#============================================================================= data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 16 _journal_issue 3 _journal_year 2025 _journal_page_first 251 _journal_page_last 258 #============================================================================= _audit_creation_date 2025-05-01 _audit_creation_method ; Olex2 1.3-beta (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; APEX3 (Bruker, 2020) Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K. & Puschmann, H. (2009). J. Appl. Cryst. 42, 339-341. SADABS2016/2, Bruker axs, Madison, WI (2016). SAINT V8.40B - Software for the Integration of CCD Detector System Bruker Analytical X-ray Systems, Bruker axs, Madison, WI (2016). Sheldrick, G. M. (2008). Acta Cryst. A64, 112-122. Sheldrick, G. M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M., Crystal structure refinement with SHELXL, Acta Cryst., (2015). C71, 3-8. ; loop_ _publcif_info_cif.paper_type ? _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '2(C6 H16 N), 2(C2 H O4), H2 O' _chemical_formula_sum 'C16 H36 N2 O9' _chemical_formula_weight 400.47 _chemical_absolute_configuration . _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'orthorhombic' _space_group_IT_number 33 _space_group_name_H-M_alt 'P n a 21' _space_group_name_Hall 'P 2c -2n' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' _cell_length_a 14.1534(8) _cell_length_b 5.6656(3) _cell_length_c 26.8153(16) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 2150.3(2) _cell_formula_units_Z 4 _cell_measurement_reflns_used 9864 _cell_measurement_temperature 110 _cell_measurement_theta_max 27.52 _cell_measurement_theta_min 2.98 _shelx_estimated_absorpt_T_max 0.992 _shelx_estimated_absorpt_T_min 0.975 _exptl_absorpt_coefficient_mu 0.100 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.7044 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0532 before and 0.0467 after correction. The Ratio of minimum to maximum transmission is 0.9447. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.237 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description plate _exptl_crystal_F_000 872 _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.08 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0312 _diffrn_reflns_av_unetI/netI 0.0148 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 7 _diffrn_reflns_limit_k_min -7 _diffrn_reflns_limit_l_max 34 _diffrn_reflns_limit_l_min -34 _diffrn_reflns_number 60974 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.602 _diffrn_reflns_theta_min 2.878 _diffrn_ambient_temperature 110 _diffrn_detector 'CCD Plate' _diffrn_detector_area_resol_mean '512 x 512' _diffrn_detector_type APEX2 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'Bruker Kappa Apex II' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_collimation '0.6 mm' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_xray_symbol K-L~3~ _diffrn_source 'X-ray tube' _diffrn_source_current 0.0 _diffrn_source_power 0.0 _diffrn_source_target Mo _diffrn_source_type 'Siemens KFF Mo 2K-180' _diffrn_source_voltage 0.0 _diffrn_standards_number 0 _reflns_Friedel_coverage 0.956 _reflns_Friedel_fraction_full 0.999 _reflns_Friedel_fraction_max 0.996 _reflns_number_gt 4652 _reflns_number_total 4996 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. Completness statistics refer to single and composite reflections containing twin component 1 only. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT V8.40B (Bruker, 2016)' _computing_data_collection 'APEX3 (Bruker, 2020)' _computing_data_reduction 'SAINT V8.40B (Bruker, 2016)' _computing_molecular_graphics 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _refine_diff_density_max 0.289 _refine_diff_density_min -0.140 _refine_diff_density_rms 0.032 _refine_ls_abs_structure_details ; ; _refine_ls_abs_structure_Flack ? _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.055 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 254 _refine_ls_number_reflns 4996 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0309 _refine_ls_R_factor_gt 0.0269 _refine_ls_restrained_S_all 1.054 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0371P)^2^+0.3725P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0674 _refine_ls_wR_factor_ref 0.0697 _refine_special_details ; Refined as a 2-component inversion twin. ; _olex2_refinement_description ; 1. Twinned data refinement Scales: 1.34163 -0.34163 2.a Free rotating group: O9(H9C,H9D) 2.b Secondary CH2 refined with riding coordinates: C1(H1D,H1E), C2(H2A,H2B), C3(H3A,H3B), C4(H4A,H4B), C5(H5A,H5B), C7(H7A,H7B), C8(H8A,H8B), C9(H9A,H9B), C10(H10A,H10B), C11(H11A,H11B) 2.c Idealised Me refined as rotating group: N1(H1A,H1B,H1C), C6(H6A,H6B,H6C), N2(H2C,H2D,H2E), C12(H12A,H12B,H12C) 2.d Idealised tetrahedral OH refined as rotating group: O1(H1), O5(H5) ; _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.28200(9) 0.3489(2) 0.45172(5) 0.0180(3) Uani 1 1 d . . . . . H1 H 0.308323 0.216900 0.448511 0.027 Uiso 1 1 calc R U . . . O2 O 0.21324(9) 0.7836(2) 0.45517(5) 0.0196(3) Uani 1 1 d . . . . . O3 O 0.35854(8) 0.9346(2) 0.44988(5) 0.0152(3) Uani 1 1 d . . . . . O4 O 0.42687(9) 0.4905(2) 0.43488(5) 0.0199(3) Uani 1 1 d . . . . . C13 C 0.34458(12) 0.5176(3) 0.44472(6) 0.0120(3) Uani 1 1 d . . . . . C14 C 0.30026(11) 0.7668(3) 0.45046(7) 0.0120(3) Uani 1 1 d . . . . . O5 O 0.44623(8) 1.1534(2) 0.55262(5) 0.0176(3) Uani 1 1 d . . . . . H5 H 0.418534 1.284494 0.551764 0.026 Uiso 1 1 calc R U . . . O6 O 0.30243(9) 1.0126(2) 0.57171(5) 0.0209(3) Uani 1 1 d . . . . . O7 O 0.36966(8) 0.5682(2) 0.55440(5) 0.0145(3) Uani 1 1 d . . . . . O8 O 0.51521(8) 0.7184(2) 0.55118(6) 0.0193(3) Uani 1 1 d . . . . . C15 C 0.38424(12) 0.9855(3) 0.56075(6) 0.0126(3) Uani 1 1 d . . . . . C16 C 0.42798(11) 0.7358(3) 0.55475(7) 0.0117(3) Uani 1 1 d . . . . . O9 O 0.61520(9) 0.37141(18) 0.50395(5) 0.0151(2) Uani 1 1 d G . . . . H9C H 0.650105 0.463763 0.487131 0.023 Uiso 1 1 d G U . . . H9D H 0.581119 0.457668 0.517803 0.023 Uiso 1 1 d G U . . . N1 N 0.67499(10) 1.0105(3) 0.56662(5) 0.0150(3) Uani 1 1 d . . . . . H1A H 0.666538 1.143376 0.548081 0.018 Uiso 1 1 calc R U . . . H1B H 0.631630 0.900051 0.557491 0.018 Uiso 1 1 calc R U . . . H1C H 0.734198 0.952972 0.561398 0.018 Uiso 1 1 calc R U . . . C1 C 0.66286(13) 1.0680(3) 0.62051(6) 0.0169(4) Uani 1 1 d . . . . . H1D H 0.597381 1.122521 0.626508 0.020 Uiso 1 1 calc R U . . . H1E H 0.706352 1.197721 0.629754 0.020 Uiso 1 1 calc R U . . . C2 C 0.68309(13) 0.8540(3) 0.65273(7) 0.0185(4) Uani 1 1 d . . . . . H2A H 0.750499 0.810322 0.649259 0.022 Uiso 1 1 calc R U . . . H2B H 0.644636 0.719377 0.640801 0.022 Uiso 1 1 calc R U . . . C3 C 0.66117(13) 0.8988(4) 0.70762(7) 0.0193(4) Uani 1 1 d . . . . . H3A H 0.691617 1.048198 0.718057 0.023 Uiso 1 1 calc R U . . . H3B H 0.592073 0.917731 0.711742 0.023 Uiso 1 1 calc R U . . . C4 C 0.69526(15) 0.6999(4) 0.74138(7) 0.0227(4) Uani 1 1 d . . . . . H4A H 0.764931 0.689568 0.738953 0.027 Uiso 1 1 calc R U . . . H4B H 0.668878 0.549048 0.729012 0.027 Uiso 1 1 calc R U . . . C5 C 0.66804(14) 0.7290(4) 0.79630(8) 0.0251(4) Uani 1 1 d . . . . . H5A H 0.598430 0.741450 0.798747 0.030 Uiso 1 1 calc R U . . . H5B H 0.687575 0.585648 0.814732 0.030 Uiso 1 1 calc R U . . . C6 C 0.71186(18) 0.9424(5) 0.82110(8) 0.0347(5) Uani 1 1 d . . . . . H6A H 0.689493 1.086229 0.804570 0.052 Uiso 1 1 calc R U . . . H6B H 0.780820 0.933157 0.818431 0.052 Uiso 1 1 calc R U . . . H6C H 0.693659 0.946151 0.856348 0.052 Uiso 1 1 calc R U . . . N2 N 0.55366(11) 1.0120(3) 0.44097(5) 0.0146(3) Uani 1 1 d . . . . . H2C H 0.494704 0.950984 