 1.30 7 5 4 0.70 2.90 5 5 4 17.00 3.40 -2 -5 -4 98.39 5.30 -2 -5 -4 102.69 4.30 -2 -5 -4 96.89 4.70 2 5 4 96.29 5.00 2 5 4 101.59 6.20 0 5 -4 45.50 3.00 0 -5 -4 48.60 3.60 0 5 -4 45.70 2.80 0 5 4 47.30 3.70 0 -5 4 48.30 2.90 2 -5 -4 165.08 8.30 -2 5 4 164.68 8.40 3 -5 -4 16.50 2.90 -3 5 4 14.00 3.00 -4 5 -4 36.10 3.90 4 -5 4 36.00 2.10 -5 5 -4 15.90 3.50 5 -5 4 16.60 1.60 -7 5 -4 -0.80 2.20 -7 5 4 2.90 2.60 -8 5 4 11.30 3.70 -9 5 4 3.10 3.20 -10 5 4 -0.70 3.10 10 5 5 0.30 4.40 9 5 5 -0.20 3.80 8 5 5 -2.10 3.20 7 5 5 17.40 4.50 6 5 -5 1.90 1.80 6 5 5 -0.20 2.70 4 5 5 23.10 4.50 -3 -5 -5 219.98 8.90 -3 -5 -5 207.58 9.50 3 5 5 203.48 10.90 -2 -5 -5 11.10 2.30 -2 -5 -5 10.60 1.50 2 5 5 7.60 2.20 1 5 -5 73.79 4.10 1 5 -5 75.29 4.50 -1 -5 -5 70.49 4.80 1 5 5 70.19 5.50 1 5 5 69.59 4.70 -1 -5 5 80.39 4.50 0 5 -5 0.60 0.80 0 -5 -5 0.20 1.40 0 5 -5 0.40 0.90 0 5 5 -0.60 1.40 0 -5 5 0.20 0.80 0 5 5 -1.10 1.50 -1 5 -5 70.49 3.80 1 -5 -5 79.99 5.20 1 -5 5 68.89 3.90 -1 5 5 78.49 5.40 -2 5 5 -0.50 1.80 -4 5 -5 20.80 4.00 4 -5 5 22.30 2.00 -6 5 -5 -0.90 2.00 -6 5 5 2.20 2.50 -7 5 5 0.70 2.70 -8 5 5 5.40 3.30 -9 5 5 33.20 5.80 -10 5 5 0.40 3.10 9 5 6 -0.70 4.10 8 5 6 39.40 7.70 7 5 6 4.70 3.80 6 5 -6 50.19 4.90 5 5 6 11.00 3.60 -4 -5 -6 82.49 5.40 4 5 6 109.29 8.10 3 5 -6 2.70 1.40 -3 -5 -6 0.50 0.90 -3 -5 -6 -0.80 1.70 3 5 6 -0.70 2.10 -2 -5 -6 21.40 3.40 -2 -5 -6 19.20 2.00 2 5 6 22.40 4.20 -1 -5 -6 3.10 1.90 1 5 -6 3.30 1.20 1 5 -6 3.60 1.50 1 5 6 1.30 2.00 -1 -5 6 4.20 1.40 0 5 -6 26.40 2.40 0 5 -6 24.50 2.50 0 -5 -6 24.70 3.50 0 5 6 19.10 3.80 0 -5 6 21.90 2.60 0 5 6 20.40 3.60 -1 5 -6 2.40 1.10 1 -5 -6 5.50 2.20 1 -5 6 2.50 1.10 -1 5 6 3.30 2.10 3 -5 6 0.80 0.90 -3 5 6 1.50 2.20 -5 5 -6 9.60 3.10 -5 5 6 1.20 2.40 -6 5 -6 79.89 6.50 -7 5 -6 6.60 3.20 -7 5 6 0.20 2.80 -8 5 6 11.00 4.00 -9 5 6 3.50 3.60 -10 5 6 11.30 5.50 9 5 7 11.90 5.70 8 5 7 -0.30 4.00 7 5 7 0.90 3.90 6 5 -7 1.50 1.90 6 5 7 0.60 3.20 4 5 -7 3.70 1.80 4 5 7 1.20 2.80 -3 -5 -7 35.20 4.50 3 5 -7 33.30 3.50 -3 -5 7 34.30 3.00 3 5 7 29.90 5.40 2 5 -7 1.60 1.30 -2 -5 -7 2.80 2.20 -2 -5 -7 3.20 1.20 2 5 7 1.90 2.30 0 -5 -7 5.50 2.50 0 5 -7 3.30 1.20 0 5 -7 2.80 1.40 0 5 7 2.60 2.10 0 5 7 2.10 2.30 -1 5 -7 58.19 3.60 1 -5 7 51.89 3.60 -2 5 -7 2.10 1.00 -2 5 7 2.00 2.50 2 -5 7 1.70 1.10 -3 5 7 33.70 4.70 3 -5 7 26.10 2.40 -4 5 7 3.70 2.90 -5 5 7 43.60 5.50 -6 5 -7 -1.10 2.60 -6 5 7 -0.20 2.70 -8 5 7 -0.50 3.30 -9 5 7 6.70 4.20 8 5 8 1.60 4.60 7 5 8 -0.70 3.90 6 5 8 18.40 5.20 5 5 -8 7.10 2.40 5 5 8 0.40 3.20 4 5 8 26.20 6.00 2 5 -8 35.70 3.70 -2 -5 8 33.10 4.00 1 5 -8 -0.10 1.50 -1 -5 -8 0.20 2.20 1 5 -8 -1.00 1.20 1 5 8 0.40 2.50 0 5 -8 28.90 2.90 0 5 -8 26.80 3.10 0 -5 -8 27.20 4.40 0 5 8 24.20 4.90 -1 5 -8 0.10 1.20 -2 5 -8 48.20 2.90 -2 5 8 38.00 5.30 -3 5 8 0.40 2.60 -4 5 8 9.80 3.80 -5 5 8 10.10 3.80 -6 5 -8 19.90 4.60 -7 5 -8 -0.70 3.00 -7 5 8 2.40 3.50 -8 5 8 0.20 3.60 7 5 9 17.60 5.90 6 5 9 -1.00 3.80 5 5 9 24.90 5.60 4 5 -9 -0.30 1.70 4 5 9 3.30 3.50 2 5 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4.00 1 -5 13 -0.40 4.00 10 6 0 0.50 2.30 9 6 0 -1.30 2.50 9 6 0 1.20 2.20 9 6 0 -0.10 1.80 8 6 0 -0.20 1.50 8 6 0 -0.50 1.70 8 6 0 -0.20 2.20 7 6 0 2.60 2.20 7 6 0 3.80 1.50 7 6 0 2.70 1.80 6 6 0 100.89 6.10 6 6 0 101.49 6.30 6 6 0 108.29 5.70 5 6 0 2.90 1.20 5 6 0 2.00 1.60 5 6 0 2.10 1.40 4 6 0 136.39 6.40 4 6 0 139.39 6.80 4 6 0 142.39 7.00 -4 -6 0 141.59 6.70 3 6 0 57.39 3.20 3 6 0 58.19 3.60 3 6 0 57.09 3.40 -3 -6 0 59.89 3.40 -2 -6 0 242.38 9.80 2 6 0 243.08 10.10 2 6 0 241.08 9.70 -2 -6 0 251.67 10.20 -2 -6 0 241.88 11.00 2 6 0 246.38 10.10 -2 -6 0 244.18 10.20 -1 -6 0 261.17 10.80 1 6 0 255.17 10.40 -1 -6 0 254.97 10.10 -1 -6 0 259.37 10.40 1 6 0 256.97 10.60 0 6 0 977.60 36.30 0 -6 0 987.30 36.40 0 -6 0 974.00 35.90 -1 6 0 265.77 11.10 1 -6 0 255.07 11.00 2 -6 0 244.48 10.60 -2 6 0 242.88 10.60 -3 6 0 58.49 4.10 3 -6 0 58.89 4.00 -4 6 0 133.79 7.10 4 -6 0 135.99 7.00 5 -6 0 2.80 1.70 -5 6 0 1.70 1.80 -6 6 0 95.39 6.20 -7 6 0 2.00 2.30 -8 6 0 0.00 2.20 -9 6 0 0.00 2.50 -10 6 0 0.00 2.50 11 6 -1 37.90 5.90 10 6 -1 1.50 2.70 10 6 1 -0.20 3.20 10 6 1 0.70 2.80 9 6 -1 25.40 4.60 9 6 -1 26.50 4.40 9 6 -1 27.00 4.30 8 6 -1 13.50 3.10 8 6 -1 12.50 2.50 8 6 -1 12.20 2.80 8 6 1 2.20 1.90 7 6 -1 44.80 4.60 7 6 -1 47.50 4.10 7 6 -1 44.80 4.30 6 6 -1 14.00 2.80 6 6 -1 16.50 2.70 6 6 -1 15.10 2.70 6 6 1 11.90 2.80 6 6 1 10.40 1.80 6 6 1 11.80 2.20 -4 -6 -1 5.00 1.30 4 6 1 4.60 1.30 4 6 1 4.20 1.10 4 6 1 5.50 1.80 1 6 -1 20.90 1.90 1 6 -1 19.90 2.20 -1 -6 1 23.10 2.00 -1 -6 1 21.20 1.70 0 6 -1 1.90 1.20 0 6 -1 1.50 0.70 0 -6 1 2.40 1.20 0 -6 1 1.50 0.70 -1 6 -1 49.90 3.50 1 -6 1 49.90 3.40 1 -6 1 48.50 2.80 4 -6 -1 14.80 2.60 -4 6 1 12.10 2.80 -6 6 -1 10.00 2.70 -6 6 1 15.60 3.10 -7 6 1 41.20 4.70 -8 6 1 11.00 3.20 -9 6 1 27.10 4.70 -10 6 1 0.80 3.00 -11 6 1 34.70 5.60 10 6 -2 28.30 5.50 9 6 -2 2.80 2.60 9 6 2 0.50 3.20 9 6 2 2.80 2.00 8 6 -2 72.69 6.30 8 6 -2 78.99 5.80 8 6 -2 69.69 5.00 8 6 2 69.39 7.10 8 6 2 67.29 5.00 8 6 2 69.99 4.60 7 6 -2 10.40 2.20 7 6 -2 9.90 2.30 7 6 -2 10.80 2.70 7 6 2 12.70 2.30 7 6 2 11.90 3.30 7 6 2 10.90 1.80 6 6 2 48.90 5.30 6 6 2 50.09 3.80 6 6 2 52.99 3.40 -2 -6 -2 116.69 5.10 -2 -6 -2 114.59 5.60 -2 -6 -2 120.99 5.60 2 6 2 115.09 5.50 2 6 2 123.09 6.50 1 6 -2 49.50 3.70 -1 -6 -2 64.29 3.20 -1 -6 -2 64.19 3.50 1 6 -2 48.40 3.00 1 6 -2 51.79 3.20 -1 -6 2 49.60 3.00 -1 -6 2 49.00 3.20 0 6 -2 71.79 3.80 0 6 -2 79.39 4.60 0 -6 -2 74.69 4.30 0 -6 2 71.99 3.70 0 6 2 72.99 4.30 0 -6 2 76.89 3.90 -1 6 -2 65.39 4.10 1 -6 -2 48.50 3.60 -1 6 2 48.90 3.70 1 -6 2 65.69 3.30 4 -6 -2 140.09 7.20 -4 6 2 128.59 7.20 -6 6 -2 43.30 4.40 -7 6 -2 10.10 2.90 -7 6 2 14.30 3.40 -8 6 -2 63.79 5.50 -8 6 2 62.99 5.90 -9 6 2 1.20 2.80 -10 6 2 27.00 5.30 -11 6 2 0.00 3.10 10 6 -3 0.50 3.00 10 6 3 1.00 3.80 9 6 -3 -1.80 2.50 9 6 3 -0.80 3.30 8 6 -3 2.30 2.00 8 6 3 3.40 3.30 8 6 3 4.80 1.90 6 6 -3 0.00 1.40 6 6 3 0.60 1.20 