0.445129 0.018 Uiso 1 1 calc R U . . . H2D H 0.559866 1.144429 0.459883 0.018 Uiso 1 1 calc R U . . . H2E H 0.597449 0.903517 0.450570 0.018 Uiso 1 1 calc R U . . . C7 C 0.56829(13) 1.0725(3) 0.38756(6) 0.0165(3) Uani 1 1 d . . . . . H7A H 0.634103 1.126618 0.382522 0.020 Uiso 1 1 calc R U . . . H7B H 0.525401 1.203017 0.378088 0.020 Uiso 1 1 calc R U . . . C8 C 0.54915(13) 0.8597(3) 0.35457(7) 0.0178(4) Uani 1 1 d . . . . . H8A H 0.480879 0.822013 0.355585 0.021 Uiso 1 1 calc R U . . . H8B H 0.584080 0.721776 0.367769 0.021 Uiso 1 1 calc R U . . . C9 C 0.57869(13) 0.9030(4) 0.30078(7) 0.0188(4) Uani 1 1 d . . . . . H9A H 0.648317 0.918168 0.299275 0.023 Uiso 1 1 calc R U . . . H9B H 0.551040 1.053979 0.289275 0.023 Uiso 1 1 calc R U . . . C10 C 0.54757(14) 0.7061(4) 0.26572(7) 0.0198(4) Uani 1 1 d . . . . . H10A H 0.569052 0.553053 0.279484 0.024 Uiso 1 1 calc R U . . . H10B H 0.477673 0.702944 0.264495 0.024 Uiso 1 1 calc R U . . . C11 C 0.58544(14) 0.7316(4) 0.21281(7) 0.0231(4) Uani 1 1 d . . . . . H11A H 0.563824 0.884009 0.198809 0.028 Uiso 1 1 calc R U . . . H11B H 0.655355 0.734205 0.213830 0.028 Uiso 1 1 calc R U . . . C12 C 0.55325(17) 0.5325(4) 0.17883(8) 0.0313(5) Uani 1 1 d . . . . . H12A H 0.582478 0.551099 0.145931 0.047 Uiso 1 1 calc R U . . . H12B H 0.484334 0.537374 0.175425 0.047 Uiso 1 1 calc R U . . . H12C H 0.572171 0.380703 0.193217 0.047 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0145(6) 0.0082(5) 0.0313(7) 0.0001(5) 0.0021(5) 0.0001(5) O2 0.0108(6) 0.0134(6) 0.0346(8) -0.0051(6) 0.0014(5) 0.0008(5) O3 0.0137(6) 0.0096(6) 0.0224(6) -0.0004(5) 0.0002(5) -0.0009(5) O4 0.0141(7) 0.0144(6) 0.0313(7) 0.0006(5) 0.0069(5) 0.0024(5) C13 0.0124(8) 0.0101(8) 0.0135(8) 0.0001(6) 0.0009(6) -0.0002(6) C14 0.0139(8) 0.0097(8) 0.0126(8) -0.0007(6) 0.0002(6) 0.0003(7) O5 0.0149(6) 0.0076(5) 0.0302(7) -0.0009(5) 0.0016(5) -0.0006(4) O6 0.0144(6) 0.0145(6) 0.0337(7) 0.0016(5) 0.0081(5) 0.0026(5) O7 0.0135(6) 0.0091(5) 0.0210(6) 0.0004(5) -0.0002(5) -0.0018(4) O8 0.0107(6) 0.0129(6) 0.0342(8) -0.0040(6) 0.0017(5) 0.0015(5) C15 0.0147(8) 0.0101(8) 0.0131(8) -0.0001(6) 0.0004(6) 0.0001(6) C16 0.0130(7) 0.0104(8) 0.0118(8) -0.0011(6) 0.0002(6) 0.0008(6) O9 0.0127(5) 0.0113(5) 0.0212(5) -0.0001(5) 0.0046(4) 0.0001(5) N1 0.0129(7) 0.0149(7) 0.0173(7) 0.0013(6) -0.0007(5) -0.0011(6) C1 0.0177(9) 0.0161(9) 0.0169(8) -0.0005(7) 0.0016(7) 0.0007(7) C2 0.0187(9) 0.0188(9) 0.0180(9) 0.0007(7) 0.0017(7) 0.0027(7) C3 0.0184(9) 0.0216(9) 0.0178(9) 0.0008(7) 0.0019(7) 0.0024(7) C4 0.0238(10) 0.0248(9) 0.0195(10) 0.0029(8) 0.0011(7) 0.0050(8) C5 0.0246(10) 0.0315(11) 0.0192(10) 0.0054(8) 0.0027(8) 0.0031(9) C6 0.0433(14) 0.0406(13) 0.0203(10) -0.0008(9) -0.0019(9) 0.0014(11) N2 0.0129(7) 0.0158(7) 0.0151(7) -0.0017(6) -0.0006(5) 0.0017(6) C7 0.0161(8) 0.0174(9) 0.0159(8) 0.0000(7) 0.0020(7) 0.0010(7) C8 0.0185(9) 0.0184(9) 0.0164(8) -0.0024(7) 0.0018(7) -0.0027(7) C9 0.0202(9) 0.0201(9) 0.0160(8) -0.0019(7) 0.0020(7) -0.0021(8) C10 0.0208(9) 0.0219(9) 0.0166(9) -0.0021(8) 0.0008(7) -0.0005(7) C11 0.0230(9) 0.0260(10) 0.0202(10) -0.0032(7) 0.0032(8) 0.0014(8) C12 0.0387(13) 0.0344(12) 0.0208(10) -0.0078(9) 0.0009(9) 0.0012(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 H1 0.8400 . ? O1 C13 1.317(2) . ? O2 C14 1.242(2) . ? O3 C14 1.259(2) . ? O4 C13 1.204(2) . ? C13 C14 1.553(2) . ? O5 H5 0.8400 . ? O5 C15 1.312(2) . ? O6 C15 1.204(2) . ? O7 C16 1.258(2) . ? O8 C16 1.242(2) . ? C15 C16 1.553(2) . ? O9 H9C 0.8493 . ? O9 H9D 0.7807 . ? N1 H1A 0.9100 . ? N1 H1B 0.9100 . ? N1 H1C 0.9100 . ? N1 C1 1.491(2) . ? C1 H1D 0.9900 . ? C1 H1E 0.9900 . ? C1 C2 1.516(3) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C2 C3 1.526(2) . ? C3 H3A 0.9900 . ? C3 H3B 0.9900 . ? C3 C4 1.524(3) . ? C4 H4A 0.9900 . ? C4 H4B 0.9900 . ? C4 C5 1.531(3) . ? C5 H5A 0.9900 . ? C5 H5B 0.9900 . ? C5 C6 1.513(3) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? N2 H2C 0.9100 . ? N2 H2D 0.9100 . ? N2 H2E 0.9100 . ? N2 C7 1.487(2) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C7 C8 1.520(3) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C8 C9 1.522(2) . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C9 C10 1.524(3) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C10 C11 1.524(3) . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C11 C12 1.520(3) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C13 O1 H1 109.5 . . ? O1 C13 C14 111.98(13) . . ? O4 C13 O1 126.11(16) . . ? O4 C13 C14 121.92(15) . . ? O2 C14 O3 126.39(16) . . ? O2 C14 C13 118.71(14) . . ? O3 C14 C13 114.89(14) . . ? C15 O5 H5 109.5 . . ? O5 C15 C16 112.13(13) . . ? O6 C15 O5 126.21(16) . . ? O6 C15 C16 121.65(15) . . ? O7 C16 C15 115.26(13) . . ? O8 C16 O7 126.29(15) . . ? O8 C16 C15 118.45(14) . . ? H9C O9 H9D 103.1 . . ? H1A N1 H1B 109.5 . . ? H1A N1 H1C 109.5 . . ? H1B N1 H1C 109.5 . . ? C1 N1 H1A 109.5 . . ? C1 N1 H1B 109.5 . . ? C1 N1 H1C 109.5 . . ? N1 C1 H1D 109.5 . . ? N1 C1 H1E 109.5 . . ? N1 C1 C2 110.83(15) . . ? H1D C1 H1E 108.1 . . ? C2 C1 H1D 109.5 . . ? C2 C1 H1E 109.5 . . ? C1 C2 H2A 109.2 . . ? C1 C2 H2B 109.2 . . ? C1 C2 C3 112.22(16) . . ? H2A C2 H2B 107.9 . . ? C3 C2 H2A 109.2 . . ? C3 C2 H2B 109.2 . . ? C2 C3 H3A 109.1 . . ? C2 C3 H3B 109.1 . . ? H3A C3 H3B 107.8 . . ? C4 C3 C2 112.68(16) . . ? C4 C3 H3A 109.1 . . ? C4 C3 H3B 109.1 . . ? C3 C4 H4A 108.7 . . ? C3 C4 H4B 108.7 . . ? C3 C4 C5 114.34(17) . . ? H4A C4 H4B 107.6 . . ? C5 C4 H4A 108.7 . . ? C5 C4 H4B 108.7 . . ? C4 C5 H5A 108.8 . . ? C4 C5 H5B 108.8 . . ? H5A C5 H5B 107.7 . . ? C6 C5 C4 113.92(18) . . ? C6 C5 H5A 108.8 . . ? C6 C5 H5B 108.8 . . ? C5 C6 H6A 109.5 . . ? C5 C6 H6B 109.5 . . ? C5 C6 H6C 109.5 . . ? H6A C6 H6B 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? H2C N2 H2D 109.5 . . ? H2C N2 H2E 109.5 . . ? H2D N2 H2E 109.5 . . ? C7 N2 H2C 109.5 . . ? C7 N2 H2D 109.5 . . ? C7 N2 H2E 109.5 . . ? N2 C7 H7A 109.5 . . ? N2 C7 H7B 109.5 . . ? N2 C7 C8 110.67(15) . . ? H7A C7 H7B 108.1 . . ? C8 C7 H7A 109.5 . . ? C8 C7 H7B 109.5 . . ? C7 C8 H8A 109.2 . . ? C7 C8 H8B 109.2 . . ? C7 C8 C9 112.02(15) . . ? H8A C8 H8B 107.9 . . ? C9 C8 H8A 109.2 . . ? C9 C8 H8B 109.2 . . ? C8 C9 H9A 109.0 . . ? C8 C9 H9B 109.0 . . ? C8 C9 C10 112.78(16) . . ? H9A C9 H9B 107.8 . . ? C10 C9 H9A 109.0 . . ? C10 C9 H9B 109.0 . . ? C9 C10 H10A 108.8 . . ? C9 C10 H10B 108.8 . . ? H10A C10 H10B 107.7 . . ? C11 C10 C9 113.78(17) . . ? C11 C10 H10A 108.8 . . ? C11 C10 H10B 108.8 . . ? C10 C11 H11A 109.1 . . ? C10 C11 H11B 109.1 . . ? H11A C11 H11B 107.8 . . ? C12 C11 C10 112.48(18) . . ? C12 C11 H11A 109.1 . . ? C12 C11 H11B 109.1 . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C13 C14 O2 -7.7(2) . . . . ? O1 C13 C14 O3 172.21(16) . . . . ? O4 C13 C14 O2 172.16(18) . . . . ? O4 C13 C14 O3 -8.0(2) . . . . ? O5 C15 C16 O7 -169.48(16) . . . . ? O5 C15 C16 O8 11.0(2) . . . . ? O6 C15 C16 O7 10.6(3) . . . . ? O6 C15 C16 O8 -168.88(18) . . . . ? N1 C1 C2 C3 -173.86(15) . . . . ? C1 C2 C3 C4 -171.12(16) . . . . ? C2 C3 C4 C5 -175.59(17) . . . . ? C3 C4 C5 C6 -63.8(2) . . . . ? N2 C7 C8 C9 -170.70(14) . . . . ? C7 C8 C9 C10 -171.90(16) . . . . ? C8 C9 C10 C11 -173.67(16) . . . . ? C9 C10 C11 C12 179.94(17) . . . . ? _shelx_res_file ; TITL 2212lp122_0ma_a.res in Pna2(1) 2212lp122_0ma.res created by SHELXL-2018/3 at 10:06:05 on 08-Dec-2022 REM Old TITL 2212lp122_0ma in Pna2(1) REM SHELXT solution in Pna2(1): R1 0.120, Rweak 0.006, Alpha 0.002 REM 0.509 for 342 systematic absences, Orientation as input REM Flack x = 0.281 ( 0.176 ) from 1956 Parsons' quotients REM Formula found by SHELXT: C18 O9 CELL 0.71073 14.1534 5.6656 26.8153 90 90 90 ZERR 4 0.0008 0.0003 0.0016 0 0 0 LATT -1 SYMM -X,-Y,0.5+Z SYMM 0.5+X,0.5-Y,+Z SYMM 0.5-X,0.5+Y,0.5+Z SFAC C H N O UNIT 64 144 8 36 L.S. 10 PLAN 10 SIZE 0.25 0.1 0.08 TEMP -163.15 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta TWIN -1 0 0 0 -1 0 0 0 -1 2 OMIT 0 0 2 OMIT 0 0 -2 REM REM REM WGHT 0.037100 0.372500 BASF -0.34163 FVAR 0.39488 O1 4 0.281997 0.348907 0.451722 11.00000 0.01447 0.00823 = 0.03132 0.00010 0.00207 0.00010 AFIX 147 H1 2 0.308323 0.216900 0.448511 11.00000 -1.50000 AFIX 0 O2 4 0.213236 0.783565 0.455171 11.00000 0.01081 0.01342 = 0.03459 -0.00507 0.00143 0.00075 O3 4 0.358541 0.934642 0.449881 11.00000 0.01369 0.00959 = 0.02243 -0.00037 0.00022 -0.00093 O4 4 0.426871 0.490474 0.434879 11.00000 0.01410 0.01435 = 0.03130 0.00058 0.00690 0.00244 C13 1 0.344582 0.517614 0.444723 11.00000 0.01240 0.01011 = 0.01354 0.00010 0.00086 -0.00017 C14 1 0.300262 0.766798 0.450464 11.00000 0.01387 0.00970 = 0.01255 -0.00072 0.00015 0.00025 O5 4 0.446232 1.153430 0.552620 11.00000 0.01489 0.00765 = 0.03024 -0.00086 0.00162 -0.00058 AFIX 147 H5 2 0.418534 1.284494 0.551764 11.00000 -1.50000 AFIX 0 O6 4 0.302433 1.012633 0.571706 11.00000 0.01438 0.01445 = 0.03372 0.00159 0.00810 0.00261 O7 4 0.369664 0.568240 0.554401 11.00000 0.01348 0.00910 = 0.02103 0.00042 -0.00016 -0.00181 O8 4 0.515208 0.718436 0.551178 11.00000 0.01065 0.01295 = 0.03424 -0.00403 0.00170 0.00149 C15 1 0.384245 0.985524 0.560751 11.00000 0.01467 0.01007 = 0.01314 -0.00010 0.00045 0.00010 C16 1 0.427983 0.735791 0.554750 11.00000 0.01295 0.01043 = 0.01180 -0.00106 0.00020 0.00083 AFIX 6 O9 4 0.615196 0.371406 0.503952 11.00000 0.01267 0.01134 = 0.02118 -0.00007 0.00459 0.00009 H9C 2 0.650105 0.463763 0.487131 11.00000 -1.50000 H9D 2 0.581119 0.457668 0.517803 11.00000 -1.50000 AFIX 0 N1 3 0.674989 1.010505 0.566618 11.00000 0.01292 0.01486 = 0.01727 0.00128 -0.00075 -0.00105 AFIX 137 H1A 2 0.666538 1.143376 0.548081 11.00000 -1.20000 H1B 2 0.631630 0.900051 0.557491 11.00000 -1.20000 H1C 2 0.734198 0.952972 0.561398 11.00000 -1.20000 AFIX 0 C1 1 0.662864 1.068049 0.620506 11.00000 0.01766 0.01609 = 0.01695 -0.00050 0.00160 0.00069 AFIX 23 H1D 2 0.597381 1.122521 0.626508 11.00000 -1.20000 H1E 2 0.706352 1.197721 0.629754 11.00000 -1.20000 AFIX 0 C2 1 0.683090 0.853982 0.652728 11.00000 0.01866 0.01878 = 0.01802 0.00069 0.00170 0.00270 AFIX 23 H2A 2 0.750499 0.810322 0.649259 11.00000 -1.20000 H2B 2 0.644636 0.719377 0.640801 11.00000 -1.20000 AFIX 0 C3 1 0.661171 0.898829 0.707624 11.00000 0.01841 0.02156 = 0.01782 0.00076 0.00189 0.00242 AFIX 23 H3A 2 0.691617 1.048198 0.718057 11.00000 -1.20000 H3B 2 0.592073 0.917731 0.711742 11.00000 -1.20000 AFIX 0 C4 1 0.695258 0.699927 0.741380 11.00000 0.02377 0.02476 = 0.01951 0.00289 0.00108 0.00504 AFIX 23 H4A 2 0.764931 0.689568 0.738953 11.00000 -1.20000 H4B 2 0.668878 0.549048 0.729012 11.00000 -1.20000 AFIX 0 C5 1 0.668045 0.728978 0.796300 11.00000 0.02464 0.03154 = 0.01919 0.00544 0.00267 0.00309 AFIX 23 H5A 2 0.598430 0.741450 0.798747 11.00000 -1.20000 H5B 2 0.687575 0.585648 0.814732 11.00000 -1.20000 AFIX 0 C6 1 0.711863 0.942427 0.821096 11.00000 0.04327 0.04064 = 0.02028 -0.00079 -0.00187 0.00142 AFIX 137 H6A 2 0.689493 1.086229 0.804570 11.00000 -1.50000 H6B 2 0.780820 0.933157 0.818431 11.00000 -1.50000 H6C 2 0.693659 0.946151 0.856348 11.00000 -1.50000 AFIX 0 N2 3 0.553658 1.011982 0.440966 11.00000 0.01292 0.01581 = 0.01515 -0.00167 -0.00064 0.00165 AFIX 137 H2C 2 0.494704 0.950984 0.445129 11.00000 -1.20000 H2D 2 0.559866 1.144429 0.459883 11.00000 -1.20000 H2E 2 0.597449 0.903517 0.450570 11.00000 -1.20000 AFIX 0 C7 1 0.568288 1.072466 0.387565 11.00000 0.01615 0.01737 = 0.01587 -0.00004 0.00202 0.00099 AFIX 23 H7A 2 0.634103 1.126618 0.382522 11.00000 -1.20000 H7B 2 0.525401 1.203017 0.378088 11.00000 -1.20000 AFIX 0 C8 1 0.549155 0.859685 0.354570 11.00000 0.01846 0.01844 = 0.01636 -0.00242 0.00181 -0.00275 AFIX 23 H8A 2 0.480879 0.822013 0.355585 11.00000 -1.20000 H8B 2 0.584080 0.721776 0.367769 11.00000 -1.20000 AFIX 0 C9 1 0.578692 0.902994 0.300780 11.00000 0.02025 0.02005 = 0.01604 -0.00187 0.00200 -0.00211 AFIX 23 H9A 2 0.648317 0.918168 0.299275 11.00000 -1.20000 H9B 2 0.551040 1.053979 0.289275 11.00000 -1.20000 AFIX 0 C10 1 0.547572 0.706058 0.265721 11.00000 0.02080 0.02188 = 0.01662 -0.00212 0.00078 -0.00054 AFIX 23 H10A 2 0.569052 0.553053 0.279484 11.00000 -1.20000 H10B 2 0.477673 0.702944 0.264495 11.00000 -1.20000 AFIX 0 C11 1 0.585442 0.731606 0.212809 11.00000 0.02298 0.02604 = 0.02015 -0.00316 0.00321 0.00136 AFIX 23 H11A 2 0.563824 0.884009 0.198809 11.00000 -1.20000 H11B 2 0.655355 0.734205 0.213830 11.00000 -1.20000 AFIX 0 C12 1 0.553247 0.532514 0.178828 11.00000 0.03875 0.03440 = 0.02083 -0.00780 0.00086 0.00117 AFIX 137 H12A 2 0.582478 0.551099 0.145931 11.00000 -1.50000 H12B 2 0.484334 0.537374 0.175425 11.00000 -1.50000 H12C 2 0.572171 0.380703 0.193217 11.00000 -1.50000 AFIX 0 HKLF 4 REM 2212lp122_0ma_a.res in Pna2(1) REM wR2 = 0.0697, GooF = S = 1.055, Restrained GooF = 1.054 for all data REM R1 = 0.0269 for 4652 Fo > 4sig(Fo) and 0.0309 for all 4996 data REM 254 parameters refined using 1 restraints END WGHT 0.0372 0.3727 REM Highest difference peak 0.289, deepest hole -0.140, 1-sigma level 0.032 Q1 1 0.4066 0.8579 0.5567 11.00000 0.05 0.29 Q2 1 0.3196 0.6420 0.4486 11.00000 0.05 0.24 Q3 1 0.5600 0.7394 0.2400 11.00000 0.05 0.22 Q4 1 0.6676 0.9711 0.6403 11.00000 0.05 0.19 Q5 1 0.6744 0.8823 0.6817 11.00000 0.05 0.18 Q6 1 0.5628 0.8123 0.2812 11.00000 0.05 0.17 Q7 1 0.5581 0.8962 0.3228 11.00000 0.05 0.16 Q8 1 0.6741 0.7793 0.7239 11.00000 0.05 0.15 Q9 1 0.6702 1.0377 0.5987 11.00000 0.05 0.14 Q10 1 0.5601 1.0539 0.4168 11.00000 0.05 0.14 ; _shelx_res_checksum 16925 _shelx_hkl_file ; 1 0 0 0.00 0.10 1 0 0 0.00 0.10 1 0 0 0.10 0.10 1 0 0 0.00 0.10 1 0 0 -0.10 0.10 1 0 0 -0.20 0.10 1 0 0 -0.10 0.10 -1 0 0 -0.10 0.10 -1 0 0 0.10 0.20 -1 0 0 -0.10 0.10 -1 0 0 -0.10 0.10 -1 0 0 0.10 0.10 -1 0 0 0.00 0.10 -1 0 0 0.00 0.10 -1 0 0 0.00 0.10 1 0 0 0.10 0.10 2 0 0 4.30 0.60 2 0 0 3.40 0.50 -2 0 0 3.10 0.60 -2 0 0 3.50 0.50 -2 0 0 2.80 0.30 2 0 0 3.00 0.50 2 0 0 2.90 0.40 -2 0 0 4.40 0.60 2 0 0 5.10 0.60 2 0 0 4.00 0.40 -2 0 0 4.80 0.40 -2 0 0 5.50 0.60 -2 0 0 2.80 0.50 -3 0 0 0.70 0.90 -3 0 0 0.30 0.70 -3 0 0 0.10 0.50 3 0 0 -0.50 0.70 3 0 0 -0.50 0.50 3 0 0 -0.90 0.70 3 0 0 1.00 0.80 -3 0 0 0.70 0.70 -3 0 0 -0.70 0.80 -4 0 0 705.33 13.00 -4 0 0 734.63 13.10 4 0 0 703.03 12.40 4 0 0 712.93 13.00 4 0 0 730.73 13.00 -4 0 0 700.73 12.40 4 0 0 719.03 13.00 -4 0 0 715.73 12.90 -4 0 0 716.83 13.00 5 0 0 1.40 0.90 5 0 0 -0.10 0.60 5 0 0 -0.30 0.80 -5 0 0 -0.30 0.60 -5 0 0 -0.50 0.90 -5 0 0 0.20 0.50 5 0 0 -0.50 0.70 -5 0 0 0.30 0.90 -5 0 0 -0.70 0.80 -5 0 0 0.40 0.80 -6 0 0 8.40 1.30 -6 0 0 6.00 1.30 6 0 0 5.60 1.20 -6 0 0 8.10 1.30 6 0 0 4.90 1.00 -6 0 0 7.50 1.30 6 0 0 7.90 0.90 -6 0 0 7.50 0.80 6 0 0 9.60 1.40 -6 0 0 6.60 0.90 7 0 0 -1.60 0.80 -7 0 0 -0.50 0.60 7 0 0 0.70 1.00 7 0 0 0.20 0.70 -7 0 0 -0.10 1.10 -7 0 0 -2.10 0.90 -7 0 0 -0.30 0.70 -7 0 0 -0.30 1.00 -7 0 0 -0.20 1.20 -8 0 0 1681.63 29.40 -8 0 0 1692.03 30.20 8 0 0 1683.33 30.30 -8 0 0 1739.73 29.20 8 0 0 1700.33 30.40 -8 0 0 1706.53 30.60 8 0 0 1689.93 29.30 -8 0 0 1712.53 30.40 -8 0 0 1678.63 30.30 -9 0 0 0.50 0.80 -9 0 0 -0.40 1.10 -9 0 0 0.50 1.10 -9 0 0 -0.10 0.70 9 0 0 -0.10 1.10 9 0 0 0.30 0.80 -9 0 0 0.70 1.20 9 0 0 -1.60 1.00 10 0 0 9.50 1.80 -10 0 0 9.90 1.80 -10 0 0 9.30 1.20 10 0 0 11.20 1.80 -10 0 0 10.40 1.20 -10 0 0 11.10 1.80 -10 0 0 11.70 1.80 10 0 0 13.70 1.40 -11 0 0 1.80 1.60 -11 0 0 0.10 1.30 -11 0 0 -0.10 0.90 11 0 0 -0.30 1.30 -11 0 0 0.20 1.40 11 0 0 0.10 1.30 -11 0 0 -0.50 