6 6 3 0.20 2.20 5 6 3 238.88 10.00 5 6 3 229.38 11.90 -3 -6 -3 111.29 5.40 -3 -6 -3 112.89 5.90 3 6 -3 135.09 6.20 3 6 -3 143.89 6.80 3 6 3 112.19 7.10 -3 -6 3 148.59 6.60 -2 -6 -3 30.80 2.00 -2 -6 -3 31.20 2.40 -2 -6 -3 28.70 2.60 2 6 3 31.90 3.60 2 6 3 32.60 2.60 -1 -6 -3 160.78 6.90 -1 -6 -3 163.78 7.50 1 6 3 157.98 7.40 0 6 -3 56.39 3.40 0 -6 -3 65.09 4.10 0 -6 3 61.69 3.40 0 -6 3 62.09 3.60 0 6 3 67.49 4.20 -1 6 -3 165.38 8.20 -1 6 -3 155.38 6.90 1 -6 3 160.58 6.80 1 -6 3 161.08 7.00 -2 6 -3 30.50 3.30 2 -6 3 31.10 2.20 3 -6 -3 138.89 6.90 -3 6 -3 107.19 6.70 -3 6 3 137.19 7.10 3 -6 3 110.59 5.40 4 -6 -3 11.00 2.60 -4 6 3 8.10 2.40 -5 6 3 94.79 6.50 -6 6 -3 -0.60 2.10 -6 6 3 -0.30 2.20 -8 6 3 0.10 2.70 -9 6 3 0.70 2.80 -10 6 3 0.50 3.10 -11 6 3 0.60 3.80 10 6 4 -1.50 3.90 9 6 4 -0.70 3.50 8 6 4 45.20 7.00 7 6 -4 14.30 2.80 6 6 -4 22.10 3.50 5 6 -4 3.20 1.60 5 6 4 1.70 2.40 -2 -6 -4 67.09 4.40 -2 -6 -4 65.89 3.70 2 6 4 63.09 4.00 2 6 4 68.79 5.30 1 6 -4 0.80 0.90 1 6 -4 1.30 1.10 1 6 4 4.60 1.70 1 6 4 2.80 1.80 -1 -6 4 1.60 0.90 0 6 -4 56.29 3.50 0 -6 -4 56.89 4.20 0 -6 4 56.59 3.40 0 6 4 58.29 4.30 1 -6 -4 0.10 1.40 -1 6 -4 4.40 1.10 1 -6 4 4.30 1.00 -1 6 4 2.20 1.60 -4 6 -4 105.99 6.70 4 -6 4 106.99 4.90 -5 6 -4 2.10 2.30 5 -6 4 2.50 1.00 -5 6 4 3.90 2.40 -6 6 4 20.10 4.40 -8 6 4 33.10 5.30 -9 6 4 2.10 3.10 -10 6 4 7.30 4.00 10 6 5 0.70 4.50 9 6 5 31.60 6.50 8 6 5 0.50 3.50 6 6 -5 -0.50 1.50 6 6 5 4.20 3.10 4 6 -5 42.00 3.70 4 6 5 35.40 5.10 1 6 -5 47.50 3.60 1 6 -5 49.99 3.40 -1 -6 5 53.19 3.70 0 6 -5 2.90 1.20 0 -6 -5 3.40 1.80 0 -6 5 2.70 1.10 0 6 5 2.60 1.80 1 -6 5 80.19 4.30 2 -6 -5 71.29 5.50 -2 6 5 77.69 5.60 -4 6 -5 39.20 4.60 4 -6 5 37.80 2.70 -4 6 5 39.40 4.70 -6 6 -5 4.50 2.80 -6 6 5 -1.60 2.40 -7 6 -5 58.89 5.80 -8 6 5 3.00 3.10 -9 6 5 26.90 5.90 -10 6 5 -0.60 3.40 9 6 6 1.20 4.30 8 6 6 -0.10 3.70 7 6 6 5.70 3.90 6 6 -6 15.00 2.80 6 6 6 2.30 3.20 5 6 -6 2.30 1.70 5 6 6 6.40 3.20 -4 -6 -6 148.79 8.20 4 6 6 182.78 10.70 -3 -6 -6 47.20 3.30 -3 -6 -6 50.59 4.40 3 6 6 48.80 5.70 2 6 -6 87.79 5.00 -2 -6 -6 80.39 5.60 2 6 -6 79.79 5.30 -2 -6 -6 76.19 4.30 2 6 6 75.29 6.50 -2 -6 6 84.29 5.20 -1 -6 -6 10.20 2.50 1 6 6 8.60 2.50 1 6 6 6.70 2.70 0 6 -6 103.89 5.60 0 -6 -6 106.69 6.60 0 6 6 100.99 6.50 0 -6 6 103.69 5.60 -1 6 -6 9.10 1.60 1 -6 6 8.40 1.50 2 -6 -6 98.19 7.80 2 -6 6 78.79 4.40 -5 6 -6 5.40 2.80 -5 6 6 2.70 2.60 -6 6 -6 3.30 2.90 -6 6 6 14.30 3.70 -7 6 -6 5.20 3.20 -7 6 6 0.90 3.00 -8 6 6 6.60 3.70 -9 6 6 -0.10 3.50 8 6 7 2.30 4.30 7 6 7 36.40 7.80 6 6 7 2.00 3.50 4 6 -7 1.20 1.50 4 6 7 7.00 3.30 -2 -6 -7 0.30 1.10 2 6 -7 0.90 1.60 -2 -6 -7 1.40 2.10 2 6 -7 1.70 1.40 2 6 7 1.70 2.50 -1 -6 -7 7.60 2.60 1 6 -7 5.50 1.70 1 6 -7 6.50 1.60 1 6 7 6.20 2.80 -1 -6 7 7.70 1.90 0 -6 -7 11.50 3.00 0 6 -7 8.70 1.90 0 -6 7 7.40 1.70 0 6 7 7.20 2.70 1 -6 -7 7.60 2.80 -1 6 -7 6.40 1.60 1 -6 7 6.90 1.70 -1 6 7 9.00 3.10 2 -6 7 0.90 1.10 -2 6 7 0.90 2.30 -4 6 7 1.00 2.60 -6 6 -7 2.40 3.00 -6 6 7 4.40 3.10 -8 6 7 2.00 3.40 -9 6 7 13.90 5.00 8 6 8 11.50 5.40 7 6 8 0.20 4.00 6 6 8 22.70 5.40 5 6 -8 12.60 2.70 5 6 8 2.20 3.30 4 6 -8 17.10 2.90 3 6 -8 16.00 2.70 -3 -6 8 16.00 3.00 3 6 8 15.00 4.10 2 6 -8 3.90 2.00 2 6 -8 3.70 1.70 2 6 8 -0.40 2.70 1 6 -8 2.00 1.40 -1 -6 -8 2.40 3.30 1 6 -8 2.00 1.70 1 6 8 2.80 2.80 0 -6 -8 27.70 4.70 0 6 -8 27.50 3.20 -1 6 -8 3.50 1.50 -1 6 8 2.30 2.80 -2 6 8 5.50 3.20 -3 6 8 14.00 3.80 -4 6 8 23.00 4.80 -5 6 -8 2.30 3.20 -5 6 8 14.60 4.10 -6 6 -8 22.90 4.90 -7 6 -8 1.00 3.40 -7 6 8 1.80 3.60 -8 6 8 4.90 4.10 7 6 9 1.70 4.30 6 6 9 1.10 4.10 5 6 9 0.80 3.70 4 6 -9 5.70 2.20 4 6 9 1.30 3.50 3 6 -9 21.50 3.70 -3 -6 9 18.60 3.60 2 6 -9 6.80 2.10 2 6 -9 5.50 2.40 -2 -6 9 7.90 2.60 2 6 9 10.00 4.10 1 6 -9 37.80 4.10 1 6 -9 38.20 3.70 1 6 9 27.40 6.00 0 6 -9 8.80 2.20 -1 6 -9 27.00 3.10 -2 6 9 7.50 3.50 -3 6 9 24.60 5.40 -4 6 9 4.80 3.60 -5 6 9 8.60 4.30 -6 6 -9 3.50 3.80 -6 6 9 1.00 3.70 -7 6 9 2.10 3.90 -8 6 9 0.70 5.40 6 6 10 19.20 6.10 5 6 10 4.50 4.30 4 6 10 8.90 4.40 3 6 -10 1.90 2.00 3 6 -10 1.30 2.30 3 6 10 2.70 4.00 1 6 -10 1.40 1.90 1 6 -10 0.90 1.70 -1 -6 10 0.40 2.50 1 6 10 2.80 3.50 0 6 -10 0.60 1.80 5 6 11 8.30 5.40 4 6 -11 4.20 3.00 4 6 11 0.60 4.30 3 6 -11 -0.20 2.50 3 6 11 2.00 4.10 2 6 -11 0.20 2.20 2 6 -11 0.20 1.80 2 6 11 3.30 4.10 1 6 -11 10.50 2.90 -1 -6 11 8.80 3.50 0 -6 11 4.60 3.40 1 -6 11 0.90 3.60 4 6 -12 2.40 4.00 3 6 -12 1.00 2.70 3 6 12 2.30 4.50 2 6 12 18.40 5.70 0 -6 12 2.80 3.60 1 -6 12 1.40 3.70 2 -6 12 12.40 4.90 3 -6 12 0.10 4.50 10 7 0 11.30 3.30 9 7 0 76.59 5.80 9 7 0 73.09 6.80 9 7 0 71.99 6.20 8 7 0 49.00 4.90 8 7 0 53.09 4.60 8 7 0 54.29 5.50 7 7 0 4.20 2.30 7 7 0 5.50 1.70 7 7 0 5.80 2.10 6 7 0 0.40 1.50 6 7 0 -0.40 1.70 6 7 0 0.10 1.20 5 7 0 125.19 6.70 5 7 0 123.39 6.20 -5 -7 0 127.19 6.60 5 7 0 128.39 7.00 4 7 0 184.68 8.10 -4 -7 0 189.28 8.50 4 7 0 186.38 8.60 -3 -7 0 170.08 7.40 3 7 0 162.98 7.40 -3 -7 0 166.38 7.80 3 7 0 162.78 7.20 -3 -7 0 166.08 7.80 3 7 0 163.28 7.60 -2 -7 0 129.49 6.50 2 7 0 129.69 6.20 -2 -7 0 133.49 6.00 2 7 0 132.39 6.40 -2 -7 0 135.49 6.40 -1 -7 0 4.20 1.40 1 7 0 2.60 1.00 -1 -7 0 3.30 0.90 0 -7 0 0.00 0.90 0 -7 0 0.50 0.60 0 7 0 0.80 1.10 1 -7 0 3.00 1.50 -1 7 0 2.50 1.40 1 -7 0 2.00 0.90 2 -7 0 126.49 6.70 -2 7 0 128.09 6.80 3 -7 0 161.58 8.00 -3 7 0 157.98 8.10 4 -7 0 180.88 8.90 -4 7 0 179.88 9.00 -5 7 0 109.19 6.70 -6 7 0 0.50 2.10 -7 7 0 4.10 2.70 -8 7 0 48.30 5.30 -9 7 0 64.89 6.20 -10 7 0 8.60 3.30 -11 7 0 2.50 3.30 11 7 -1 1.40 4.50 10 7 1 33.80 6.10 10 7 1 37.20 8.00 9 7 -1 23.20 5.90 9 7 -1 18.00 3.20 9 7 -1 14.80 3.40 8 7 1 6.90 3.00 8 7 1 6.00 2.30 8 7 1 7.60 2.00 7 7 -1 57.09 5.20 7 7 -1 61.39 4.90 7 7 -1 61.39 5.10 7 7 1 79.79 4.80 7 7 1 80.69 6.20 7 7 1 81.99 5.30 6 7 1 61.69 4.10 6 7 1 63.99 5.50 6 7 1 63.89 4.50 4 7 -1 81.59 5.00 4 7 -1 80.09 4.60 4 7 -1 81.99 4.70 -4 -7 1 84.19 4.90 1 7 -1 421.16 17.50 1 7 -1 446.66 17.20 -1 -7 1 430.26 16.90 -1 -7 1 457.15 17.90 -1 -7 1 456.05 17.30 0 7 -1 257.27 10.60 0 -7 -1 263.47 10.60 0 -7 -1 264.57 11.20 0 7 -1 255.37 11.20 0 -7 1 267.97 11.40 0 -7 1 259.77 10.70 0 7 1 261.37 11.20 -4 7 -1 28.00 3.70 4 -7 1 24.60 3.20 -7 7 -1 71.29 5.70 -7 7 1 53.09 5.50 -8 7 -1 7.20 3.00 -8 7 1 13.90 3.60 -9 7 1 17.50 4.00 -11 7 1 1.30 3.10 10 7 -2 1.50 2.90 10 7 2 1.00 3.50 9 7 -2 1.10 2.50 9 7 2 6.20 2.40 9 7 2 5.00 3.40 8 7 2 25.40 3.50 8 7 2 22.70 4.50 8 7 2 26.80 3.20 7 7 2 55.19 5.90 7 7 2 55.79 3.80 7 7 2 53.59 4.30 -3 -7 -2 152.38 6.80 -3 -7 -2 157.18 7.30 3 7 2 156.68 7.10 3 7 2 154.78 8.20 -2 -7 -2 146.19 6.90 -2 -7 -2 148.19 6.70 -2 -7 -2 140.89 6.20 2 7 2 143.59 6.70 0 7 -2 439.86 17.90 0 -7 -2 449.56 17.60 0 7 -2 425.66 17.00 0 7 2 443.96 17.70 0 -7 2 445.56 17.20 0 -7 2 436.96 16.80 2 -7 -2 51.29 3.90 -2 7 2 51.29 4.20 -7 7 2 29.50 4.60 -8 7 -2 23.70 4.50 -9 7 -2 5.90 3.10 -9 7 2 1.80 2.90 -10 7 2 5.10 3.40 -11 7 2 21.30 5.70 9 7 -3 21.20 4.20 9 7 3 18.70 4.90 4 7 -3 59.79 4.50 4 7 -3 60.79 4.20 -4 -7 -3 64.19 3.70 -4 -7 -3 61.59 4.20 4 7 3 66.29 5.50 4 7 3 64.69 4.00 -4 -7 3 63.09 4.50 -3 -7 -3 181.48 8.20 -3 -7 -3 175.28 7.50 3 7 3 177.28 9.40 -2 -7 -3 25.40 2.00 -2 -7 -3 25.00 2.30 -2 -7 -3 23.90 2.70 2 7 3 22.70 3.40 2 7 3 22.70 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167.18 8.50 0 8 -4 32.10 3.00 0 -8 -4 33.60 3.70 0 -8 4 33.50 2.90 0 8 4 34.60 3.80 -1 8 -4 176.48 8.00 -1 8 -4 183.68 9.70 1 -8 4 172.68 7.80 -2 8 -4 -0.50 1.70 2 -8 -4 6.90 2.30 -2 8 4 7.30 2.40 -3 8 -4 271.77 13.10 3 -8 4 272.67 11.30 -4 8 -4 -1.70 2.10 4 -8 4 -0.30 1.00 -4 8 4 6.90 2.70 -5 8 -4 32.90 4.70 5 -8 4 32.20 2.80 -6 8 -4 7.70 3.00 -6 8 4 2.00 2.60 -8 8 -4 -2.20 2.60 -8 8 4 2.80 3.30 -9 8 4 5.20 3.70 -10 8 4 0.40 3.60 9 8 5 2.00 4.10 7 8 -5 -2.40 2.10 7 8 5 0.70 3.20 6 8 -5 43.40 4.50 6 8 -5 42.90 5.10 5 8 -5 11.80 2.70 5 8 -5 12.30 2.30 -4 -8 -5 44.00 3.00 -4 -8 -5 45.30 3.80 4 8 5 40.90 5.80 -3 -8 -5 17.30 2.50 -3 -8 -5 14.50 3.20 -3 -8 -5 16.10 2.00 3 8 5 15.60 3.60 1 8 -5 94.29 5.20 1 8 -5 83.99 5.30 -1 -8 5 92.69 5.30 0 8 -5 40.20 3.40 0 -8 -5 38.60 4.40 0 -8 5 42.30 3.40 0 8 5 37.80 4.40 -3 8 -5 16.60 3.70 3 -8 5 15.50 2.30 3 -8 5 15.90 2.20 -4 8 -5 42.00 5.30 4 -8 5 40.90 3.00 4 -8 5 42.20 3.30 -5 8 -5 4.00 2.90 -5 8 5 14.70 3.70 -7 8 -5 0.30 3.00 -7 8 5 -0.20 3.00 -9 8 5 4.60 3.80 9 8 6 2.10 4.40 8 8 -6 -0.60 2.60 8 8 6 6.20 4.40 6 8 -6 1.20 2.20 6 8 -6 -0.10 2.20 6 8 6 3.80 3.60 5 8 -6 8.50 2.20 5 8 -6 9.50 2.80 5 8 6 11.60 3.90 3 8 -6 114.29 6.30 -3 -8 -6 101.99 5.90 3 8 -6 104.19 6.70 -3 -8 -6 103.99 6.90 -3 -8 -6 107.89 5.10 3 8 6 112.19 8.70 -3 -8 6 110.59 6.80 -2 -8 -6 1.60 1.20 2 8 -6 0.20 1.20 2 8 -6 0.70 1.50 -2 -8 -6 2.20 2.30 2 8 6 2.00 2.10 -2 -8 6 0.40 1.50 2 8 6 0.60 2.50 1 8 -6 147.29 7.70 1 8 -6 151.58 7.40 -1 -8 6 153.08 7.70 0 8 -6 10.00 2.00 0 -8 -6 13.40 3.10 0 -8 6 11.20 2.00 0 8 6 10.10 2.80 2 -8 6 1.90 1.20 -2 8 6 1.70 2.30 -3 8 -6 109.49 8.20 -3 8 6 112.69 7.90 3 -8 6 110.79 5.70 -4 8 -6 37.00 5.30 4 -8 6 37.40 3.10 -5 8 -6 12.20 3.70 -5 8 6 12.70 3.70 -6 8 -6 4.50 3.20 -6 8 6 1.40 3.10 -8 8 -6 7.00 3.80 -8 8 6 1.30 3.50 -9 8 6 -1.00 3.60 8 8 7 14.70 5.40 7 8 -7 -0.20 2.60 7 8 7 -0.10 3.60 5 8 -7 1.00 1.80 5 8 -7 0.60 2.20 5 8 7 1.50 3.20 3 8 -7 -0.20 1.70 3 8 -7 1.60 1.60 3 8 7 -0.60 2.70 -3 -8 7 1.70 1.80 -1 -8 -7 0.70 2.20 1 8 -7 4.20 1.80 1 8 -7 4.00 1.60 -1 -8 7 4.10 1.90 0 -8 -7 24.30 4.40 0 8 -7 23.30 3.00 0 8 7 20.20 4.10 0 -8 7 21.90 3.20 -1 8 -7 -0.40 1.20 -1 8 7 1.90 2.50 1 -8 7 0.10 1.30 -3 8 7 1.10 2.70 3 -8 7 0.00 1.20 -5 8 -7 0.90 3.00 -5 8 7 1.80 3.20 -7 8 -7 0.00 3.30 -7 8 7 -0.20 3.40 -8 8 -7 16.70 5.10 -8 8 7 9.10 4.40 7 8 -8 7.60 4.30 7 8 8 16.30 5.70 6 8 -8 1.30 2.60 6 8 8 2.10 3.80 5 8 -8 17.90 3.70 4 8 -8 0.00 2.10 4 8 -8 0.30 1.70 4 8 8 2.20 3.60 3 8 -8 39.10 4.60 3 8 -8 45.10 4.40 -3 -8 8 37.50 3.70 2 8 -8 11.80 2.30 2 8 -8 9.60 2.50 2 8 8 10.60 3.90 1 8 -8 4.20 2.10 1 8 -8 5.30 1.90 -1 -8 8 5.50 2.00 0 8 -8 7.50 2.10 0 -8 8 6.80 2.00 0 8 8 8.10 3.30 -1 8 -8 6.80 1.90 -1 8 8 6.00 3.30 1 -8 8 6.60 2.00 -2 8 8 12.40 3.80 2 -8 8 12.50 3.00 -4 8 -8 3.80 3.60 -4 8 8 1.30 2.90 -6 8 -8 0.50 3.50 -6 8 8 0.70 3.40 -7 8 -8 10.90 7.30 -7 8 8 14.30 5.00 -8 8 8 0.00 3.70 6 8 -9 -0.20 2.70 6 8 9 2.00 4.30 5 8 -9 0.90 2.60 5 8 9 -0.70 4.00 4 8 -9 17.80 3.70 4 8 9 1.70 3.70 3 8 -9 2.70 1.90 2 8 -9 44.10 4.30 2 8 -9 40.60 4.70 2 8 9 30.60 6.80 1 8 -9 4.90 2.20 0 8 -9 13.30 2.60 -1 8 -9 6.40 2.00 -1 8 9 4.10 3.50 -2 8 9 44.00 6.40 -3 8 9 2.30 3.60 -4 8 -9 3.60 4.00 -4 8 9 19.90 4.80 -5 8 -9 0.70 3.50 -5 8 9 -0.20 3.60 -6 8 9 -0.40 3.60 -7 8 9 0.30 4.00 5 8 10 28.20 6.90 4 8 -10 -0.10 2.40 4 8 10 1.00 4.10 3 8 -10 1.00 2.40 3 8 10 9.60 4.50 2 8 -10 1.20 1.90 2 8 -10 -0.50 2.10 -2 -8 10 -0.10 2.40 1 8 -10 1.80 2.10 0 8 -10 0.70 1.90 -3 8 10 -0.20 3.40 -4 8 10 -1.30 3.50 -5 8 10 -1.10 3.70 -6 8 10 2.00 4.20 4 8 -11 5.20 3.10 4 8 11 -1.00 4.10 3 8 -11 1.40 2.60 3 8 11 2.00 4.10 2 8 -11 2.30 2.70 -1 -8 11 -0.90 2.80 3 8 -12 6.50 3.40 0 -8 12 4.80 4.50 1 -8 12 5.60 4.70 10 9 0 18.70 4.00 9 9 0 47.10 5.40 9 9 0 50.59 5.20 8 9 0 8.30 2.70 8 9 0 7.50 2.20 7 9 0 33.20 3.60 7 9 0 33.10 4.00 -6 -9 0 78.39 5.50 6 9 0 78.79 5.00 6 9 0 79.29 5.60 -5 -9 0 313.47 13.70 5 9 0 307.97 13.70 5 9 0 317.07 13.10 -4 -9 0 6.20 1.60 4 9 0 4.50 1.40 4 9 0 5.50 1.80 4 9 0 7.60 2.00 3 9 0 117.99 6.30 3 9 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3 4.20 4.40 9 10 -3 1.40 2.80 9 10 3 2.40 3.70 8 10 -3 10.80 3.40 8 10 3 0.80 3.40 8 10 3 0.70 1.90 7 10 -3 1.40 2.20 7 10 -3 0.30 1.80 7 10 3 3.50 2.00 7 10 3 1.40 3.10 -6 -10 -3 5.60 1.90 6 10 -3 6.30 2.10 6 10 -3 9.50 3.00 6 10 -3 7.80 2.70 -6 -10 3 8.70 2.50 6 10 3 2.50 3.00 6 10 3 3.70 1.90 5 10 -3 51.29 4.90 5 10 -3 49.00 5.10 5 10 -3 49.20 4.30 -5 -10 3 46.40 4.70 4 10 -3 -0.60 1.50 4 10 -3 0.50 1.30 4 10 -3 1.50 2.10 -4 -10 -3 3.70 2.20 -4 -10 -3 2.20 1.40 -4 -10 -3 3.50 1.80 -4 -10 3 0.40 1.40 -3 -10 -3 125.69 6.80 3 10 -3 125.19 7.70 3 10 -3 121.59 7.00 -3 -10 -3 128.59 7.10 3 10 -3 125.99 6.60 -3 -10 -3 131.79 6.30 3 10 3 119.99 6.70 -3 -10 3 123.29 6.90 1 10 -3 459.35 19.60 1 10 -3 453.25 18.60 -1 -10 3 462.95 18.90 -1 -10 3 458.75 18.30 0 -10 -3 96.19 6.20 0 -10 -3 100.79 5.40 0 10 -3 90.89 5.50 0 10 -3 99.49 6.70 0 -10 3 97.49 5.60 0 -10 3 93.99 5.20 0 10 3 95.79 6.40 -3 10 -3 123.79 8.00 -3 10 3 121.79 8.00 3 -10 3 126.99 6.50 -4 10 -3 1.80 2.70 -4 10 3 0.70 2.50 4 -10 3 4.00 1.60 -6 10 -3 3.30 3.10 -6 10 3 8.50 3.40 -7 10 -3 2.80 3.00 -7 10 3 0.40 3.00 -8 10 3 12.30 4.20 -9 10 -3 1.00 3.30 -9 10 3 -1.30 3.30 9 10 4 17.60 5.30 8 10 4 27.30 5.70 6 10 -4 7.00 2.70 6 10 -4 6.70 2.10 6 10 -4 11.50 3.50 5 10 -4 3.00 2.10 -5 -10 -4 -0.50 1.30 5 10 -4 2.00 2.60 5 10 -4 2.20 1.60 5 10 4 0.20 2.60 -5 -10 4 3.20 2.10 -3 -10 -4 14.50 2.30 -3 -10 -4 14.60 2.70 2 10 -4 49.40 5.30 2 10 -4 46.30 4.20 2 10 -4 48.60 3.80 -2 -10 4 45.30 3.90 -1 -10 -4 11.70 2.10 1 10 -4 2.30 2.30 1 10 4 11.60 2.80 0 10 -4 149.99 8.90 0 10 -4 142.99 7.40 0 -10 -4 145.79 8.20 0 10 4 144.69 8.30 0 -10 4 143.59 7.20 0 -10 4 144.99 7.60 -1 10 -4 10.00 2.80 -1 10 -4 9.20 2.00 1 -10 4 11.70 2.10 1 -10 4 8.30 1.70 -2 10 -4 104.79 7.50 2 -10 4 109.89 5.80 2 -10 4 106.79 6.00 -3 10 -4 15.90 3.90 3 -10 4 17.50 2.60 -4 10 -4 117.59 8.30 4 -10 4 117.69 6.30 -5 10 -4 0.30 2.50 -5 10 4 4.30 3.00 -8 10 -4 23.40 5.50 -9 10 -4 18.20 4.70 -9 10 4 8.00 4.30 9 10 5 24.80 6.30 8 10 -5 6.00 3.10 8 10 5 0.30 3.80 7 10 -5 49.99 5.90 6 10 -5 21.80 4.90 6 10 -5 15.60 3.40 5 10 -5 28.90 4.30 5 10 -5 28.20 3.90 5 10 -5 29.20 5.40 -4 -10 -5 1.90 1.20 4 10 -5 0.20 1.80 4 10 -5 1.10 1.50 -4 -10 -5 2.30 1.70 4 10 5 1.30 2.70 -4 -10 5 -0.70 1.50 -2 -10 5 18.90 3.10 0 10 -5 29.20 3.30 0 10 -5 29.30 4.90 0 -10 -5 28.40 4.20 0 10 5 29.00 4.20 0 -10 5 27.20 3.20 -1 10 -5 11.10 2.10 -1 10 -5 13.80 3.80 1 -10 5 10.90 1.90 -2 10 -5 0.90 2.40 2 -10 5 2.50 1.30 -4 10 -5 1.80 2.70 4 -10 5 -0.20 1.30 -4 10 5 0.90 2.80 -5 10 -5 13.70 3.90 -6 10 5 14.30 4.00 -7 10 -5 14.90 4.30 -8 10 -5 -1.60 3.20 -8 10 5 7.70 4.20 -9 10 5 12.50 5.00 8 10 6 2.10 4.20 7 10 -6 5.00 3.00 7 10 6 -0.50 3.70 6 10 -6 8.50 3.00 6 10 6 4.40 3.90 5 10 -6 -0.30 1.70 5 10 -6 0.10 2.00 5 10 6 0.90 3.30 4 10 -6 12.70 2.40 4 10 -6 14.40 3.00 -4 -10 6 18.50 3.30 3 10 -6 13.70 2.90 3 10 -6 14.80 2.50 -3 -10 6 16.80 3.00 -2 -10 -6 137.59 8.20 2 10 -6 110.39 6.60 2 10 -6 105.59 6.90 -2 -10 -6 126.89 6.70 -2 -10 6 106.49 7.00 2 10 6 126.29 7.60 0 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4.00 5 10 -8 -0.50 2.30 5 10 8 0.60 3.80 3 10 -8 7.90 2.70 3 10 -8 9.10 2.40 2 10 -8 15.40 2.80 2 10 -8 11.30 2.90 -2 -10 8 14.70 3.10 1 10 -8 18.80 3.60 -1 -10 8 18.50 3.20 0 10 -8 1.20 1.80 0 10 8 -0.10 2.70 0 -10 8 0.90 1.90 -1 10 -8 1.90 1.80 -1 10 8 13.80 3.90 1 -10 8 2.60 1.80 -2 10 -8 4.70 4.00 -2 10 8 10.20 3.80 -3 10 -8 1.70 3.40 -3 10 8 7.60 3.70 -5 10 -8 0.10 3.40 -5 10 8 1.00 3.60 -6 10 8 7.50 4.20 -7 10 8 3.60 4.50 6 10 9 1.20 4.30 5 10 -9 3.70 2.90 5 10 9 2.00 4.20 4 10 -9 3.60 2.70 3 10 -9 27.10 4.60 2 10 -9 10.10 3.00 2 10 -9 9.50 2.50 1 10 -9 26.50 4.10 -1 -10 9 21.70 3.50 0 10 -9 2.40 2.10 0 10 9 1.50 3.30 -1 10 9 21.30 5.10 -2 10 9 8.30 4.00 -3 10 9 25.10 5.80 -4 10 -9 -1.90 3.40 -4 10 9 3.20 3.90 -5 10 9 0.70 3.80 -6 10 9 2.60 4.30 -7 10 9 2.20 4.50 5 10 10 4.80 4.60 4 10 -10 1.10 2.80 3 10 -10 1.50 2.60 2 10 -10 1.10 2.50 1 10 -10 0.80 2.10 -1 10 10 1.00 3.70 -2 10 10 -0.90 3.70 -3 10 10 0.60 3.80 -4 10 10 -0.70 3.80 -5 10 10 -0.80 3.80 -6 10 10 -1.00 4.10 3 10 -11 3.50 3.10 2 10 -11 3.70 2.80 -3 10 11 3.80 4.40 -4 10 11 2.80 4.40 -5 10 11 3.20 5.10 10 11 0 20.00 5.20 9 11 0 -0.10 2.30 8 11 0 33.00 4.70 8 11 0 30.90 4.10 7 11 0 20.50 3.60 7 11 0 19.30 3.40 6 11 0 15.40 2.50 -6 -11 0 19.40 3.30 6 11 0 18.50 3.20 -5 -11 0 2.20 1.80 5 11 0 2.20 2.00 4 11 0 191.08 9.30 -4 -11 0 183.58 9.00 4 11 0 175.78 9.00 3 11 0 2.30 1.90 -3 -11 0 1.70 2.00 -3 -11 0 2.10 1.30 -3 -11 0 1.80 1.50 3 11 0 1.80 1.50 2 11 0 0.30 1.20 -2 -11 0 0.80 1.00 2 11 0 2.60 1.90 -2 -11 0 0.50 1.10 -2 -11 0 0.50 1.60 -1 -11 0 1.10 1.80 -1 -11 0 1.30 1.20 1 11 0 2.30 2.00 -1 -11 0 1.70 1.00 0 -11 0 1.80 1.70 -1 11 0 2.00 2.20 1 -11 0 1.00 1.90 1 -11 0 2.00 1.20 -2 11 0 0.90 1.90 2 -11 0 -0.50 1.00 -3 11 0 0.50 2.10 -4 11 0 175.98 10.00 -5 11 0 -0.10 2.70 -6 11 0 13.50 3.70 -7 11 0 19.10 4.50 -8 11 0 30.20 5.90 -9 11 0 -1.40 3.30 9 11 -1 5.20 3.10 9 11 1 12.10 3.30 8 11 -1 2.70 2.50 8 11 1 8.70 2.80 7 11 -1 14.20 2.70 7 11 -1 16.60 3.40 5 11 -1 117.29 6.50 5 11 -1 111.89 6.80 5 11 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17.70 2.70 -1 -11 2 17.20 2.40 0 11 -2 105.89 6.10 0 -11 -2 111.29 5.90 0 -11 -2 110.59 6.90 0 11 -2 113.49 7.20 0 11 2 108.79 7.00 0 -11 2 104.09 5.70 0 -11 2 104.99 6.20 1 -11 -2 15.30 3.50 -1 11 -2 11.70 3.10 1 -11 2 8.70 1.90 -1 11 2 16.80 3.40 -2 11 -2 193.48 10.40 2 -11 2 194.68 9.10 -3 11 -2 7.20 3.00 3 -11 2 10.50 2.00 -4 11 -2 155.58 9.70 4 -11 2 162.08 8.00 -7 11 -2 3.70 3.20 -7 11 2 6.50 3.60 -8 11 -2 10.30 4.00 -8 11 2 2.30 3.40 -9 11 -2 3.20 3.70 -9 11 2 3.00 3.70 8 11 -3 7.00 3.10 8 11 3 -0.10 2.00 7 11 -3 29.00 4.80 7 11 3 45.40 4.40 5 11 -3 86.39 6.60 5 11 -3 88.09 6.50 5 11 -3 86.29 5.70 -5 -11 3 85.49 6.50 4 11 -3 7.90 2.40 4 11 -3 7.70 2.90 -4 -11 -3 3.90 1.60 -4 -11 -3 4.40 2.40 -4 -11 -3 4.90 2.10 4 11 -3 6.70 1.90 -4 -11 3 7.00 2.00 2 11 -3 12.60 3.00 -2 -11 -3 9.40 2.00 2 11 -3 11.80 2.30 -2 -11 -3 9.60 2.70 -2 -11 -3 8.90 1.70 -2 -11 3 13.70 2.30 2 11 3 7.50 2.40 -1 -11 -3 5.70 2.30 1 11 -3 0.20 1.40 1 11 -3 2.10 2.10 -1 -11 -3 5.30 1.60 1 11 3 5.70 2.40 -1 -11 3 1.80 1.30 -1 -11 3 3.00 1.60 0 11 -3 11.20 3.20 0 -11 -3 12.20 3.10 0 -11 -3 11.00 2.10 0 11 -3 9.30 2.10 0 -11 3 9.10 1.80 0 -11 3 9.60 2.10 0 11 3 10.40 3.00 -1 11 -3 5.60 2.60 1 -11 -3 1.50 2.00 -1 11 3 1.40 2.40 1 -11 3 4.90 1.50 1 -11 3 4.70 1.80 -2 11 -3 5.70 2.70 2 -11 3 6.40 1.80 -3 11 -3 127.59 8.50 3 -11 3 132.79 7.00 -4 11 -3 