1.00 11 0 0 -1.20 0.80 -11 0 0 -0.60 0.80 -11 0 0 0.00 1.40 -12 0 0 57.69 3.20 -12 0 0 57.69 3.70 12 0 0 63.09 2.80 -12 0 0 54.29 3.60 -12 0 0 55.99 2.50 -12 0 0 52.39 2.90 12 0 0 58.49 3.80 -12 0 0 60.69 3.80 12 0 0 58.79 3.80 13 0 0 0.10 1.70 -13 0 0 -0.10 1.60 -13 0 0 -1.40 1.60 -13 0 0 -1.80 1.50 13 0 0 0.40 1.10 -14 0 0 131.29 5.60 -14 0 0 127.59 5.70 -14 0 0 134.59 5.90 14 0 0 135.99 5.80 15 0 0 2.00 1.90 -15 0 0 1.70 2.20 -15 0 0 0.20 1.90 16 0 0 26.50 3.10 -16 0 0 35.40 3.80 16 0 0 24.90 3.40 -16 0 0 35.00 4.00 17 0 0 -1.20 2.10 -17 0 0 -0.50 2.10 17 0 0 1.00 1.90 -17 0 0 2.10 2.70 18 0 0 31.70 4.10 18 0 0 32.40 3.70 -18 0 0 27.40 4.00 -18 0 0 32.00 3.90 0 1 0 -0.30 0.50 0 1 0 0.00 0.50 0 1 0 0.00 0.50 0 -1 0 0.70 0.60 0 1 0 1.60 0.60 0 1 0 0.90 0.50 0 1 0 0.50 0.50 1 1 0 502.35 8.80 1 1 0 512.65 8.90 1 1 0 494.55 8.80 -1 -1 0 474.75 8.30 -1 1 0 507.45 8.80 -1 1 0 503.25 8.60 1 1 0 492.95 8.60 -1 -1 0 483.25 8.30 -1 -1 0 470.75 8.40 -1 -1 0 466.45 8.40 -1 1 0 490.35 8.90 1 -1 0 480.05 8.30 1 -1 0 504.15 8.30 1 -1 0 475.55 8.60 -1 -1 0 468.85 8.40 -1 1 0 497.65 8.70 1 1 0 503.05 8.80 -1 -1 0 466.85 8.80 -1 1 0 498.05 8.60 1 1 0 512.65 8.50 1 -1 0 469.95 8.30 -1 1 0 501.55 8.90 1 1 0 501.65 8.80 2 1 0 659.33 11.50 2 -1 0 638.74 11.10 2 1 0 642.84 11.00 -2 1 0 628.84 11.00 2 1 0 672.33 11.10 2 -1 0 625.74 11.00 2 -1 0 637.24 11.00 2 -1 0 629.24 10.80 2 1 0 641.24 11.40 -2 1 0 652.03 10.90 -2 1 0 628.44 10.80 -2 -1 0 648.84 11.10 -2 1 0 636.84 11.50 -2 -1 0 644.34 10.90 2 1 0 641.94 10.90 -2 1 0 644.84 11.10 2 1 0 639.54 11.30 2 1 0 640.14 11.40 2 -1 0 633.34 11.00 -2 -1 0 635.24 11.10 -2 1 0 624.74 11.40 2 1 0 582.44 11.00 -2 -1 0 634.54 11.10 -2 -1 0 642.24 11.50 -2 -1 0 647.14 11.10 -2 -1 0 643.24 10.80 -2 1 0 632.94 11.10 2 1 0 622.24 11.40 -3 1 0 526.25 10.00 -3 -1 0 527.15 9.90 -3 1 0 516.05 9.80 -3 1 0 528.85 9.40 -3 -1 0 537.15 9.60 -3 1 0 534.65 9.60 -3 1 0 529.05 9.50 -3 1 0 537.65 9.90 -3 -1 0 534.35 9.70 3 -1 0 532.55 9.80 3 1 0 530.75 9.90 -3 -1 0 529.05 9.70 3 -1 0 532.65 9.60 3 1 0 518.45 9.80 3 -1 0 543.05 9.60 -3 -1 0 533.55 9.70 3 1 0 521.95 9.20 3 -1 0 525.85 9.60 3 1 0 532.55 9.60 3 1 0 540.65 9.90 -4 -1 0 9.40 1.20 4 1 0 12.50 1.20 -4 1 0 10.70 1.20 -4 1 0 9.70 1.00 -4 -1 0 12.50 1.20 -4 -1 0 11.20 1.10 -4 -1 0 11.20 1.10 4 -1 0 12.90 1.30 4 -1 0 10.80 1.10 4 1 0 12.30 1.30 -4 1 0 9.20 1.10 -4 1 0 9.30 1.00 -4 -1 0 10.90 1.10 4 -1 0 9.00 1.00 4 1 0 13.60 1.20 4 1 0 9.30 1.10 -4 1 0 9.50 0.90 4 -1 0 10.60 1.10 5 -1 0 340.57 7.00 -5 1 0 335.77 6.90 -5 1 0 335.37 7.20 -5 1 0 333.27 6.80 5 1 0 315.27 6.90 5 1 0 343.07 7.30 5 1 0 335.97 7.10 -5 1 0 340.87 7.00 -5 -1 0 339.47 7.00 -5 -1 0 329.47 7.00 -5 -1 0 339.67 7.30 -5 -1 0 334.97 7.00 5 -1 0 345.87 7.20 5 1 0 329.77 6.90 5 1 0 335.47 7.00 -5 -1 0 336.77 7.10 5 -1 0 329.47 7.00 5 -1 0 340.37 7.00 6 1 0 1695.23 29.10 -6 1 0 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4 3 0 16.70 1.80 4 -3 0 16.50 1.30 4 3 0 15.60 1.70 -4 -3 0 17.50 1.30 4 -3 0 17.70 1.20 4 -3 0 15.80 1.30 4 3 0 18.40 1.50 -4 3 0 13.60 1.60 4 -3 0 16.60 1.20 -4 -3 0 18.40 1.40 -4 -3 0 17.30 1.30 -4 -3 0 16.10 1.20 4 -3 0 16.20 1.30 4 3 0 16.70 1.60 -4 3 0 15.10 1.50 -4 3 0 19.50 2.00 -4 -3 0 17.30 2.00 4 3 0 14.80 1.70 5 3 0 252.67 6.20 -5 3 0 240.28 5.30 -5 3 0 251.77 5.90 5 3 0 233.88 6.20 5 3 0 246.48 6.50 -5 3 0 241.88 6.40 5 -3 0 240.68 5.00 5 -3 0 242.48 5.40 -5 -3 0 244.78 6.50 -5 -3 0 237.78 6.70 -5 3 0 241.88 6.60 5 -3 0 234.68 4.90 -5 -3 0 244.38 5.60 5 -3 0 242.08 5.30 -5 -3 0 244.68 5.60 5 3 0 239.78 6.40 5 -3 0 234.58 5.40 5 3 0 237.38 5.30 5 -3 0 238.48 5.20 -5 -3 0 238.88 5.50 -5 -3 0 234.28 5.50 6 3 0 233.28 6.30 -6 3 0 244.78 6.50 6 -3 0 232.98 5.60 -6 3 0 222.28 6.50 -6 -3 0 238.48 5.80 6 -3 0 230.38 4.50 -6 -3 0 235.08 5.80 6 3 0 236.58 5.10 -6 -3 0 227.08 5.60 6 3 0 227.68 4.80 -6 -3 0 234.68 6.50 -6 3 0 243.68 5.90 6 -3 0 239.48 4.60 6 3 0 238.88 6.50 6 -3 0 242.98 5.60 6 3 0 233.48 6.20 -6 -3 0 242.28 6.80 6 -3 0 233.08 5.50 -6 -3 0 235.78 5.70 -6 3 0 242.78 5.60 7 -3 0 6.90 1.30 7 3 0 8.90 1.80 -7 -3 0 4.30 1.50 -7 -3 0 5.70 1.70 7 3 0 7.30 1.00 -7 3 0 7.80 1.30 -7 3 0 8.00 0.70 -7 -3 0 8.20 1.40 -7 3 0 8.30 1.40 -7 3 0 6.70 1.60 7 -3 0 7.40 1.30 -7 -3 0 7.10 1.50 7 3 0 7.40 1.60 7 -3 0 8.00 1.30 7 3 0 8.60 1.50 -7 -3 0 7.20 1.40 -7 -3 0 7.50 1.40 7 3 0 5.30 0.90 -7 3 0 5.80 1.70 -8 3 0 80.39 3.70 8 -3 0 82.09 3.40 8 3 0 78.59 3.60 -8 -3 0 76.59 3.50 -8 3 0 80.19 3.20 8 -3 0 86.79 3.40 8 3 0 70.79 3.60 -8 -3 0 76.69 4.00 -8 -3 0 73.49 3.40 -8 -3 0 83.09 3.50 8 3 0 79.29 2.80 8 3 0 81.59 3.80 -8 3 0 83.39 2.50 -8 -3 0 82.69 3.90 9 3 0 273.07 7.50 -9 3 0 272.17 6.80 -9 3 0 282.37 7.70 9 -3 0 278.07 7.20 9 3 0 264.27 7.50 9 -3 0 263.07 7.10 -9 -3 0 268.87 7.20 -9 3 0 277.97 6.00 -9 -3 0 285.57 8.00 -9 -3 0 274.27 7.20 -9 -3 0 264.57 8.00 9 3 0 275.47 6.50 -9 -3 0 278.17 7.40 9 3 0 270.37 7.60 10 -3 0 85.09 4.00 10 3 0 85.99 4.00 -10 -3 0 82.19 4.10 -10 3 0 84.99 4.30 10 3 0 81.49 3.40 10 -3 0 76.69 3.80 -10 -3 0 82.19 4.00 10 3 0 85.29 4.20 -10 -3 0 86.79 4.50 -10 -3 0 87.49 4.10 -10 3 0 91.09 3.60 -10 -3 0 78.49 4.40 -10 3 0 83.69 3.10 10 3 0 82.79 4.10 11 -3 0 1.50 1.60 11 3 0 0.90 1.50 11 3 0 0.60 1.40 -11 -3 0 -0.30 1.80 -11 3 0 1.00 1.60 -11 -3 0 -0.50 1.60 -11 -3 0 1.70 1.70 11 -3 0 2.10 1.50 -11 3 0 1.30 1.20 -11 -3 0 2.10 1.90 11 3 0 2.70 1.60 11 3 0 0.60 1.10 -11 3 0 2.50 1.20 -11 -3 0 0.90 1.50 12 3 0 1.50 1.30 -12 -3 0 0.50 2.20 12 3 0 -1.80 1.30 12 -3 0 0.30 1.50 -12 -3 0 -1.30 1.60 -12 -3 0 -0.30 1.70 -12 3 0 0.00 1.60 -12 -3 0 -1.50 1.60 12 -3 0 -0.70 1.50 12 3 0 0.90 1.60 12 3 0 2.00 1.60 -12 3 0 -0.80 1.10 13 -3 0 32.70 3.20 -13 -3 0 33.30 3.30 -13 -3 0 41.00 3.70 -13 -3 0 35.90 3.60 13 3 0 38.20 3.00 -13 -3 0 40.60 3.70 13 3 0 32.80 3.20 -13 3 0 33.40 3.10 13 -3 0 35.60 3.30 13 3 0 39.70 3.60 -13 -3 0 34.40 3.50 13 3 0 35.30 3.40 -14 -3 0 -0.30 2.20 -14 -3 0 7.00 2.30 -14 -3 0 3.30 2.10 -14 -3 0 1.80 2.10 14 -3 0 1.30 2.10 14 -3 0 3.50 2.00 14 3 0 2.00 1.80 -14 -3 0 4.00 2.20 14 3 0 4.90 2.00 -14 3 0 1.30 1.80 14 3 0 1.10 1.50 14 3 0 5.10 2.00 -15 -3 0 -2.40 2.00 15 -3 0 -0.10 2.00 15 3 0 -0.90 1.70 15 3 0 0.20 1.80 15 -3 0 1.40 1.90 -15 -3 0 -3.80 1.90 -15 -3 0 1.90 2.20 -15 -3 0 1.90 2.10 15 3 0 0.10 1.50 15 3 0 1.40 1.90 16 -3 0 -3.50 2.00 -16 -3 0 -0.80 2.40 16 3 0 0.00 1.90 16 3 0 1.50 2.00 16 -3 0 0.80 2.00 16 3 0 0.50 2.00 -16 -3 0 -3.90 2.20 16 3 0 -1.80 2.30 -16 -3 0 3.00 2.30 0 4 0 312.07 7.70 0 4 0 316.97 7.60 0 4 0 306.17 7.70 0 -4 0 321.17 7.80 0 -4 0 305.07 7.70 0 4 0 312.57 7.60 0 4 0 318.57 7.50 -1 -4 0 105.49 2.30 1 4 0 94.79 3.70 1 4 0 102.99 4.00 1 4 0 100.59 3.80 -1 4 0 97.59 3.60 -1 4 0 109.99 3.90 1 4 0 99.69 3.80 -1 4 0 106.89 3.90 1 -4 0 106.19 3.90 -1 -4 0 104.19 4.10 -1 -4 0 98.49 3.90 -1 4 0 101.79 3.80 1 4 0 104.29 3.80 -1 4 0 99.39 3.60 -1 4 0 108.09 4.00 -1 -4 0 97.29 2.20 1 -4 0 99.59 3.90 2 4 0 -0.80 1.10 -2 4 0 0.00 1.10 -2 4 0 0.60 1.00 -2 -4 0 -0.40 0.50 -2 -4 0 -0.40 1.00 2 -4 0 0.70 1.00 -2 -4 0 -0.80 0.50 -2 4 0 -1.10 1.10 -2 4 0 0.90 1.20 -2 4 0 -1.80 0.90 2 -4 0 -0.90 1.00 2 4 0 -1.10 0.90 -2 4 0 -1.50 1.10 -2 -4 0 0.20 1.30 2 4 0 -0.60 1.20 2 -4 0 -0.40 1.00 2 4 0 0.80 1.00 2 -4 0 0.30 0.40 2 4 0 1.90 1.10 3 -4 0 168.48 3.70 3 4 0 176.68 5.20 3 -4 0 170.58 4.80 3 -4 0 172.58 4.80 -3 -4 0 174.98 5.50 -3 -4 0 175.48 4.00 -3 4 0 171.08 5.10 3 -4 0 173.08 5.30 -3 4 0 167.18 4.90 -3 4 0 166.38 5.40 -3 -4 0 176.88 3.90 3 4 0 168.68 5.20 3 -4 0 169.38 3.70 -3 -4 0 168.18 3.50 -3 -4 0 175.48 5.80 3 4 0 170.18 5.40 3 4 0 167.88 5.50 -3 4 0 174.38 5.60 -3 4 0 167.68 5.30 -3 -4 0 169.48 4.00 3 4 0 170.28 4.80 4 4 0 11.60 1.70 4 4 0 12.00 1.70 4 -4 0 12.30 1.10 -4 -4 0 10.20 2.00 4 4 0 10.80 1.40 4 4 0 15.90 2.00 -4 4 0 11.60 1.60 -4 4 0 13.60 1.90 4 -4 0 15.30 1.60 -4 -4 0 13.10 1.90 4 4 0 13.20 1.90 4 -4 0 11.50 1.50 -4 -4 0 13.40 1.30 -4 -4 0 12.60 1.10 -4 4 0 13.90 2.00 -4 -4 0 13.80 1.20 -4 -4 0 14.20 1.30 4 -4 0 14.10 1.10 5 4 0 -0.60 0.90 5 -4 0 0.60 0.90 -5 -4 0 0.90 0.80 5 4 0 0.70 1.40 -5 -4 0 -0.90 0.80 5 4 0 0.90 1.40 5 -4 0 1.10 1.00 -5 -4 0 0.20 0.80 -5 4 0 -1.10 1.40 -5 -4 0 -0.90 1.40 -5 -4 0 0.10 1.50 5 4 0 -0.80 1.10 5 -4 0 1.10 0.80 -5 4 0 -2.00 1.40 -5 4 0 -0.10 1.00 5 4 0 1.10 1.20 5 -4 0 0.60 0.80 -5 -4 0 0.50 0.90 6 4 0 14.40 1.90 -6 -4 0 10.90 2.30 -6 4 0 11.10 2.10 -6 -4 0 11.30 1.50 -6 -4 0 13.80 2.20 6 4 0 9.40 2.00 6 -4 0 10.50 1.40 -6 4 0 9.80 2.00 6 4 0 12.00 2.20 -6 -4 0 10.30 1.40 -6 4 0 12.40 1.70 6 -4 0 10.60 1.30 -6 -4 0 12.60 1.60 6 -4 0 15.20 1.70 6 4 0 12.20 1.90 -7 4 0 3.40 1.80 7 4 0 2.40 1.40 -7 4 0 3.10 1.30 7 -4 0 1.20 1.10 7 4 0 4.00 1.40 -7 -4 0 1.20 1.20 -7 -4 0 1.50 1.20 7 4 0 1.60 1.60 -7 -4 0 4.60 2.00 -7 -4 0 1.40 1.60 -7 -4 0 1.20 1.20 7 -4 0 2.10 1.20 -7 4 0 2.30 1.50 -8 -4 0 92.39 3.90 8 4 0 95.99 4.70 8 4 0 99.59 4.30 -8 -4 0 99.89 3.90 -8 -4 0 93.09 3.80 8 4 0 88.59 4.30 8 -4 0 101.79 3.80 8 -4 0 96.89 3.70 -8 4 0 105.09 4.80 -8 -4 0 92.39 4.80 -8 -4 0 87.29 4.90 -8 4 0 90.29 3.80 9 -4 0 7.50 1.60 9 4 0 4.30 1.90 -9 -4 0 2.50 2.10 -9 -4 0 6.20 1.60 -9 4 0 4.00 2.00 -9 -4 0 6.40 1.70 9 -4 0 5.80 1.50 -9 -4 0 4.40 1.60 -9 4 0 8.50 1.60 9 4 0 4.60 1.60 -9 -4 0 2.00 1.90 9 4 0 5.80 1.80 10 -4 0 20.90 2.30 -10 -4 0 23.20 2.60 -10 -4 0 15.40 2.70 -10 -4 0 19.20 2.30 10 4 0 25.30 2.90 10 -4 0 19.70 2.40 -10 4 0 20.60 2.20 -10 -4 0 24.30 2.50 -10 -4 0 24.10 3.20 10 4 0 20.50 2.70 -10 4 0 21.00 2.80 10 4 0 18.70 2.40 11 4 0 143.39 5.90 -11 -4 0 144.49 5.50 11 -4 0 150.28 5.50 -11 4 0 151.18 6.00 11 4 0 150.18 5.80 11 4 0 159.18 6.30 11 -4 0 147.49 5.50 -11 -4 0 150.58 5.70 -12 -4 0 9.30 2.20 12 -4 0 9.60 2.00 12 4 0 7.50 2.00 -12 -4 0 7.90 2.30 -12 -4 0 7.80 2.70 12 4 0 7.00 2.20 12 4 0 12.70 2.40 12 -4 0 8.10 2.10 -12 4 0 9.20 2.40 -13 -4 0 3.50 2.00 -13 4 0 -1.80 1.90 13 4 0 -0.60 1.70 -13 -4 0 -1.50 1.70 13 -4 0 1.20 1.60 13 4 0 0.70 1.70 -13 -4 0 2.10 2.40 13 4 0 2.80 1.80 13 -4 0 -2.20 1.70 -13 -4 0 0.20 1.90 -14 -4 0 14.00 2.80 -14 -4 0 19.90 3.00 -14 -4 0 19.30 3.10 14 4 0 14.80 2.70 14 4 0 16.50 2.90 14 -4 0 13.40 2.80 -14 -4 0 15.10 3.00 14 -4 0 15.70 2.70 14 4 0 13.90 2.70 15 4 0 38.50 4.00 -15 -4 0 46.00 4.30 -15 -4 0 48.60 4.40 15 4 0 44.80 4.30 -15 -4 0 56.29 4.90 15 -4 0 47.50 4.20 15 4 0 43.10 4.30 -15 -4 0 46.60 4.50 15 -4 0 41.90 4.00 0 5 0 1.30 1.40 0 -5 0 -1.30 1.20 0 5 0 -0.20 1.20 0 -5 0 0.90 1.50 0 5 0 -0.80 1.30 0 -5 0 -0.30 1.50 0 5 0 2.10 1.60 0 5 0 -0.80 1.40 1 -5 0 124.49 4.90 1 5 0 125.69 4.80 -1 5 0 118.39 4.90 1 5 0 124.79 4.70 1 -5 0 134.49 4.90 -1 5 0 121.19 4.80 -1 -5 0 121.19 4.90 1 5 0 121.49 4.90 -1 -5 0 119.29 5.00 -1 5 0 120.29 4.60 1 5 0 124.69 4.90 1 5 0 127.49 4.70 -1 5 0 118.09 4.60 -1 5 0 118.79 4.80 1 -5 0 127.49 4.80 2 5 0 117.79 5.00 -2 5 0 130.69 4.60 2 -5 0 123.09 4.70 2 -5 0 122.19 4.90 -2 5 0 125.99 5.10 2 5 0 124.89 5.00 -2 5 0 124.59 4.80 -2 -5 0 121.09 5.00 2 -5 0 119.69 4.60 2 5 0 123.89 4.60 -2 -5 0 117.79 5.20 -2 -5 0 127.89 2.90 -2 5 0 126.19 4.90 -2 -5 0 122.49 2.90 2 5 0 120.79 4.70 2 5 0 124.79 4.80 -2 5 0 127.19 4.60 -3 5 0 11.80 2.10 -3 -5 0 10.20 2.10 -3 5 0 5.50 1.60 -3 -5 0 4.10 2.10 3 -5 0 9.00 0.80 -3 -5 0 6.10 1.00 3 -5 0 5.60 1.70 3 -5 0 6.00 1.80 -3 5 0 6.60 1.60 -3 5 0 6.40 2.00 3 5 0 7.70 1.80 3 5 0 8.00 1.80 3 5 0 8.80 2.30 -3 -5 0 9.00 1.00 3 5 0 7.60 2.00 3 -5 0 5.30 1.60 3 5 0 3.10 1.50 3 -5 0 6.50 0.70 4 -5 0 2.00 0.80 -4 -5 0 3.40 0.90 -4 -5 0 2.90 1.00 -4 5 0 2.00 1.70 4 5 0 3.90 2.00 4 -5 0 1.30 0.70 4 5 0 0.10 1.70 4 -5 0 1.30 1.40 4 -5 0 2.90 1.60 -4 -5 0 1.20 1.90 4 5 0 0.80 1.40 -4 5 0 5.00 1.90 4 5 0 2.00 1.40 -4 -5 0 2.00 1.60 -4 5 0 1.90 1.50 4 5 0 1.10 1.50 -5 5 0 4.60 2.00 -5 -5 0 2.20 0.80 -5 5 0 1.00 1.40 5 -5 0 2.20 0.90 5 -5 0 3.30 0.90 -5 -5 0 2.30 1.00 5 -5 0 2.00 1.40 5 5 0 -1.30 1.80 -5 -5 0 3.20 2.10 5 5 0 1.70 1.40 5 5 0 -0.20 1.40 5 5 0 1.90 1.70 -5 -5 0 2.90 1.70 -5 5 0 3.80 1.90 -6 -5 0 3.90 2.20 -6 -5 0 5.10 2.00 -6 5 0 8.20 2.00 -6 5 0 4.60 1.50 6 5 0 7.40 1.90 -6 -5 0 7.30 1.10 6 5 0 5.30 2.00 -6 5 0 6.30 2.10 -6 -5 0 6.40 1.30 6 -5 0 6.60 1.20 6 5 0 6.40 1.80 7 5 0 19.60 2.70 7 5 0 15.00 2.30 -7 5 0 12.40 2.00 -7 -5 0 17.30 1.70 -7 -5 0 15.40 2.80 7 -5 0 16.10 1.70 7 5 0 20.00 2.40 -7 -5 0 16.30 2.80 -7 -5 0 14.90 1.80 -7 5 0 15.10 2.40 -8 5 0 32.20 3.40 8 5 0 37.20 3.40 8 -5 0 38.80 2.60 8 5 0 40.10 3.30 -8 -5 0 34.90 2.50 8 5 0 44.10 3.80 -8 -5 0 29.20 3.30 -8 5 0 36.80 2.80 9 -5 0 47.70 3.00 9 5 0 53.79 3.80 9 5 0 49.00 3.80 -9 5 0 49.20 4.10 9 5 0 57.79 4.40 -9 -5 0 44.70 2.90 -10 -5 0 3.00 1.80 10 5 0 4.30 1.90 -10 5 0 7.70 2.40 10 5 0 5.50 2.30 -10 -5 0 4.20 1.60 10 -5 0 4.00 1.50 -10 -5 0 6.50 2.50 10 5 0 4.60 2.00 -11 -5 0 6.20 2.50 -11 -5 0 2.00 1.70 11 5 0 4.10 2.10 11 5 0 1.10 1.80 -11 -5 0 1.90 1.80 11 -5 0 2.60 1.50 12 -5 0 84.49 4.50 -12 -5 0 81.09 4.80 12 5 0 86.09 5.60 -12 -5 0 86.39 4.50 12 5 0 85.39 5.20 -12 -5 0 78.99 5.80 13 -5 0 167.48 6.50 -13 -5 0 173.68 6.60 13 5 0 178.38 7.70 -13 -5 0 169.58 6.90 13 5 0 168.98 7.40 -13 -5 0 160.28 7.70 0 -6 0 2.50 1.80 0 -6 0 1.20 1.60 0 6 0 3.40 1.90 0 6 0 3.10 1.80 0 6 0 3.00 1.70 0 6 0 1.70 1.70 0 6 0 3.70 1.80 0 -6 0 0.70 1.70 1 -6 0 124.59 5.40 -1 6 0 114.09 5.20 -1 -6 0 124.89 5.50 1 6 0 124.09 5.20 -1 -6 0 120.39 5.50 -1 6 0 114.49 5.40 -1 6 0 115.89 5.00 -1 6 0 115.19 5.00 1 6 0 124.29 5.20 1 6 0 123.89 5.10 -1 -6 0 122.99 5.40 -1 6 0 121.09 5.40 1 6 0 109.39 5.30 1 6 0 120.09 5.30 1 -6 0 118.39 5.30 1 -6 0 120.39 5.20 2 6 0 -0.40 1.40 -2 6 0 -2.50 1.30 -2 -6 0 -1.90 1.70 2 6 0 -0.90 1.50 -2 -6 0 -1.30 1.70 2 -6 0 -2.10 1.30 -2 6 0 -3.90 1.50 2 -6 0 0.60 1.60 -2 6 0 1.10 1.80 2 6 0 1.70 1.70 2 6 0 -3.10 1.70 -2 6 0 2.00 1.70 -2 -6 0 -3.30 1.60 -3 -6 0 88.29 2.50 -3 6 0 93.99 5.10 -3 6 0 94.69 4.90 3 6 0 82.99 4.90 -3 6 0 91.89 4.70 3 6 0 92.59 4.60 3 6 0 91.49 4.80 -3 -6 0 92.39 2.50 -3 -6 0 97.39 5.10 3 6 0 98.99 4.70 3 -6 0 98.69 4.80 -3 -6 0 88.49 5.20 -3 6 0 88.59 4.30 4 6 0 27.10 2.90 -4 6 0 31.10 3.50 4 6 0 25.60 3.10 -4 -6 0 27.80 1.80 -4 -6 0 20.40 3.30 -4 6 0 24.20 2.80 4 6 0 29.80 3.40 -4 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-4 7.60 1.80 -9 -2 -4 8.80 1.70 9 -2 4 7.90 1.60 9 -2 4 5.80 1.50 -9 -2 -4 6.50 2.00 -9 2 4 6.50 1.30 9 2 -4 8.70 1.60 -9 2 4 8.50 1.70 -9 -2 4 10.40 1.80 -9 -2 4 5.30 1.60 9 2 4 6.20 1.60 -9 2 -4 7.10 1.30 -9 -2 4 8.00 1.70 9 2 4 5.70 1.30 9 -2 -4 6.60 1.60 -9 -2 4 7.70 2.00 -9 2 -4 6.90 1.70 -9 -2 4 7.90 0.80 9 -2 -4 8.10 1.70 -9 2 -4 5.50 1.40 9 2 4 6.90 1.50 9 2 4 8.80 1.60 -10 -2 -4 522.85 11.80 -10 2 4 544.25 10.60 -10 -2 -4 546.05 12.00 -10 2 4 537.75 11.10 10 2 -4 544.75 11.70 -10 2 4 541.95 11.80 -10 -2 -4 518.05 11.90 -10 -2 -4 547.45 11.90 10 -2 4 537.05 11.90 -10 2 4 515.45 11.50 10 2 -4 531.95 11.70 -10 -2 -4 523.15 12.30 10 -2 4 527.25 11.80 -10 2 4 518.35 11.80 -10 -2 -4 508.05 11.80 10 2 -4 518.75 11.90 10 2 4 541.45 12.00 -10 2 -4 537.65 11.60 -10 -2 4 518.65 11.90 10 2 4 521.55 11.50 10 -2 -4 524.15 11.80 10 2 4 529.55 11.50 -10 -2 4 527.85 11.90 -10 2 -4 539.15 11.80 -10 2 -4 514.25 11.20 -10 -2 4 527.95 11.80 10 -2 -4 514.25 11.80 -10 -2 4 534.95 12.40 10 2 4 534.05 12.30 11 -2 4 8.50 1.90 -11 2 4 10.60 2.00 -11 -2 -4 10.70 2.00 -11 -2 -4 11.50 2.50 11 2 -4 7.40 1.70 -11 -2 -4 11.20 2.20 -11 -2 -4 12.10 2.20 11 2 -4 10.30 1.90 -11 -2 -4 11.70 2.10 -11 2 4 10.50 1.90 -11 2 4 10.40 1.50 -11 -2 -4 10.10 2.10 11 -2 4 8.00 1.90 11 2 -4 11.50 1.90 -11 2 4 10.80 1.80 -11 2 4 8.60 1.70 -11 -2 4 9.40 2.00 11 2 4 11.70 1.80 11 -2 -4 12.20 2.10 11 -2 -4 7.10 1.90 -11 2 -4 15.00 2.00 -11 -2 4 9.50 2.00 -11 2 -4 13.10 2.10 -11 -2 4 10.20 2.10 -11 -2 4 12.70 2.50 -11 2 -4 13.50 2.20 11 2 4 9.00 1.70 11 2 4 14.00 2.20 11 2 4 9.40 2.00 12 2 -4 137.39 5.50 -12 2 4 140.09 5.50 -12 -2 -4 140.19 6.10 -12 2 4 145.49 5.20 12 -2 4 137.79 5.50 12 -2 4 140.69 5.60 -12 -2 -4 136.39 5.40 12 2 -4 138.29 5.30 12 2 -4 147.99 5.40 -12 -2 -4 146.39 5.80 -12 2 4 136.19 5.00 -12 -2 -4 138.89 5.60 -12 2 4 143.49 5.50 -12 -2 -4 133.09 5.30 -12 -2 -4 139.29 5.60 12 2 4 138.19 5.70 12 -2 -4 146.49 5.70 -12 2 -4 144.79 5.60 12 2 4 140.69 5.60 12 -2 -4 131.59 5.40 -12 2 -4 136.39 5.00 12 2 4 138.79 5.00 -12 -2 4 140.29 5.60 -12 -2 4 134.49 5.50 -12 2 -4 144.19 5.80 -12 -2 4 139.89 5.40 12 2 4 134.19 5.10 -12 -2 4 142.19 5.60 -12 -2 4 140.69 5.90 -13 2 4 259.37 7.50 -13 -2 -4 272.87 8.60 -13 2 4 249.68 7.30 13 -2 4 258.97 8.00 13 2 -4 258.37 8.10 13 -2 4 259.47 8.10 -13 -2 -4 266.07 7.80 -13 -2 -4 255.97 8.10 13 2 -4 261.87 7.70 -13 -2 -4 263.57 8.20 -13 -2 -4 258.17 7.80 -13 -2 -4 265.07 8.30 -13 2 4 250.87 8.00 -13 2 4 257.97 8.20 13 2 -4 253.37 7.70 13 -2 -4 269.87 8.20 13 2 4 257.17 7.60 -13 -2 4 251.27 8.10 -13 2 -4 264.07 8.10 -13 2 -4 259.97 7.50 13 2 4 258.17 8.20 13 2 4 258.17 7.40 -13 -2 4 266.47 8.20 -13 -2 4 254.97 8.40 13 -2 -4 242.78 7.90 -13 2 -4 261.07 8.40 -13 -2 4 255.37 8.00 -13 -2 4 269.47 7.90 13 2 4 267.57 8.10 -14 -2 -4 20.70 3.00 14 -2 4 17.70 2.70 -14 -2 -4 18.20 2.70 -14 2 4 19.70 2.70 14 -2 4 16.40 2.60 14 2 -4 23.00 2.80 -14 -2 -4 17.60 2.80 14 2 -4 18.90 2.70 -14 -2 -4 16.40 2.80 -14 2 4 18.10 2.50 -14 -2 -4 15.00 2.60 -14 2 4 23.40 2.70 14 2 -4 25.60 2.90 -14 -2 4 30.40 3.30 -14 -2 4 23.70 3.30 14 2 4 22.20 2.70 -14 2 -4 20.00 2.60 -14 -2 4 24.90 2.90 14 2 4 17.90 2.60 -14 -2 4 22.30 2.80 14 -2 -4 14.60 2.60 14 -2 -4 20.40 2.90 -14 2 -4 23.30 3.80 14 2 4 21.80 2.50 15 2 -4 5.10 2.10 15 -2 4 3.50 2.10 -15 -2 -4 5.30 2.40 -15 -2 -4 5.20 2.50 -15 2 4 5.10 1.90 15 2 -4 -0.10 1.80 -15 -2 -4 8.30 2.70 15 2 -4 6.40 2.00 -15 2 4 4.80 2.00 15 -2 4 8.00 2.50 15 -2 -4 3.30 2.00 -15 -2 4 4.70 2.40 15 2 4 1.80 1.70 15 2 4 5.30 2.00 15 2 4 5.80 1.80 -15 -2 4 2.90 2.20 15 -2 -4 7.20 2.40 15 2 4 2.30 1.90 -15 2 -4 4.10 2.00 16 2 -4 1.60 2.10 -16 -2 -4 0.90 2.40 -16 2 4 2.10 1.90 -16 -2 -4 0.20 2.40 16 2 -4 -1.20 1.70 16 -2 4 -1.70 1.90 16 2 -4 0.90 1.80 -16 -2 4 3.10 2.40 16 -2 -4 1.70 2.20 16 2 4 1.50 1.90 -16 2 -4 1.00 2.00 16 2 4 -2.30 1.70 -16 2 -4 -2.90 1.80 -16 -2 4 1.20 2.50 16 2 4 1.50 1.90 17 2 -4 6.50 2.40 17 -2 4 2.10 2.30 17 2 -4 3.40 2.20 -17 2 4 3.40 2.10 -17 -2 -4 -0.70 2.50 -17 -2 -4 1.20 2.60 -17 -2 4 2.50 2.50 17 2 4 1.40 1.90 17 -2 -4 -0.70 2.30 17 2 4 -1.10 1.90 17 2 4 -0.10 2.00 -17 2 -4 1.60 2.20 -17 -2 4 1.40 2.70 0 -3 4 -0.40 0.40 0 -3 4 0.00 0.50 0 3 4 -0.40 0.90 0 -3 -4 0.00 0.30 0 -3 -4 0.20 1.00 0 3 4 0.20 1.10 0 3 -4 -0.20 0.90 0 3 -4 0.90 0.90 0 -3 -4 -1.10 0.70 0 -3 4 -0.60 0.90 0 -3 -4 -0.20 0.30 0 3 -4 0.60 1.00 0 -3 -4 -0.30 1.00 0 -3 4 0.40 0.50 0 3 4 0.40 0.90 0 3 4 -1.50 0.90 0 3 4 -0.50 0.90 0 3 -4 -0.30 0.70 0 -3 4 0.20 0.50 0 3 4 -1.00 0.80 0 -3 4 0.10 0.50 0 3 -4 -0.30 0.70 1 -3 4 188.88 3.90 -1 -3 -4 181.78 4.80 -1 -3 -4 182.38 3.70 -1 -3 -4 192.58 3.80 1 -3 4 192.78 4.00 1 3 -4 194.78 4.70 1 -3 4 188.48 5.20 -1 3 4 193.38 5.00 1 -3 4 195.28 3.90 1 3 -4 184.38 4.60 -1 3 4 195.88 5.10 -1 -3 -4 192.38 5.20 -1 3 4 186.68 5.30 -1 -3 -4 191.18 5.30 1 3 -4 190.88 5.20 1 -3 4 185.68 4.00 -1 3 4 180.68 4.60 1 3 -4 189.98 5.00 1 -3 4 186.68 3.80 -1 3 4 179.38 5.20 1 3 -4 187.78 4.50 1 3 4 188.88 4.90 -1 3 -4 192.58 4.70 -1 -3 4 197.58 4.00 1 3 4 180.28 5.00 1 -3 -4 191.68 4.80 1 3 4 197.88 5.10 -1 -3 4 184.88 5.30 1 3 4 192.28 5.10 1 -3 -4 183.98 3.60 -1 -3 4 186.18 3.90 -1 3 -4 189.18 4.40 1 -3 -4 187.48 5.00 -1 -3 4 187.88 4.00 1 3 4 187.68 5.30 -1 -3 4 190.38 3.90 -1 3 -4 193.78 5.20 1 3 4 190.18 4.80 1 3 4 190.28 4.70 -1 -3 4 194.78 4.10 1 -3 -4 188.58 4.90 -1 3 -4 184.78 4.70 1 -3 -4 191.78 3.60 -2 -3 -4 42.50 1.40 -2 -3 -4 44.70 1.40 2 3 -4 47.10 2.00 -2 3 4 40.40 2.40 -2 -3 -4 42.20 2.20 2 -3 4 47.40 1.70 2 -3 4 46.40 1.60 -2 3 4 47.20 2.70 -2 3 4 44.20 2.30 -2 3 4 43.00 2.00 -2 -3 -4 44.40 2.70 2 3 -4 42.40 1.90 2 -3 4 42.10 1.60 -2 -3 -4 43.80 1.60 2 3 -4 41.30 2.10 2 3 -4 45.00 2.50 2 -3 4 43.70 1.60 -2 -3 -4 42.20 1.60 2 3 -4 43.30 2.40 -2 3 4 44.40 2.20 -2 3 4 41.10 2.50 -2 -3 -4 46.90 2.70 2 3 4 46.40 2.40 2 3 4 43.10 2.20 -2 -3 4 43.30 1.70 2 -3 -4 45.30 1.40 -2 -3 4 48.70 2.70 2 3 4 43.70 2.40 2 3 4 40.70 2.30 -2 3 -4 40.50 2.00 -2 3 -4 42.90 1.80 2 -3 -4 46.80 2.20 -2 -3 4 42.30 1.70 2 3 4 44.50 2.40 2 3 4 45.50 2.60 2 -3 -4 44.30 2.20 -2 -3 4 41.70 1.60 2 -3 -4 43.80 2.10 2 -3 -4 46.10 1.20 -2 -3 4 44.30 1.60 2 3 4 40.10 2.00 2 -3 -4 41.90 1.40 -2 3 -4 43.10 2.40 3 -3 4 150.08 3.60 -3 3 4 149.69 4.40 3 -3 4 146.19 3.60 3 3 -4 158.08 4.70 -3 -3 -4 158.68 4.40 -3 -3 -4 152.78 3.40 3 -3 4 148.69 3.90 -3 -3 -4 150.28 4.90 -3 3 4 155.68 4.60 -3 -3 -4 153.48 3.50 -3 -3 -4 144.49 3.50 -3 3 4 145.19 4.70 3 3 -4 152.08 3.70 3 -3 4 151.48 3.50 -3 -3 -4 158.48 4.90 3 3 -4 145.59 4.60 3 -3 4 147.29 3.60 3 3 -4 150.58 4.20 3 3 -4 145.69 3.90 -3 -3 -4 148.49 3.60 -3 3 4 144.99 4.70 -3 3 4 141.99 3.90 -3 3 4 152.58 4.10 3 3 4 147.19 4.60 3 3 4 153.78 4.30 3 3 4 143.69 4.60 -3 -3 4 145.39 3.70 -3 -3 4 149.19 3.70 3 3 4 149.49 4.60 3 -3 -4 151.48 3.40 -3 -3 4 142.19 4.70 -3 3 -4 153.28 4.50 3 -3 -4 150.88 4.00 -3 3 -4 146.59 3.70 -3 -3 4 146.39 3.60 3 -3 -4 153.08 3.30 3 3 4 152.48 3.70 3 -3 -4 144.89 4.00 3 -3 -4 154.48 3.20 -3 -3 4 146.39 3.60 3 -3 -4 154.18 3.40 -3 -3 4 151.18 3.80 4 -3 4 52.19 2.00 4 -3 4 51.99 2.10 4 3 -4 48.00 1.80 -4 -3 -4 47.20 2.90 -4 -3 -4 53.29 2.10 -4 -3 -4 50.99 2.00 -4 -3 -4 46.90 2.80 4 3 -4 52.39 2.80 -4 3 4 50.79 2.90 -4 -3 -4 47.80 2.00 4 3 -4 51.59 2.80 -4 3 4 46.90 2.60 -4 3 4 49.90 2.10 -4 -3 -4 50.19 2.00 -4 3 4 51.29 2.70 -4 -3 -4 50.79 2.50 4 -3 4 52.19 2.10 4 -3 4 51.29 2.00 4 -3 4 46.40 1.90 4 3 -4 49.90 2.20 4 3 -4 48.20 2.50 4 -3 -4 50.59 1.90 -4 3 -4 48.80 1.80 -4 -3 4 49.99 2.90 4 3 4 52.39 2.80 -4 -3 4 46.70 2.10 4 3 4 45.80 2.30 4 -3 -4 45.80 2.10 4 -3 -4 47.90 1.90 -4 3 -4 49.00 2.50 -4 3 -4 50.19 2.00 4 -3 -4 45.00 2.10 4 -3 -4 49.80 1.80 -4 -3 4 46.60 2.10 4 3 4 50.39 2.80 4 3 4 47.80 1.80 4 -3 -4 49.80 2.30 4 -3 -4 51.39 1.90 -4 -3 4 48.30 2.10 4 3 4 48.10 2.70 -4 -3 4 52.59 2.20 5 3 -4 25.40 1.20 5 3 -4 24.90 2.00 5 3 -4 23.90 1.20 5 3 -4 24.70 2.30 -5 -3 -4 24.60 2.20 -5 -3 -4 22.80 2.30 -5 3 4 18.40 1.90 -5 3 4 25.60 1.60 5 3 -4 25.90 1.70 5 -3 4 25.50 1.30 -5 3 4 23.90 1.60 -5 -3 -4 23.70 2.30 -5 -3 -4 22.60 1.80 5 3 -4 27.50 2.30 5 -3 4 24.60 1.70 -5 -3 -4 25.00 1.70 -5 -3 -4 28.30 1.80 -5 -3 -4 26.40 1.80 -5 3 4 23.70 2.10 5 -3 4 27.70 1.80 5 -3 4 22.10 1.70 5 -3 -4 23.90 1.70 -5 -3 4 25.00 1.70 5 3 4 23.90 1.80 5 -3 -4 20.80 1.60 -5 3 -4 21.90 1.70 5 -3 -4 25.90 1.70 5 -3 -4 24.20 1.50 5 -3 -4 22.30 1.60 -5 -3 4 24.80 1.80 -5 3 -4 24.60 2.00 5 3 4 26.50 2.30 -5 -3 4 28.20 1.90 -5 -3 4 24.20 1.80 5 3 4 21.60 2.00 5 -3 -4 21.80 1.50 -5 -3 4 22.30 2.20 5 3 4 25.80 2.20 6 -3 4 20.40 1.10 -6 -3 -4 26.90 1.90 6 -3 4 20.10 1.70 -6 3 4 21.60 2.20 6 3 -4 19.90 1.40 -6 -3 -4 20.70 2.10 6 3 -4 25.00 1.80 -6 3 4 22.00 1.60 -6 3 4 20.60 2.00 -6 3 4 20.90 1.70 6 -3 4 22.10 1.70 6 -3 4 21.80 1.80 6 -3 4 21.70 1.20 6 3 -4 26.00 2.50 -6 -3 -4 17.70 2.10 6 3 -4 19.10 2.00 -6 -3 -4 23.40 1.80 -6 -3 -4 23.30 1.80 -6 -3 -4 20.70 2.20 6 3 -4 24.30 2.20 -6 -3 -4 24.50 1.90 6 -3 -4 21.90 1.50 -6 3 -4 22.30 1.10 6 -3 -4 21.20 1.70 -6 -3 4 22.20 1.80 6 -3 -4 20.50 1.40 -6 -3 4 21.60 2.20 6 -3 -4 20.70 1.70 6 3 4 24.20 