3.40 2.90 4 -11 3 3.80 1.70 -4 11 3 8.00 3.20 -6 11 -3 20.30 4.50 -7 11 3 25.30 5.20 -8 11 -3 -0.50 3.20 -8 11 3 7.40 3.90 -9 11 -3 33.70 6.20 -9 11 3 20.30 5.20 9 11 4 4.40 4.10 8 11 -4 -0.50 2.50 8 11 4 6.80 4.10 7 11 -4 -0.60 2.20 7 11 4 2.40 3.50 6 11 -4 58.79 5.50 6 11 -4 56.19 5.70 6 11 -4 51.29 6.00 5 11 -4 3.20 1.70 5 11 -4 4.70 2.90 5 11 -4 3.80 2.30 -5 -11 4 4.10 2.60 4 11 -4 44.20 5.40 4 11 -4 44.50 4.60 4 11 -4 45.80 4.10 -4 -11 4 44.80 4.60 -1 -11 -4 5.70 1.60 1 11 -4 2.30 1.70 -1 -11 -4 7.50 2.60 1 11 -4 1.80 2.30 1 11 4 6.60 2.60 0 -11 -4 89.69 5.20 0 11 -4 80.49 5.30 0 -11 -4 86.69 6.30 0 11 -4 83.89 6.80 0 -11 4 85.79 5.60 0 11 4 83.99 6.40 0 -11 4 82.19 5.20 -1 11 -4 5.70 2.70 1 -11 -4 2.70 2.40 1 -11 4 4.40 1.70 1 -11 4 5.40 1.60 -1 11 4 1.40 2.40 -3 11 -4 18.70 4.20 3 -11 4 17.80 2.90 -5 11 -4 19.40 4.40 -7 11 -4 2.10 3.30 -7 11 4 -0.10 3.40 -8 11 -4 4.10 3.60 -8 11 4 1.00 3.40 -9 11 4 -0.30 3.60 9 11 5 14.80 5.50 8 11 5 0.20 3.80 7 11 -5 2.50 2.80 7 11 5 11.50 4.60 6 11 -5 0.70 3.10 6 11 -5 2.20 2.40 6 11 5 1.30 3.30 5 11 -5 5.30 2.00 5 11 -5 9.10 3.70 5 11 -5 7.00 2.60 4 11 -5 0.20 1.50 -4 -11 -5 2.40 1.40 4 11 -5 2.00 2.00 4 11 -5 -0.90 2.70 -4 -11 -5 1.70 1.90 -4 -11 5 1.30 1.80 -2 -11 -5 11.10 2.30 -2 -11 -5 10.30 2.90 2 11 -5 10.90 2.50 2 11 -5 9.20 3.30 2 11 5 10.10 2.90 -2 -11 5 8.70 2.20 1 11 -5 85.99 7.60 -1 -11 -5 117.79 6.30 1 11 -5 83.79 6.00 1 11 5 122.49 7.40 0 -11 -5 0.50 2.10 0 11 -5 -0.50 1.40 0 11 -5 1.60 2.40 0 11 5 0.50 2.20 0 -11 5 0.30 1.30 -1 11 -5 120.39 8.60 -1 11 -5 125.69 6.90 1 -11 5 126.99 6.70 1 -11 5 119.19 6.90 -2 11 -5 9.40 3.50 2 -11 5 10.20 2.00 2 -11 5 10.80 2.40 -2 11 5 10.70 3.50 -3 11 -5 97.09 8.00 3 -11 5 100.09 6.00 3 -11 5 96.49 5.70 -4 11 -5 0.00 2.70 -4 11 5 -0.60 2.70 4 -11 5 0.80 1.50 -6 11 -5 -0.80 2.90 -6 11 5 3.20 3.40 -7 11 -5 9.10 4.10 -7 11 5 2.20 3.50 -8 11 -5 -0.10 3.40 -8 11 5 2.30 3.90 8 11 6 36.70 8.30 7 11 -6 3.60 3.00 7 11 6 3.50 4.10 6 11 -6 16.00 5.00 6 11 -6 12.80 3.40 5 11 -6 5.00 4.00 5 11 -6 3.30 2.40 4 11 -6 6.30 2.50 4 11 -6 7.20 2.10 3 11 -6 6.20 2.40 3 11 -6 5.30 2.00 -3 -11 6 6.40 2.30 -1 -11 -6 11.60 3.40 1 11 -6 -0.30 3.10 1 11 -6 0.20 1.70 1 11 6 11.00 3.10 -1 -11 6 0.30 1.50 0 11 -6 6.20 2.00 0 -11 -6 5.50 3.60 0 11 -6 7.30 3.40 0 11 6 5.70 2.90 0 -11 6 4.80 1.80 -1 11 -6 7.70 3.40 -1 11 -6 8.10 2.20 1 -11 6 7.80 1.90 -2 11 -6 51.39 6.40 2 -11 6 52.49 4.30 -3 11 -6 1.20 2.90 3 -11 6 0.20 1.40 -3 11 6 6.40 3.30 -4 11 -6 4.00 3.40 -4 11 6 7.60 3.60 4 -11 6 4.40 2.10 -5 11 -6 16.90 4.60 -6 11 6 14.90 4.90 -7 11 -6 3.80 3.90 -7 11 6 3.10 3.70 -8 11 6 9.80 4.60 7 11 7 4.60 4.50 6 11 -7 -1.20 2.30 6 11 7 -0.80 3.60 5 11 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11 -9 -0.20 2.20 1 11 -9 1.90 2.30 0 11 -9 0.40 2.00 -1 11 -9 16.80 3.30 -1 11 9 2.40 3.50 -2 11 -9 0.90 3.70 -2 11 9 0.10 3.20 -3 11 -9 1.10 3.80 -3 11 9 3.10 3.90 -4 11 9 -0.30 3.70 -5 11 9 5.10 4.20 -6 11 9 3.10 4.50 4 11 -10 7.00 3.30 3 11 -10 -0.10 2.50 2 11 -10 12.50 3.40 1 11 -10 1.40 2.40 -2 11 10 10.30 4.70 -3 11 10 0.10 3.80 -4 11 10 7.20 5.00 -5 11 10 -2.00 4.00 -6 11 10 2.90 5.10 3 11 -11 5.20 3.30 2 11 -11 0.10 2.60 -3 11 11 5.10 4.80 -4 11 11 0.00 4.40 -5 11 11 0.20 5.00 9 12 0 1.30 2.60 8 12 0 -1.00 2.20 7 12 0 16.40 3.30 6 12 0 13.60 3.00 -6 -12 0 13.00 3.10 5 12 0 51.79 4.60 5 12 0 57.69 5.00 -5 -12 0 58.89 4.90 -4 -12 0 23.00 3.40 4 12 0 26.20 3.80 4 12 0 26.70 3.60 3 12 0 153.78 8.10 3 12 0 156.88 8.50 -3 -12 0 154.38 7.90 -3 -12 0 152.28 8.90 -2 -12 0 15.50 3.30 -2 -12 0 12.10 2.00 2 12 0 13.00 2.90 2 12 0 11.40 2.30 -2 -12 0 13.40 2.50 -1 -12 0 86.89 5.10 -1 -12 0 92.29 6.50 -1 -12 0 90.09 5.50 1 12 0 88.39 6.20 0 -12 0 56.89 5.10 0 12 0 50.69 4.90 0 -12 0 54.99 4.10 1 -12 0 89.79 5.40 -1 12 0 87.69 6.40 -2 12 0 14.10 3.40 2 -12 0 12.40 2.40 -3 12 0 153.18 9.30 3 -12 0 155.78 7.90 -4 12 0 26.50 4.90 -5 12 0 47.60 5.90 -6 12 0 11.40 3.80 -7 12 0 14.20 4.30 -8 12 0 -0.50 3.40 -9 12 0 0.00 3.50 9 12 -1 19.60 4.30 8 12 -1 5.60 2.80 8 12 1 11.30 3.10 -7 -12 -1 23.00 3.70 6 12 -1 53.89 4.60 6 12 -1 51.59 5.10 -6 -12 -1 38.20 4.80 6 12 1 42.10 4.50 -6 -12 1 48.60 5.00 5 12 -1 18.80 3.80 5 12 -1 15.90 3.00 -5 -12 -1 12.70 2.60 -5 -12 1 17.60 3.20 5 12 1 11.30 2.50 2 12 -1 4.00 1.80 2 12 -1 6.50 2.40 -2 -12 1 7.50 2.50 -2 -12 1 4.00 1.40 1 12 -1 11.60 2.80 1 12 -1 8.40 2.10 -1 -12 1 12.70 2.40 -1 -12 1 12.10 3.10 -1 -12 1 9.60 1.80 0 -12 -1 -0.70 1.70 0 12 -1 0.20 1.90 0 -12 -1 0.20 1.10 0 -12 1 -0.10 0.90 0 -12 1 -0.30 1.80 0 -12 1 0.40 1.20 0 12 1 0.60 2.10 1 -12 -1 13.40 3.50 1 -12 -1 11.30 2.20 -1 12 1 9.20 2.70 -3 12 -1 117.79 8.20 3 -12 1 117.19 6.50 -4 12 -1 155.08 9.80 4 -12 1 169.18 8.60 -5 12 -1 10.00 3.40 -5 12 1 15.70 4.10 -6 12 -1 39.50 5.90 -6 12 1 42.70 6.10 -7 12 -1 19.40 4.50 -8 12 -1 12.90 4.50 -8 12 1 4.90 3.80 -9 12 -1 1.10 3.80 -9 12 1 14.90 4.80 9 12 2 7.40 4.00 8 12 -2 15.10 3.70 8 12 2 20.50 3.60 7 12 2 16.90 3.30 -6 -12 -2 4.00 2.30 6 12 -2 15.80 3.30 6 12 -2 16.20 2.80 5 12 -2 76.09 5.90 5 12 -2 72.39 5.90 5 12 -2 72.99 5.40 -5 -12 2 67.19 5.80 3 12 -2 9.10 2.40 3 12 -2 9.40 2.80 -3 -12 2 8.30 2.00 1 12 -2 2.00 2.30 -1 -12 -2 11.00 2.90 -1 -12 2 2.10 1.50 1 12 2 9.30 2.80 0 12 -2 28.80 4.30 0 -12 -2 28.80 3.00 0 -12 -2 26.20 4.00 0 12 2 26.80 4.20 0 -12 2 29.00 3.30 0 -12 2 27.20 2.90 1 -12 -2 2.50 2.30 1 -12 -2 1.80 1.30 -1 12 2 0.90 2.20 -3 12 -2 -0.40 2.40 -3 12 2 8.00 3.10 3 -12 2 0.10 1.40 -5 12 -2 23.00 4.50 5 -12 2 21.40 3.70 -6 12 -2 2.20 3.00 -6 12 2 14.90 4.20 -7 12 -2 17.40 4.60 -8 12 -2 16.00 4.60 -8 12 2 12.10 4.40 -9 12 -2 7.20 4.50 -9 12 2 6.20 4.30 8 12 -3 5.70 3.10 8 12 3 3.60 2.40 7 12 -3 2.60 2.50 -6 -12 -3 45.60 6.60 6 12 -3 49.50 5.40 6 12 -3 46.30 4.90 5 12 -3 12.20 2.50 5 12 -3 13.50 3.20 5 12 -3 17.00 3.70 -5 -12 3 15.00 3.20 4 12 -3 133.19 8.00 4 12 -3 142.49 7.60 4 12 -3 138.39 8.60 -4 -12 3 132.29 7.90 -2 -12 -3 70.49 5.60 -2 -12 -3 64.39 4.30 -2 -12 -3 64.69 5.50 2 12 3 66.69 5.50 1 12 -3 51.49 5.20 1 12 -3 46.50 4.10 -1 -12 -3 36.80 3.90 -1 -12 -3 35.80 4.50 -1 -12 3 48.80 3.90 -1 -12 3 51.99 4.50 1 12 3 32.60 4.50 0 12 -3 41.40 3.90 0 -12 -3 46.00 4.60 0 12 -3 46.20 5.20 0 -12 -3 44.40 4.90 0 -12 3 41.90 3.70 0 -12 3 45.10 4.10 0 12 3 43.00 5.00 -1 12 -3 34.10 4.80 1 -12 3 32.90 3.60 1 -12 3 34.70 3.40 -2 12 -3 69.59 6.40 2 -12 3 68.39 4.90 -3 12 -3 32.30 5.10 3 -12 3 32.10 3.60 -4 12 -3 51.59 6.00 4 -12 3 49.99 4.30 -5 12 -3 30.00 5.60 5 -12 3 31.10 4.20 -6 12 -3 39.90 6.10 -6 12 3 47.00 6.60 -7 12 -3 2.10 3.30 -7 12 3 2.90 3.50 -8 12 -3 2.40 3.60 -8 12 3 7.00 4.00 -9 12 3 0.40 4.00 8 12 -4 0.90 4.20 7 12 -4 52.69 5.90 6 12 -4 13.70 3.40 5 12 -4 -0.30 2.50 4 12 -4 17.20 4.10 -4 -12 -4 11.70 2.30 4 12 -4 13.40 2.50 4 12 -4 16.30 3.20 -4 -12 4 12.80 2.80 0 12 -4 13.90 3.50 0 -12 -4 16.60 3.70 0 12 -4 15.00 2.70 0 -12 4 18.10 3.00 0 12 4 17.50 3.70 0 -12 4 15.50 2.80 -1 12 -4 33.40 5.10 1 -12 4 32.90 3.30 1 -12 4 31.40 3.60 -2 12 -4 57.19 6.20 2 -12 4 59.39 4.70 2 -12 4 62.09 4.50 -3 12 -4 105.39 8.20 3 -12 4 102.49 6.30 -4 12 -4 10.50 3.80 4 -12 4 9.50 2.30 -4 12 4 14.60 3.90 -5 12 -4 14.20 4.00 -6 12 4 11.70 4.00 -7 12 4 52.29 7.30 -8 12 -4 2.00 3.70 -8 12 4 0.40 3.50 7 12 -5 7.00 3.20 6 12 -5 19.60 3.80 5 12 -5 52.99 5.50 5 12 -5 48.90 6.50 4 12 -5 24.40 3.80 4 12 -5 22.50 4.90 4 12 -5 25.10 4.20 3 12 -5 26.80 3.60 3 12 -5 24.00 5.20 3 12 -5 26.20 3.80 -3 -12 5 26.60 3.90 2 12 -5 9.30 2.50 -2 -12 -5 4.00 1.50 -2 -12 -5 3.80 3.00 2 12 -5 8.80 3.30 2 12 5 2.50 2.70 -2 -12 5 9.60 2.30 1 12 -5 20.50 3.40 1 12 -5 19.10 4.40 -1 -12 5 18.90 3.30 0 12 -5 17.40 3.20 0 12 -5 21.10 4.60 0 -12 -5 20.40 4.30 0 -12 5 17.40 3.10 0 12 5 20.70 4.40 -1 12 -5 8.30 3.40 1 -12 5 7.20 1.90 1 -12 5 6.90 2.20 -2 12 -5 3.90 3.00 2 -12 5 4.10 1.70 -2 12 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1.30 1.70 -2 13 3 5.90 3.30 -3 13 -3 2.10 2.90 -3 13 3 7.40 3.40 3 -13 3 1.70 1.80 -4 13 -3 5.70 3.40 4 -13 3 7.60 2.80 -4 13 3 8.00 3.60 -5 13 -3 4.60 3.50 -5 13 3 1.20 3.20 -6 13 -3 32.80 6.00 -6 13 3 20.50 5.00 -7 13 -3 6.60 3.90 -7 13 3 -0.60 3.50 -8 13 -3 23.10 5.50 -8 13 3 20.70 5.30 7 13 -4 3.60 2.90 6 13 -4 8.00 2.90 5 13 -4 17.30 4.40 5 13 -4 18.00 3.60 3 13 -4 86.99 6.30 3 13 -4 77.49 7.20 -3 -13 4 82.59 6.00 2 13 -4 11.90 2.70 2 13 -4 10.50 3.30 2 13 4 1.60 2.40 1 13 -4 59.59 4.90 -1 -13 -4 43.90 5.50 1 13 -4 63.79 6.50 -1 -13 4 63.19 4.70 0 13 -4 27.40 5.10 0 13 -4 27.30 3.60 0 -13 4 26.90 3.40 0 13 4 28.10 4.90 -1 13 -4 39.20 5.60 1 -13 4 39.80 3.80 -2 13 -4 -0.30 2.60 2 -13 4 0.40 1.70 2 -13 4 0.30 1.30 -3 13 -4 24.50 5.30 3 -13 4 25.80 3.70 3 -13 4 28.00 3.40 -5 13 4 16.00 4.50 -6 13 -4 5.40 4.00 -6 13 4 12.30 4.50 -7 13 -4 6.70 3.90 -7 13 4 3.90 4.00 -8 13 4 6.00 4.30 7 13 -5 -0.40 3.60 6 13 -5 1.00 2.60 5 13 -5 1.10 3.30 5 13 -5 -0.10 2.30 4 13 -5 0.50 2.20 4 13 -5 0.00 3.10 4 13 -5 0.00 2.60 3 13 -5 22.80 5.20 3 13 -5 23.60 4.00 1 13 -5 21.30 4.60 1 13 -5 22.30 3.60 -1 -13 5 23.90 3.60 0 13 -5 23.20 3.60 0 13 -5 22.30 5.10 0 13 5 23.40 4.90 0 -13 5 23.20 3.50 -1 13 -5 4.40 3.10 -2 13 -5 27.30 5.50 2 -13 5 28.20 4.60 2 -13 5 27.70 3.60 -4 13 -5 26.40 5.80 4 -13 5 25.20 3.70 -5 13 -5 0.90 3.40 -5 13 5 4.10 3.80 -6 13 -5 23.60 5.40 -7 13 -5 2.20 4.20 -7 13 5 -0.30 3.70 -8 13 5 5.10 4.40 6 13 -6 0.40 2.70 5 13 -6 1.40 2.50 5 13 -6 2.10 3.70 4 13 -6 2.10 3.60 4 13 -6 1.50 2.30 3 13 -6 2.10 3.30 3 13 -6 2.60 2.30 2 13 -6 0.20 3.10 2 13 -6 -0.90 1.90 -2 -13 -6 2.00 1.40 1 13 -6 1.60 3.20 1 13 -6 4.70 2.20 -1 -13 6 3.50 2.00 1 13 6 -0.40 2.60 0 13 -6 0.90 1.90 0 13 -6 0.50 2.90 0 13 6 1.90 2.90 0 -13 6 2.00 1.80 -1 13 -6 0.20 2.90 -1 13 6 3.40 3.20 1 -13 6 -0.30 1.50 -2 13 -6 1.60 3.20 -2 13 6 0.10 2.90 2 -13 6 1.60 1.70 -3 13 -6 5.90 4.00 3 -13 6 3.50 2.00 -3 13 6 1.70 3.20 -4 13 -6 1.70 3.50 -4 13 6 3.70 3.60 -5 13 -6 24.20 5.50 -6 13 -6 1.80 3.80 -6 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1.40 2.70 6 14 -3 27.00 4.80 5 14 -3 -0.30 2.70 -5 -14 -3 1.10 1.90 5 14 -3 -0.50 2.10 3 14 -3 14.20 4.10 3 14 -3 15.10 3.20 -3 -14 3 13.30 2.80 2 14 -3 120.09 8.60 2 14 -3 118.89 7.40 -2 -14 3 115.49 7.10 1 14 -3 3.80 1.90 1 14 -3 6.50 3.20 -1 -14 -3 0.30 2.30 1 14 3 0.70 2.60 -1 -14 3 4.70 1.70 0 14 -3 147.09 9.80 0 -14 3 147.59 7.90 0 14 3 149.99 9.50 -1 14 -3 -0.40 2.60 -1 14 3 5.90 3.20 1 -14 3 -0.20 1.30 -2 14 -3 39.70 5.70 2 -14 3 38.70 3.80 -3 14 3 13.90 4.00 -5 14 -3 0.80 3.40 -5 14 3 0.10 3.30 -6 14 -3 9.40 4.10 -7 14 -3 1.40 3.70 -7 14 3 3.80 4.00 -8 14 3 0.70 4.00 7 14 -4 3.40 4.40 6 14 -4 4.20 2.90 5 14 -4 10.70 3.10 5 14 -4 11.50 4.20 4 14 -4 12.70 3.20 4 14 -4 15.60 4.50 2 14 -4 0.60 1.70 2 14 -4 2.20 3.10 -2 -14 -4 3.90 1.50 -2 -14 4 -0.20 1.50 2 14 4 2.10 2.50 0 14 -4 23.80 3.70 0 14 -4 16.20 4.10 0 -14 4 21.00 3.30 0 14 4 23.20 5.00 -1 14 -4 20.20 4.60 1 -14 4 22.60 3.30 -2 14 -4 2.60 3.10 -2 14 4 -0.20 2.70 2 -14 4 1.30 1.50 -3 14 -4 26.70 5.70 3 -14 4 27.90 3.70 -4 14 4 12.30 4.10 -6 14 -4 1.30 3.70 -6 14 4 2.90 3.80 -8 14 4 1.60 4.40 6 14 -5 12.90 3.60 5 14 -5 3.20 2.60 5 14 -5 3.90 3.70 4 14 -5 105.09 9.10 4 14 -5 107.99 7.70 3 14 -5 56.19 5.50 3 14 -5 52.99 6.80 -2 -14 -5 2.40 1.50 2 14 -5 -0.50 2.80 2 14 -5 0.40 2.00 2 14 5 2.70 2.80 0 14 -5 7.90 3.70 0 14 -5 12.50 2.90 0 14 5 13.70 3.90 0 -14 5 11.70 2.50 -1 14 -5 45.30 6.40 1 -14 5 41.90 4.40 -2 14 -5 3.40 3.50 -2 14 5 1.80 3.10 2 -14 5 1.40 1.70 -5 14 -5 0.70 3.40 -5 14 5 3.30 3.70 -6 14 -5 23.30 5.60 -6 14 5 12.50 5.00 -7 14 5 3.50 4.20 5 14 -6 12.20 3.60 5 14 -6 14.00 5.00 4 14 -6 5.60 2.80 4 14 -6 2.10 3.80 3 14 -6 29.40 4.80 3 14 -6 30.30 6.20 2 14 -6 1.60 3.30 2 14 -6 2.90 2.30 1 14 -6 67.29 7.80 1 14 -6 72.89 5.90 0 14 -6 1.90 2.10 0 14 -6 0.30 3.10 0 14 6 4.10 3.30 -1 14 -6 15.20 4.50 1 -14 6 23.50 3.90 -2 14 -6 14.50 4.80 2 -14 6 11.80 2.70 -3 14 -6 88.09 8.90 3 -14 6 96.89 6.70 -4 14 -6 0.70 3.60 -4 14 6 4.50 3.80 -5 14 -6 7.70 4.40 -5 14 6 10.80 4.50 -6 14 6 0.50 3.80 -7 14 6 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4 24.10 5.60 -5 16 -4 2.60 4.10 -5 16 4 2.10 3.90 -6 16 -4 27.90 7.60 -6 16 4 6.50 4.90 -7 16 4 2.90 4.60 5 16 -5 13.40 4.50 4 16 -5 2.30 3.80 4 16 -5 4.60 2.90 3 16 -5 38.90 5.10 3 16 -5 38.80 6.90 2 16 -5 16.90 5.00 2 16 -5 15.50 3.40 1 16 -5 27.50 6.30 1 16 -5 30.30 4.50 1 16 5 24.10 5.60 0 16 -5 12.70 4.60 0 16 5 13.40 4.40 -1 16 -5 15.10 4.70 -2 16 -5 0.40 3.60 -2 16 5 14.90 4.50 -4 16 -5 4.00 4.00 -4 16 5 2.60 3.80 -5 16 5 16.00 5.60 -6 16 5 -0.80 4.10 4 16 -6 22.80 4.40 4 16 -6 26.30 6.30 3 16 -6 0.90 3.80 3 16 -6 1.20 2.60 2 16 -6 22.10 5.90 2 16 -6 15.40 3.40 1 16 -6 11.60 5.00 1 16 -6 9.40 3.00 0 16 -6 52.09 7.70 0 16 6 57.29 7.20 -1 16 -6 1.40 3.80 -1 16 6 10.50 4.30 -2 16 -6 16.80 5.40 -2 16 6 18.40 5.00 -3 16 -6 -0.90 3.90 -3 16 6 2.10 3.90 -4 16 6 25.40 5.90 -5 16 6 2.10 4.10 -6 16 6 9.90 5.20 4 16 -7 6.80 5.00 3 16 -7 0.40 2.60 3 16 -7 -0.20 3.80 2 16 -7 2.70 2.60 2 16 -7 2.90 4.40 1 16 -7 25.60 6.70 1 16 -7 25.10 4.60 0 16 -7 10.70 5.00 -1 16 -7 7.70 4.60 -2 16 -7 -0.70 3.70 -2 16 7 3.70 4.40 -3 16 -7 19.30 5.80 -3 16 7 1.40 4.10 -4 16 7 5.10 4.80 -5 16 7 1.80 4.60 -6 16 7 4.30 5.40 4 16 -8 9.60 5.40 3 16 -8 4.90 4.70 2 16 -8 12.40 5.50 2 16 -8 12.00 3.60 1 16 -8 5.70 3.10 1 16 -8 5.40 5.00 0 16 -8 5.40 4.70 -1 16 -8 0.60 4.00 -2 16 8 12.00 5.10 -3 16 8 7.60 5.00 -4 16 8 10.90 5.10 -5 16 8 3.00 4.80 4 16 -9 -1.70 4.70 3 16 -9 11.10 6.00 2 16 -9 3.20 4.70 1 16 -9 14.10 3.80 1 16 -9 12.30 5.60 -3 16 9 8.00 5.20 -4 16 9 0.30 4.70 6 17 0 26.10 4.90 5 17 0 11.10 3.30 4 17 0 45.80 5.20 3 17 0 -0.90 2.80 2 17 0 3.10 3.10 1 17 0 16.60 4.40 0 17 0 1.20 3.10 -1 17 0 14.30 4.20 -2 17 0 1.50 3.20 -3 17 0 0.10 3.40 -4 17 0 42.50 6.80 -5 17 0 12.00 4.50 -6 17 0 23.40 5.60 6 17 -1 0.90 3.20 6 17 1 6.70 3.00 5 17 -1 39.80 5.40 4 17 -1 10.90 3.20 3 17 -1 50.69 6.40 3 17 -1 50.29 5.50 2 17 -1 24.20 5.40 2 17 1 31.60 5.60 1 17 -1 25.40 5.40 0 17 -1 15.70 4.30 0 17 1 13.10 4.10 -1 17 1 23.70 5.50 -2 17 1 20.30 4.90 -4 17 -1 3.00 3.70 -4 17 1 12.70 4.60 -6 17 -1 5.70 4.40 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5.10 -1 17 4 18.30 4.90 -2 17 4 22.60 5.40 -3 17 4 18.50 5.40 -4 17 -4 0.80 4.10 -4 17 4 13.50 5.00 -5 17 -4 4.20 4.30 -5 17 4 6.80 4.70 -6 17 4 9.90 5.00 4 17 -5 1.40 4.00 4 17 -5 1.70 2.80 3 17 -5 11.00 4.70 3 17 -5 8.90 3.20 2 17 -5 1.40 3.80 2 17 -5 -1.30 2.20 0 17 -5 21.30 5.90 0 17 5 18.00 4.80 -1 17 -5 35.40 7.10 -2 17 -5 11.60 5.10 -2 17 5 1.30 3.70 -3 17 -5 22.30 5.70 -3 17 5 11.30 4.90 -4 17 -5 1.60 4.20 -4 17 5 0.90 4.20 -5 17 5 2.40 4.40 -6 17 5 1.90 4.40 4 17 -6 -0.40 4.00 3 17 -6 3.90 2.90 3 17 -6 5.50 4.30 2 17 -6 5.30 4.40 2 17 -6 4.00 2.80 1 17 -6 6.90 4.50 1 17 -6 8.30 3.10 0 17 -6 5.90 4.50 0 17 6 5.80 4.10 -1 17 -6 -0.30 3.90 -1 17 6 9.60 4.60 -2 17 -6 9.20 4.70 -2 17 6 5.60 4.20 -3 17 -6 3.90 4.50 -3 17 6 9.50 4.80 -4 17 6 -0.30 4.10 -5 17 6 1.30 4.50 -6 17 6 10.00 6.30 4 17 -7 8.40 5.50 3 17 -7 4.70 4.60 2 17 -7 8.10 3.30 2 17 -7 8.30 5.10 1 17 -7 12.10 5.70 1 17 -7 12.10 3.60 0 17 -7 8.00 4.70 -1 17 -7 3.60 4.70 -1 17 7 11.40 5.00 -2 17 -7 0.70 4.50 -2 17 7 7.60 4.90 -3 17 7 7.10 4.70 -4 17 7 3.70 4.70 -5 17 7 1.60 4.90 4 17 -8 1.40 4.90 3 17 -8 1.30 4.60 2 17 -8 2.80 4.70 1 17 -8 4.50 4.90 1 17 -8 6.20 3.20 0 17 -8 8.60 5.10 -2 17 8 2.50 4.50 -3 17 8 2.70 4.80 -4 17 8 1.80 4.60 -5 17 8 -0.50 5.60 4 17 -9 4.50 6.20 3 17 -9 4.60 5.50 2 17 -9 4.60 5.20 -3 17 9 3.70 5.20 -4 17 9 6.90 5.60 5 18 0 33.00 5.20 3 18 0 42.70 6.60 2 18 0 8.00 3.90 1 18 0 72.09 7.50 0 18 0 33.90 6.00 -1 18 0 75.99 7.90 -2 18 0 8.90 4.40 -3 18 0 49.90 7.30 -4 18 0 7.40 4.50 -5 18 0 24.30 5.80 -6 18 0 2.70 4.30 5 18 -1 2.00 3.00 4 18 -1 1.50 2.60 3 18 -1 2.80 3.40 1 18 -1 2.30 3.30 1 18 1 8.50 3.80 0 18 -1 11.10 4.00 0 18 1 12.40 4.00 -1 18 -1 7.80 3.90 -1 18 1 3.00 3.50 -3 18 -1 9.60 4.70 -3 18 1 1.00 3.70 -5 18 -1 11.40 5.10 -5 18 1 0.80 4.00 -6 18 -1 15.70 5.60 4 18 -2 14.20 3.60 3 18 -2 24.80 4.50 3 18 -2 27.40 6.30 2 18 -2 10.40 4.40 2 18 2 1.60 3.40 1 18 -2 16.40 4.90 1 18 2 1.80 3.50 0 18 -2 -0.40 3.40 0 18 2 0.20 3.50 -1 18 -2 1.30 3.60 -1 18 2 15.90 4.60 -2 18 -2 0.00 3.50 -2 18 2 10.10 4.40 -3 18 2 22.10 5.50 -4 18 -2 0.50 3.80 -4 18 2 13.70 5.00 -5 18 -2 7.80 4.60 -6 18 2 6.80 4.90 4 18 -3 39.60 5.60 3 18 -3 6.30 4.10 3 18 -3 5.00 2.80 2 18 -3 37.00 5.20 2 18 -3 36.90 6.70 1 18 3 11.30 4.40 0 18 -3 62.69 8.00 0 18 3 66.79 7.80 -1 18 3 30.30 6.60 -2 18 -3 35.20 7.10 -2 18 3 38.30 7.00 -3 18 -3 12.60 5.20 -3 18 3 3.70 4.30 -4 18 -3 31.10 7.20 -4 18 3 40.60 7.70 -5 18 -3 4.60 4.50 -5 18 3 3.10 4.30 -6 18 3 17.60 5.80 3 18 -4 0.10 2.50 3 18 -4 -0.10 3.70 2 18 -4 1.20 3.90 2 18 -4 1.20 2.50 1 18 4 34.70 6.50 0 18 -4 2.90 3.90 0 18 4 3.30 3.90 -1 18 -4 34.20 6.90 -2 18 -4 3.30 4.00 -2 18 4 1.70 3.80 -3 18 -4 28.10 6.30 -4 18 -4 10.60 5.20 -4 18 4 3.70 4.40 -5 18 4 3.90 4.80 -6 18 4 0.30 4.70 3 18 -5 4.00 3.20 3 18 -5 2.10 4.20 2 18 -5 15.40 5.30 2 18 -5 14.40 3.70 1 18 -5 1.20 4.30 0 18 -5 2.90 4.10 0 18 5 2.70 3.90 -1 18 -5 -0.30 3.80 -1 18 5 1.90 3.90 -2 18 -5 2.00 4.10 -2 18 5 14.20 5.10 -3 18 -5 0.50 4.00 -3 18 5 2.60 4.40 -4 18 5 10.50 5.10 -5 18 5 12.30 5.40 3 18 -6 5.80 4.70 2 18 -6 9.80 3.40 2 18 -6 8.40 4.80 1 18 -6 25.70 6.30 1 18 -6 30.20 5.10 0 18 -6 4.20 4.70 -1 18 -6 20.20 6.30 -1 18 6 26.70 6.00 -2 18 -6 5.40 4.90 -2 18 6 14.20 5.40 -3 18 6 5.70 4.80 -4 18 6 2.40 4.70 -5 18 6 11.70 5.50 3 18 -7 -0.50 4.30 2 18 -7 0.90 4.30 1 18 -7 0.20 2.70 1 18 -7 0.50 4.20 0 18 -7 7.50 5.10 -1 18 -7 1.70 4.50 -2 18 7 1.80 4.40 -3 18 7 0.60 4.40 -4 18 7 0.10 4.50 -5 18 7 0.60 5.20 3 18 -8 7.50 5.70 2 18 -8 2.20 4.80 1 18 -8 2.40 4.80 -3 18 8 8.70 5.40 -4 18 8 1.80 5.10 2 19 0 0.70 3.50 1 19 0 7.30 4.00 0 19 0 0.60 3.40 -1 19 0 8.10 4.10 -2 19 0 1.90 3.80 -3 19 0 18.20 5.20 -4 19 0 0.40 3.80 -5 19 0 7.50 4.60 1 19 -1 0.60 3.50 1 19 1 3.70 3.60 0 19 -1 53.89 7.50 0 19 1 56.39 7.30 -1 19 -1 5.40 4.10 -1 19 1 0.10 3.40 -3 19 -1 0.70 3.80 -3 19 1 9.90 5.00 -4 19 -1 1.20 4.10 -4 19 1 10.70 4.90 -5 19 -1 -0.10 4.10 -5 19 1 0.80 4.30 3 19 -2 8.30 4.40 2 19 -2 1.70 3.70 1 19 -2 48.50 7.50 1 19 2 49.10 7.10 0 19 -2 0.90 3.70 0 19 2 0.70 3.70 -1 19 -2 57.49 7.90 -1 19 2 52.79 7.60 -2 19 -2 6.60 4.20 -2 19 2 2.40 4.00 -3 19 -2 17.50 5.30 -3 19 2 8.30 4.60 -4 19 -2 5.40 4.40 -4 19 2 1.40 4.10 -5 19 2 2.10 4.70 3 19 -3 -1.30 2.90 3 19 -3 1.80 4.00 2 19 -3 7.80 4.40 1 19 -3 -0.30 3.80 1 19 3 0.40 3.60 0 19 -3 3.90 4.10 0 19 3 2.70 3.90 -1 19 -3 -0.50 3.80 -1 19 3 1.40 3.80 -2 19 -3 15.00 5.30 -2 19 3 6.10 4.40 -3 19 -3 1.00 4.00 -3 19 3 0.60 4.00 -4 19 -3 14.00 5.60 -4 19 3 15.60 5.50 -5 19 3 0.70 4.40 3 19 -4 36.70 7.30 2 19 -4 -0.80 2.50 2 19 -4 1.10 3.80 1 19 -4 33.50 7.10 0 19 -4 1.50 4.10 0 19 4 2.60 3.90 -1 19 4 33.90 7.10 -2 19 -4 -0.10 4.20 -2 19 4 0.90 3.90 -4 19 -4 3.50 7.60 -4 19 4 6.40 4.80 -5 19 4 5.10 5.00 3 19 -5 1.20 4.40 2 19 -5 17.90 6.00 1 19 -5 -1.50 3.90 0 19 -5 26.30 6.30 -1 19 -5 6.30 4.70 -1 19 5 0.80 4.00 -2 19 -5 11.50 5.20 -2 19 5 15.00 5.30 -3 19 -5 1.60 5.00 -3 19 5 1.30 4.50 -4 19 5 5.20 4.80 -5 19 5 1.30 4.70 3 19 -6 5.80 5.20 2 19 -6 1.80 4.60 1 19 -6 0.30 4.60 0 19 -6 1.40 4.50 -1 19 -6 3.20 4.50 -1 19 6 2.30 4.30 -2 19 -6 -0.10 5.40 -2 19 6 2.00 4.70 -3 19 6 3.20 4.60 -4 19 6 0.80 4.90 3 19 -7 0.20 4.80 2 19 -7 7.60 5.40 1 19 -7 -0.60 4.70 0 19 -7 4.10 5.00 -2 19 7 6.70 5.20 -3 19 7 1.20 4.70 -4 19 7 15.20 6.30 3 19 -8 1.70 5.50 2 19 -8 -0.80 4.90 -3 19 8 2.20 5.20 2 20 0 32.50 6.60 1 20 0 18.00 5.10 0 20 0 8.20 4.20 -1 20 0 22.60 5.80 -2 20 0 35.30 7.20 -3 20 0 8.50 4.70 -4 20 0 3.10 4.30 -5 20 0 2.80 5.50 2 20 -1 2.70 3.80 1 20 -1 0.80 3.60 1 20 1 9.60 4.40 0 20 -1 3.50 4.10 0 20 1 5.10 3.90 -1 20 -1 9.80 4.80 -1 20 1 1.80 3.80 -2 20 -1 22.50 5.50 -3 20 -1 8.60 4.70 -3 20 1 1.50 4.10 -4 20 -1 7.20 4.70 -4 20 1 3.20 4.60 -5 20 1 1.90 4.80 2 20 -2 8.00 4.40 1 20 -2 5.80 4.10 1 20 2 4.50 4.10 0 20 -2 0.00 3.90 0 20 2 -0.10 3.80 -1 20 -2 5.40 4.20 -1 20 2 5.60 4.30 -2 20 -2 0.20 4.10 -2 20 2 8.20 4.80 -3 20 2 22.80 5.90 -4 20 -2 1.70 4.30 -4 20 2 8.00 5.10 -5 20 2 6.90 5.30 2 20 -3 16.20 5.50 1 20 -3 4.20 4.60 0 20 -3 27.60 6.30 0 20 3 25.10 5.80 -1 20 -3 27.00 6.70 -2 20 -3 11.80 5.30 -2 20 3 13.80 5.40 -3 20 3 23.30 6.40 -4 20 3 3.80 4.60 -5 20 3 2.50 5.10 3 20 -4 2.10 5.40 2 20 -4 0.20 4.00 1 20 -4 2.80 4.50 0 20 -4 5.90 5.00 0 20 4 5.40 4.50 -1 20 -4 10.50 5.20 -1 20 4 3.50 4.30 -2 20 -4 4.50 5.00 -2 20 4 -0.60 4.30 -3 20 -4 2.30 5.00 -3 20 4 4.30 4.60 -4 20 4 2.00 4.50 3 20 -5 4.70 5.10 2 20 -5 2.60 4.60 1 20 -5 0.30 4.40 0 20 -5 3.00 4.80 -1 20 -5 0.20 4.30 -1 20 5 1.20 4.20 -2 20 -5 -1.00 4.30 -2 20 5 3.70 4.80 -3 20 5 7.00 5.30 -4 20 5 13.00 5.70 3 20 -6 4.30 5.50 2 20 -6 0.70 4.80 1 20 -6 18.30 6.20 0 20 -6 14.40 5.80 -1 20 -6 3.80 5.90 -2 20 6 1.80 4.80 -3 20 6 6.80 5.20 -4 20 6 8.00 5.90 3 20 -7 1.60 5.90 2 20 -7 1.50 5.40 1 20 -7 0.90 5.10 -3 20 7 0.80 5.00 1 21 0 3.30 4.10 0 21 0 -0.30 3.70 -1 21 0 5.20 4.60 -2 21 0 1.50 4.40 -3 21 0 1.80 4.20 -4 21 0 7.00 5.00 2 21 -1 4.80 5.50 1 21 -1 20.50 5.60 1 21 1 12.90 5.00 0 21 -1 1.30 3.90 0 21 1 1.90 4.00 -1 21 -1 16.00 5.60 -1 21 1 18.90 5.50 -2 21 -1 1.60 4.00 -2 21 1 7.50 5.00 -3 21 -1 5.00 4.60 -3 21 1 18.40 5.70 -4 21 -1 1.30 6.70 -4 21 1 4.00 4.70 2 21 -2 7.90 4.70 1 21 -2 -0.10 3.80 0 21 -2 9.40 4.70 0 21 2 7.80 4.70 -1 21 -2 6.00 4.60 -1 21 2 0.50 4.30 -2 21 -2 27.40 6.40 -2 21 2 8.10 5.00 -3 21 -2 2.00 4.50 -3 21 2 1.70 4.60 -4 21 2 3.90 4.90 2 21 -3 0.40 4.30 1 21 -3 -0.90 4.20 0 21 -3 4.30 4.60 0 21 3 5.10 4.50 -1 21 -3 0.00 4.30 -1 21 3 0.60 4.20 -2 21 -3 0.90 4.30 -2 21 3 0.80 4.50 -3 21 -3 2.00 6.70 -3 21 3 0.10 4.40 -4 21 3 5.80 5.20 2 21 -4 24.60 6.70 1 21 -4 2.50 4.80 0 21 -4 9.40 5.40 -1 21 -4 -1.30 4.30 -1 21 4 4.60 4.70 -2 21 -4 5.10 5.40 -2 21 4 18.90 5.90 -3 21 4 5.80 5.10 -4 21 4 12.10 6.10 2 21 -5 0.30 4.50 1 21 -5 3.80 4.90 0 21 -5 6.10 5.30 -1 21 -5 20.70 7.10 -2 21 5 1.60 4.60 -3 21 5 5.00 5.10 -4 21 5 1.10 6.10 2 21 -6 0.80 5.00 1 21 -6 0.60 4.90 -2 21 6 3.60 7.20 -3 21 6 1.90 5.10 2 21 -7 1.50 6.50 1 22 0 1.60 4.10 0 22 0 5.90 4.50 -1 22 0 0.40 4.10 -2 22 0 8.80 5.00 -3 22 0 8.30 5.10 1 22 -1 1.30 4.10 0 22 -1 1.50 4.10 0 22 1 4.00 4.40 -1 22 -1 8.50 5.00 -1 22 1 2.20 4.50 -2 22 -1 0.60 4.40 -2 22 1 1.20 4.50 -3 22 -1 21.50 6.70 -3 22 1 2.00 4.90 1 22 -2 3.10 4.50 0 22 -2 2.40 4.50 0 22 2 1.20 4.40 -1 22 -2 2.00 4.70 -1 22 2 3.90 4.70 -2 22 -2 1.80 4.50 -2 22 2 7.10 5.10 -3 22 2 0.70 4.70 1 22 -3 5.40 4.90 0 22 -3 0.40 4.40 -1 22 -3 10.80 5.40 -1 22 3 5.30 4.90 -2 22 -3 1.90 5.30 -2 22 3 0.00 4.60 -3 22 3 6.70 5.30 2 22 -4 1.80 5.60 1 22 -4 2.80 5.10 0 22 -4 1.40 5.10 -1 22 -4 1.40 5.10 -1 22 4 2.60 6.80 -2 22 4 -0.20 4.50 -3 22 4 0.80 4.70 2 22 -5 3.30 5.60 1 22 -5 -0.30 4.90 0 22 -5 1.20 5.70 -2 22 5 4.10 5.10 -3 22 5 6.00 5.50 2 22 -6 2.90 5.60 0 23 0 3.10 4.40 -1 23 0 0.30 4.30 -2 23 0 -1.70 4.30 0 23 -1 4.10 4.80 0 23 1 5.70 5.40 -1 23 -1 8.30 5.30 -1 23 1 4.00 4.90 -2 23 -1 1.60 4.80 -2 23 1 0.30 4.80 1 23 -2 4.30 5.10 0 23 -2 4.70 5.00 -1 23 -2 1.60 4.60 -1 23 2 3.80 5.00 -2 23 2 6.90 5.50 -3 23 2 0.80 7.30 1 23 -3 1.00 4.60 0 23 -3 -0.60 4.60 -1 23 -3 0.30 6.00 -1 23 3 1.30 6.00 -2 23 3 1.80 5.10 -3 23 3 0.20 6.70 1 23 -4 3.10 5.50 0 23 -4 2.20 6.00 -2 23 4 6.40 5.60 -1 24 0 8.00 5.50 0 24 -1 4.10 5.40 -1 24 -1 1.50 4.90 -1 24 1 2.40 5.20 -2 24 1 0.30 6.90 0 24 -2 1.70 5.10 -1 24 2 5.30 8.40 -2 24 2 3.60 6.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 62030 _olex2_submission_special_instructions 'No special instructions were received' # start Validation Reply Form _vrf_PLAT420_shelx ; PROBLEM: D-H Bond Without Acceptor O6 --H6B . Please Check RESPONSE: H atoms are placed at calculated positions using HFIX ; _vrf_PLAT911_shelx ; PROBLEM: Missing FCF Refl Between Thmin & STh/L= 0.594 690 Report RESPONSE: Data quality is poor FCF Refl omitted during data reduction ;