2.30 6 -3 -4 23.60 1.80 -6 -3 4 24.00 1.90 -6 3 -4 23.30 2.10 6 3 4 21.60 2.10 -6 3 -4 23.00 1.80 6 3 4 24.50 2.30 -6 -3 4 24.10 1.90 6 3 4 22.70 1.20 6 3 4 19.30 1.60 -6 -3 4 23.40 1.90 -7 3 4 60.49 3.20 7 3 -4 65.89 3.50 -7 -3 -4 61.69 3.40 7 3 -4 62.19 2.80 7 -3 4 63.39 2.90 -7 -3 -4 59.99 3.60 7 3 -4 56.09 3.20 -7 3 4 60.89 1.80 -7 -3 -4 57.39 3.50 -7 3 4 60.39 2.40 -7 -3 -4 58.59 2.90 -7 -3 -4 60.29 3.00 7 -3 4 60.19 4.30 7 -3 4 60.39 2.80 7 3 -4 59.69 2.40 -7 -3 -4 56.69 2.90 7 3 -4 59.49 3.10 -7 3 4 56.89 3.40 7 3 4 59.59 2.60 7 3 4 57.09 3.20 7 3 4 57.29 3.20 -7 -3 4 62.49 3.60 7 -3 -4 63.49 1.80 -7 3 -4 60.39 2.90 -7 3 -4 60.19 2.00 7 3 4 60.49 2.20 7 -3 -4 62.19 2.80 -7 -3 4 58.89 2.90 -7 -3 4 60.49 2.90 -7 -3 4 60.49 2.90 7 -3 -4 60.89 2.80 7 3 4 57.29 3.30 7 -3 -4 56.29 2.70 -7 3 -4 62.19 2.80 8 3 -4 75.49 2.90 -8 -3 -4 73.79 3.50 -8 -3 -4 72.39 3.40 -8 -3 -4 71.29 4.00 8 3 -4 79.99 3.30 -8 3 4 73.89 2.30 8 3 -4 73.89 3.60 -8 -3 -4 79.09 4.10 8 3 -4 86.59 4.10 8 -3 4 85.49 3.50 -8 -3 -4 76.69 4.00 -8 -3 -4 81.79 3.50 8 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4.20 -10 3 4 64.49 3.30 10 3 -4 66.09 3.40 10 3 -4 71.39 4.10 -10 3 4 70.09 3.80 10 3 -4 64.39 3.20 -10 -3 -4 64.79 3.60 -10 -3 -4 58.19 3.70 -10 3 -4 75.09 3.00 -10 -3 4 65.69 4.30 10 3 4 67.99 3.80 10 3 4 67.59 4.00 -10 -3 4 62.89 3.70 -10 -3 4 69.49 3.70 10 -3 -4 63.29 3.60 10 3 4 66.29 3.00 10 -3 -4 78.79 3.90 -10 -3 4 65.39 4.30 -10 -3 4 73.69 3.90 -10 3 -4 67.39 3.40 10 3 4 68.39 3.80 11 -3 4 187.08 6.20 11 3 -4 180.58 6.40 -11 -3 -4 178.98 6.40 -11 -3 -4 178.28 6.70 -11 -3 -4 178.98 6.20 11 3 -4 180.38 5.60 11 -3 4 189.28 6.20 -11 -3 -4 179.88 6.70 -11 -3 -4 174.18 6.20 -11 3 4 192.08 6.40 -11 -3 -4 183.58 6.70 11 3 -4 179.08 6.00 11 3 -4 182.88 6.50 -11 -3 4 185.78 6.20 11 3 4 194.28 6.50 11 -3 -4 179.18 6.00 11 3 4 188.68 6.30 11 -3 -4 185.68 6.20 -11 -3 4 189.68 6.80 -11 3 -4 171.78 5.80 -11 3 -4 181.98 5.30 -11 -3 4 180.78 6.70 11 3 4 181.38 5.40 -11 -3 4 187.08 6.40 -11 -3 4 188.78 6.30 11 3 4 180.28 6.40 12 -3 4 82.89 4.40 12 3 -4 88.79 4.70 12 3 -4 81.09 4.20 -12 3 4 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137.69 4.00 -2 2 8 3.50 1.00 -2 -2 -8 5.60 1.40 -2 -2 -8 5.20 1.30 -2 -2 -8 6.00 1.00 -2 2 8 7.00 1.20 -2 2 8 3.90 1.10 -2 2 8 5.60 0.60 -2 -2 -8 6.70 0.90 2 2 -8 6.40 0.90 -2 2 8 5.50 1.10 2 -2 8 6.10 1.00 -2 2 8 6.70 0.90 2 -2 8 4.80 0.90 2 2 -8 4.90 0.90 2 -2 8 5.50 1.00 -2 2 8 4.80 1.20 -2 -2 -8 5.20 0.90 -2 -2 -8 3.70 0.90 -2 2 8 7.00 0.80 2 2 -8 6.20 0.50 2 2 -8 7.00 1.30 2 2 -8 6.00 1.20 2 -2 8 5.20 1.00 2 2 -8 4.90 1.30 -2 -2 -8 4.20 0.90 2 -2 -8 6.40 0.70 -2 -2 8 5.60 0.90 2 -2 -8 5.80 1.20 2 2 8 4.60 0.80 2 -2 -8 5.00 0.80 -2 2 -8 5.00 0.90 2 2 8 5.20 0.70 2 -2 -8 8.50 1.30 2 -2 -8 4.80 0.80 2 2 8 6.00 1.20 -2 2 -8 5.70 1.20 2 2 8 6.50 1.30 -2 2 -8 7.50 0.90 -2 2 -8 5.60 1.10 -2 2 -8 4.70 1.10 -2 -2 8 4.30 0.90 2 2 8 6.00 1.10 -2 -2 8 6.50 1.30 -2 -2 8 6.00 1.00 2 -2 -8 5.10 0.90 2 2 8 7.20 1.00 -2 -2 8 6.70 1.00 -3 2 8 94.29 3.20 3 -2 8 88.39 2.90 3 2 -8 89.99 3.20 3 2 -8 91.89 2.00 -3 -2 -8 93.89 2.90 3 2 -8 91.89 3.20 3 2 -8 96.29 3.10 3 -2 8 87.19 2.90 -3 2 8 86.59 3.30 -3 -2 -8 94.69 3.00 -3 2 8 91.39 2.10 -3 -2 -8 90.59 2.80 3 2 -8 93.39 2.90 3 2 -8 94.39 3.60 -3 2 8 88.19 2.30 -3 -2 -8 92.89 3.60 -3 2 8 93.49 3.00 3 -2 8 91.79 2.90 -3 -2 -8 94.19 2.90 3 -2 8 92.19 2.80 -3 2 8 92.49 2.80 -3 -2 -8 89.89 2.90 -3 2 8 90.79 3.50 3 2 -8 94.59 2.90 -3 -2 -8 94.49 3.60 -3 2 -8 92.59 2.90 3 2 8 91.89 2.80 3 2 8 90.89 2.50 -3 -2 8 93.49 3.00 -3 -2 8 88.49 3.00 -3 -2 8 87.89 3.40 3 2 8 91.09 3.30 3 -2 -8 94.09 2.80 3 2 8 89.69 3.20 3 -2 -8 96.89 3.00 -3 2 -8 90.89 3.30 -3 2 -8 91.69 2.70 -3 -2 8 94.09 3.00 3 -2 -8 93.89 2.90 -3 -2 8 85.69 2.90 3 -2 -8 92.79 3.10 3 2 8 90.29 3.40 -3 2 -8 95.69 2.40 3 -2 -8 90.99 2.80 -3 2 -8 92.79 3.00 3 2 8 93.39 2.60 3 -2 -8 91.79 2.50 -3 2 -8 94.99 3.00 -4 -2 -8 200.28 5.50 4 2 -8 208.48 4.90 4 2 -8 195.78 4.10 -4 -2 -8 209.48 5.00 -4 2 8 198.38 5.50 -4 2 8 202.78 4.80 -4 2 8 199.68 3.80 -4 2 8 206.48 5.30 4 -2 8 201.68 5.00 4 2 -8 204.38 5.30 4 2 -8 202.18 5.30 4 2 -8 203.08 5.00 -4 -2 -8 205.18 5.60 4 -2 8 204.98 5.00 -4 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3.00 7 2 8 56.19 3.00 7 2 8 58.69 1.50 7 -2 -8 56.19 2.90 7 -2 -8 60.99 2.90 -7 -2 8 54.29 3.00 -7 2 -8 56.09 2.60 7 -2 -8 55.89 2.70 7 2 8 61.99 2.70 8 -2 8 18.00 2.00 -8 -2 -8 16.30 2.00 8 -2 8 14.90 1.10 8 2 -8 14.60 1.90 -8 -2 -8 11.30 1.70 -8 2 8 18.00 1.10 -8 -2 -8 18.10 2.00 -8 2 8 16.00 1.60 8 -2 8 16.20 1.80 -8 -2 -8 14.80 2.00 -8 2 8 16.70 1.70 -8 2 8 18.40 1.90 -8 2 8 15.90 2.00 -8 2 8 16.20 1.40 -8 -2 -8 11.80 1.90 8 2 -8 14.10 1.90 -8 2 8 17.80 2.10 -8 -2 -8 17.20 2.20 -8 2 -8 16.30 1.10 8 2 8 14.40 1.70 -8 2 -8 11.80 1.80 -8 -2 8 16.90 2.10 8 2 8 17.00 1.80 8 -2 -8 17.20 1.50 -8 -2 8 14.20 1.90 8 2 8 18.50 2.10 -8 -2 8 14.60 1.80 8 -2 -8 18.30 1.50 8 -2 -8 13.20 1.80 8 2 8 13.50 1.90 -8 2 -8 16.50 1.10 -8 2 -8 18.70 2.20 -8 2 -8 13.90 1.60 8 -2 -8 16.00 1.90 -8 -2 8 13.60 1.70 -9 2 8 17.80 2.10 -9 -2 -8 16.80 2.20 9 2 -8 21.20 2.30 -9 2 8 16.90 1.90 -9 2 8 18.20 2.10 -9 -2 -8 21.70 2.40 -9 -2 -8 15.60 2.00 9 -2 8 15.30 1.90 -9 -2 -8 17.40 2.20 -9 2 8 19.30 2.10 9 -2 8 23.70 2.40 -9 -2 -8 19.10 2.40 -9 2 8 17.30 1.80 9 2 -8 14.80 2.00 9 2 -8 17.60 2.20 -9 -2 -8 19.00 2.20 -9 -2 8 15.90 2.10 9 -2 -8 16.40 2.00 -9 2 -8 15.90 2.10 9 2 8 22.30 2.10 9 -2 -8 20.60 2.30 -9 -2 8 16.70 1.40 -9 -2 8 16.20 2.00 -9 2 -8 16.50 1.90 -9 2 -8 20.60 2.30 -9 -2 8 17.20 2.40 9 2 8 13.60 2.00 9 2 8 20.10 2.00 -9 -2 8 22.20 2.40 9 2 8 22.40 2.30 9 -2 -8 19.50 2.00 9 -2 -8 20.10 1.50 10 -2 8 82.89 3.90 10 2 -8 72.89 3.80 10 2 -8 76.89 4.00 -10 -2 -8 86.09 4.40 -10 2 8 79.49 3.80 -10 2 8 75.09 3.90 -10 2 8 78.39 3.50 10 -2 8 72.99 3.90 -10 2 8 76.59 3.70 -10 -2 -8 79.29 4.10 -10 -2 -8 72.79 4.00 -10 -2 -8 82.29 4.10 10 2 -8 79.99 3.90 -10 2 8 69.59 3.70 -10 -2 -8 80.49 4.10 -10 -2 -8 77.99 4.20 -10 -2 8 75.59 4.30 -10 -2 8 70.09 3.80 10 2 8 77.29 3.80 -10 -2 8 76.89 3.90 -10 2 -8 76.99 3.60 -10 2 -8 81.89 4.10 -10 2 -8 78.59 3.90 10 2 8 75.79 4.10 10 -2 -8 75.49 4.00 10 2 8 72.09 3.50 10 -2 -8 75.59 3.90 -10 -2 8 87.09 4.10 10 2 8 77.39 3.50 11 -2 8 99.39 4.60 -11 -2 -8 93.49 5.00 -11 -2 -8 105.19 4.80 11 2 -8 102.69 4.60 11 2 -8 99.89 4.60 -11 2 8 98.39 4.40 -11 2 8 98.69 4.50 -11 2 8 94.19 3.90 -11 -2 -8 96.29 4.80 -11 2 8 102.19 4.50 -11 -2 -8 97.59 4.70 -11 2 8 98.69 4.30 11 2 -8 97.19 4.50 -11 -2 -8 96.39 4.70 11 -2 8 95.69 4.60 -11 -2 -8 82.69 4.30 -11 -2 8 97.79 4.60 11 2 8 93.79 4.10 -11 -2 8 97.39 4.60 -11 2 -8 100.19 4.20 11 -2 -8 94.69 4.60 -11 -2 8 107.39 4.70 11 2 8 94.99 4.40 11 2 8 94.29 4.10 -11 -2 8 93.09 4.70 -11 2 -8 101.29 4.70 -11 2 -8 96.99 4.50 11 2 8 100.19 4.80 11 -2 -8 105.49 4.60 12 2 -8 52.99 3.70 -12 -2 -8 59.99 4.30 -12 -2 -8 51.39 4.00 -12 2 8 52.79 3.70 -12 -2 -8 49.70 4.20 -12 2 8 53.99 3.30 -12 2 8 55.39 3.60 -12 -2 -8 52.99 3.70 12 2 -8 52.79 3.60 12 -2 8 53.99 3.70 12 2 -8 53.59 3.60 12 -2 8 57.59 4.00 -12 -2 -8 53.39 4.00 -12 -2 -8 54.39 3.80 -12 2 8 49.80 3.50 -12 -2 8 51.19 3.80 12 -2 -8 51.69 3.80 -12 2 -8 55.19 3.80 12 -2 -8 52.59 4.00 -12 -2 8 49.00 4.20 -12 -2 8 50.59 3.80 -12 2 -8 53.99 4.00 12 2 8 50.69 3.50 12 2 8 49.10 3.60 12 2 8 53.49 3.40 -12 -2 8 56.69 4.00 12 2 8 51.39 3.30 -12 2 -8 52.59 3.50 -13 2 8 8.40 1.90 13 2 -8 11.30 2.30 -13 -2 -8 6.30 2.30 13 2 -8 7.30 2.00 -13 2 8 8.50 2.00 -13 -2 -8 9.00 2.40 -13 2 8 7.70 2.00 13 2 -8 9.60 2.20 -13 -2 -8 6.10 2.20 13 -2 8 4.40 2.00 -13 -2 -8 6.50 2.30 -13 -2 -8 8.30 2.40 -13 -2 -8 5.60 2.20 13 -2 8 8.00 2.10 13 2 8 8.40 2.10 13 2 8 10.00 1.90 -13 2 -8 1.30 1.90 -13 -2 8 11.10 2.50 -13 2 -8 5.70 1.90 13 -2 -8 5.80 2.10 -13 -2 8 9.90 2.10 -13 -2 8 3.20 2.00 -13 2 -8 10.30 2.50 13 2 8 5.70 2.00 13 2 8 7.10 1.90 13 -2 -8 7.90 2.30 -13 -2 8 5.60 2.20 -14 -2 -8 19.60 2.90 14 2 -8 17.70 2.70 14 -2 8 18.80 2.80 -14 -2 -8 13.30 2.90 -14 2 8 21.00 2.60 -14 -2 -8 22.00 3.00 -14 -2 -8 24.80 3.20 14 2 -8 25.30 3.00 14 2 -8 27.40 3.10 -14 -2 -8 22.70 3.30 -14 2 8 20.30 2.70 -14 2 8 21.30 2.60 14 -2 8 21.30 2.90 -14 2 -8 25.40 5.20 -14 2 -8 16.90 2.80 14 2 8 20.70 2.80 14 -2 -8 25.80 3.30 -14 -2 8 18.80 3.00 -14 2 -8 12.60 2.40 14 2 8 23.90 3.20 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-3 8 16.20 1.30 1 3 8 16.30 1.50 -1 3 -8 18.70 1.20 1 3 8 21.50 2.10 1 -3 -8 15.20 1.20 1 3 8 21.10 2.00 1 -3 -8 14.50 1.10 -1 3 -8 16.50 1.50 2 3 -8 39.00 1.50 -2 -3 -8 35.70 2.00 2 -3 8 36.50 2.10 2 3 -8 37.20 2.00 -2 3 8 38.30 2.30 -2 -3 -8 37.30 1.70 -2 -3 -8 39.60 2.80 -2 3 8 34.50 2.40 -2 -3 -8 39.20 1.70 -2 -3 -8 42.30 2.80 2 3 -8 36.00 1.20 -2 3 8 34.70 2.70 -2 3 8 39.50 2.50 2 3 -8 37.00 1.20 2 3 -8 43.80 2.70 2 3 -8 37.50 2.40 2 -3 8 38.50 1.90 2 -3 8 40.90 1.90 -2 -3 -8 34.90 1.60 -2 3 8 37.40 1.80 2 -3 8 37.80 1.90 -2 -3 -8 40.50 1.80 2 -3 -8 41.20 2.30 -2 3 -8 39.90 1.50 2 -3 -8 40.90 1.60 2 3 8 41.00 2.60 -2 3 -8 37.40 2.00 2 3 8 37.60 2.00 -2 -3 8 39.20 2.60 2 3 8 36.70 2.40 -2 -3 8 36.60 1.90 -2 -3 8 37.20 1.90 -2 -3 8 41.10 1.90 2 3 8 38.30 2.50 -2 3 -8 40.10 2.60 -2 3 -8 39.80 2.00 2 -3 -8 39.70 1.80 2 -3 -8 38.00 1.70 2 3 8 39.90 2.00 2 -3 -8 37.80 1.70 2 -3 -8 39.20 2.30 -2 -3 8 38.70 1.90 3 -3 8 139.39 3.80 -3 -3 -8 141.59 3.70 -3 3 8 140.99 4.80 3 3 -8 136.29 3.20 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2.10 4 -3 8 40.00 2.10 -4 -3 -8 38.00 2.80 4 3 -8 38.00 2.60 -4 -3 -8 36.10 2.30 4 -3 8 36.90 2.00 -4 3 8 37.70 1.90 -4 3 8 40.40 2.70 -4 3 8 33.10 2.10 4 3 -8 36.90 2.70 -4 -3 -8 38.20 2.90 4 -3 -8 38.00 2.20 4 -3 -8 38.40 1.90 -4 3 -8 37.60 2.20 4 3 8 38.30 2.70 4 -3 -8 34.80 1.90 4 -3 -8 39.50 2.00 -4 3 -8 39.30 1.70 4 -3 -8 42.00 2.00 -4 -3 8 34.80 2.10 4 3 8 41.90 2.80 -4 -3 8 36.40 2.10 4 -3 -8 40.80 2.10 -4 -3 8 40.20 2.10 -4 3 -8 38.70 1.40 -4 -3 8 37.80 2.20 4 3 8 39.50 2.50 4 3 8 38.70 1.80 4 3 8 35.70 2.60 4 -3 -8 34.50 2.20 -4 -3 8 37.60 2.50 -4 3 -8 37.30 2.60 5 -3 8 282.47 6.60 5 3 -8 270.27 7.20 -5 -3 -8 287.77 6.50 -5 3 8 270.47 5.70 5 3 -8 281.57 7.20 5 3 -8 269.57 5.80 -5 -3 -8 290.67 6.90 5 3 -8 289.07 6.90 -5 3 8 269.27 7.10 5 -3 8 278.07 6.00 -5 -3 -8 272.57 7.50 -5 -3 -8 274.67 6.40 -5 3 8 272.67 6.30 -5 -3 -8 270.57 6.50 5 3 -8 280.67 6.00 -5 3 8 281.37 6.80 -5 3 8 270.07 7.50 -5 3 8 275.67 7.50 5 -3 8 273.47 6.50 -5 -3 -8 272.17 7.50 5 -3 8 274.07 6.50 -5 -3 -8 281.47 6.40 -5 -3 8 267.57 7.40 5 -3 -8 271.47 6.30 5 3 8 273.27 6.90 5 -3 -8 286.07 6.40 5 3 8 270.37 7.50 5 3 8 284.57 7.30 -5 -3 8 268.07 6.60 5 -3 -8 273.27 6.20 -5 3 -8 271.17 5.40 5 -3 -8 278.37 6.30 5 3 8 276.47 5.20 -5 3 -8 271.57 6.40 5 3 8 264.87 7.20 5 3 8 276.27 5.70 -5 -3 8 272.27 6.50 -5 -3 8 288.77 6.70 -5 -3 8 269.37 6.50 5 -3 -8 275.27 6.30 -5 3 -8 274.67 7.20 -5 3 -8 276.87 5.60 5 -3 -8 280.47 6.30 6 3 -8 111.99 3.20 -6 3 8 108.79 3.40 -6 3 8 106.19 4.50 6 3 -8 107.89 4.30 -6 -3 -8 115.09 4.20 6 -3 8 111.19 3.80 -6 -3 -8 105.69 3.70 -6 -3 -8 107.09 3.70 6 3 -8 98.79 3.80 6 -3 8 108.99 3.80 -6 -3 -8 100.59 3.70 -6 -3 -8 113.59 5.10 6 3 -8 109.59 3.30 6 -3 8 103.79 3.00 -6 -3 -8 107.79 4.60 -6 -3 -8 110.89 4.60 -6 3 8 108.59 4.30 -6 3 8 108.59 2.80 6 3 -8 104.69 4.20 6 -3 -8 108.89 3.40 6 -3 -8 113.09 3.60 6 3 8 109.79 4.20 6 3 8 109.59 4.50 6 3 8 108.99 4.30 6 -3 -8 108.79 3.70 -6 3 -8 105.29 3.00 6 -3 -8 106.79 3.40 -6 3 -8 108.19 3.80 6 3 8 111.69 4.00 -6 -3 8 110.79 3.80 6 -3 -8 111.09 3.60 -6 3 -8 102.79 4.10 6 3 8 110.29 2.80 -6 -3 8 100.29 3.80 -6 -3 8 108.89 3.90 6 3 8 107.09 2.70 -6 -3 8 108.29 4.50 7 3 -8 99.29 3.40 -7 -3 -8 94.49 4.10 7 3 -8 94.99 3.10 -7 -3 -8 91.69 4.50 -7 -3 -8 93.29 3.70 -7 -3 -8 94.39 4.40 7 3 -8 91.49 4.20 -7 3 8 102.49 4.30 -7 -3 -8 99.79 3.80 7 3 -8 91.39 3.90 -7 -3 -8 95.09 3.80 7 3 -8 98.29 4.20 -7 3 8 89.79 4.30 7 -3 8 98.29 3.80 7 -3 8 97.69 3.70 -7 -3 8 97.59 3.80 -7 3 -8 95.69 3.00 7 3 8 91.49 3.70 7 -3 -8 95.59 3.00 7 -3 -8 94.79 3.00 7 -3 -8 91.99 3.60 -7 -3 8 91.59 4.20 -7 3 -8 98.99 3.90 -7 -3 8 95.39 3.80 7 3 8 88.19 4.00 -7 -3 8 94.39 3.80 7 3 8 90.69 4.00 -7 3 -8 96.79 4.00 7 -3 -8 97.29 3.60 7 3 8 93.39 2.90 7 3 8 100.79 4.40 8 -3 8 110.59 4.20 -8 3 8 113.19 4.80 -8 -3 -8 111.89 4.30 8 3 -8 113.09 3.80 -8 -3 -8 96.29 4.80 -8 -3 -8 110.29 4.60 8 3 -8 112.39 4.70 8 3 -8 107.19 4.30 8 3 -8 109.49 3.60 8 -3 8 103.09 4.10 8 3 -8 112.79 4.60 -8 -3 -8 112.89 4.40 -8 -3 -8 106.29 4.80 -8 -3 -8 103.39 4.20 -8 3 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-28 -0.20 2.30 -2 -2 -28 0.40 2.30 2 2 -28 -0.10 2.40 -2 2 28 -0.20 1.90 -2 -2 -28 -1.40 2.70 2 2 -28 3.70 2.20 2 2 -28 0.40 2.30 2 -2 28 1.20 1.60 -2 -2 -28 1.70 2.20 -2 2 28 0.90 1.50 2 2 28 2.20 1.60 -2 -2 28 -0.30 1.70 2 2 28 0.00 2.00 -2 2 -28 -0.60 1.90 -2 2 -28 1.40 2.10 -2 2 -28 -0.40 2.30 2 2 28 -1.60 1.90 2 2 28 1.20 1.50 -2 2 -28 0.30 2.20 2 -2 -28 4.30 2.80 2 -2 -28 -0.50 2.00 -2 -2 28 -0.10 1.70 2 -2 -28 3.00 2.10 -3 2 28 12.90 2.20 3 2 -28 10.80 2.90 3 2 -28 13.40 2.70 -3 2 28 12.10 2.60 -3 2 28 11.00 2.40 -3 -2 -28 12.90 2.90 -3 2 28 13.10 2.30 -3 -2 -28 11.00 2.80 -3 -2 -28 9.40 3.10 3 -2 28 14.10 2.60 3 -2 28 11.90 2.40 -3 -2 -28 11.70 2.90 3 -2 -28 12.00 3.10 -3 -2 28 12.00 2.60 3 -2 -28 12.80 2.80 -3 2 -28 13.30 3.00 -3 2 -28 15.10 2.70 3 2 28 12.70 2.90 -3 2 -28 15.00 2.90 3 2 28 13.70 2.30 3 -2 -28 14.30 2.90 -3 2 -28 6.20 2.40 3 2 28 12.70 2.50 3 2 28 12.10 2.40 -3 -2 28 14.20 2.70 -4 2 28 69.49 4.80 -4 -2 -28 62.69 5.00 -4 -2 -28 58.99 5.10 4 2 -28 70.49 5.20 4 -2 28 75.89 4.80 4 -2 28 64.39 4.50 4 2 -28 64.99 4.50 -4 2 28 72.19 4.30 -4 -2 -28 66.89 4.90 -4 -2 -28 67.89 5.00 -4 2 28 67.99 4.00 -4 2 28 67.49 4.70 4 2 28 68.99 3.90 4 2 28 68.39 4.50 -4 2 -28 67.29 5.20 4 2 28 69.79 4.20 -4 2 -28 79.79 4.70 -4 2 -28 63.89 4.60 4 -2 -28 71.09 5.10 4 2 28 59.39 4.60 -4 -2 28 73.79 4.70 4 2 28 68.69 4.00 -4 2 -28 63.69 4.50 -4 -2 28 71.29 4.60 4 -2 -28 72.29 5.30 4 -2 -28 49.00 4.20 5 2 -28 4.30 2.80 -5 2 28 8.50 2.60 -5 -2 -28 5.00 2.50 -5 -2 -28 0.30 2.90 -5 2 28 4.00 1.70 -5 -2 -28 6.10 2.60 -5 2 28 3.40 1.80 -5 -2 -28 8.20 2.70 5 -2 28 3.40 2.10 -5 2 28 3.50 2.10 5 2 -28 9.40 2.70 5 2 28 4.50 2.10 -5 2 -28 5.90 2.60 5 -2 -28 2.50 2.40 -5 -2 28 3.90 2.00 -5 2 -28 3.90 2.30 5 -2 -28 3.80 2.60 5 2 28 5.50 1.90 5 -2 -28 4.40 2.50 5 2 28 3.30 1.90 -5 2 -28 5.20 2.30 -5 -2 28 6.90 2.40 5 2 28 4.50 2.50 -5 2 -28 6.50 2.40 -6 2 28 13.60 2.30 -6 2 28 11.10 2.90 -6 -2 -28 17.30 3.10 -6 -2 -28 14.90 3.10 -6 2 28 19.50 3.00 -6 -2 -28 16.00 3.20 -6 -2 -28 11.20 3.60 6 -2 28 19.10 3.00 -6 2 28 13.70 2.50 6 2 -28 22.70 3.80 6 2 -28 17.60 3.00 6 -2 -28 16.40 3.10 -6 -2 28 15.40 3.00 -6 2 -28 9.00 2.60 6 -2 -28 13.70 3.00 -6 2 -28 12.30 3.10 6 -2 -28 18.20 3.30 -6 -2 28 10.50 2.60 -6 2 -28 16.80 2.90 6 2 28 11.50 2.80 -6 2 -28 11.10 2.70 6 2 28 15.80 2.50 6 2 28 13.80 2.70 7 2 -28 8.00 2.70 -7 -2 -28 5.60 3.30 -7 2 28 6.10 1.90 -7 -2 -28 9.40 2.90 7 2 -28 4.10 2.90 7 -2 28 5.60 2.30 -7 -2 -28 7.10 2.90 7 2 -28 8.00 2.50 -7 2 28 5.90 2.10 -7 2 28 5.50 2.50 -7 2 -28 4.90 2.30 -7 2 -28 7.10 2.90 7 2 28 1.80 2.30 7 -2 -28 6.20 2.80 7 -2 -28 5.50 2.50 -7 -2 28 6.10 2.10 -7 2 -28 7.10 2.40 7 2 28 5.80 2.00 -7 2 -28 3.70 2.40 7 2 28 4.90 2.10 -7 -2 28 3.30 2.20 7 -2 -28 1.10 2.50 -8 2 28 75.99 5.20 -8 -2 -28 79.99 5.90 8 -2 28 84.59 5.40 8 2 -28 83.99 5.40 8 2 -28 98.79 6.30 -8 -2 -28 83.59 6.30 8 2 -28 83.49 5.50 -8 2 28 76.99 5.00 -8 -2 -28 77.79 5.80 -8 2 28 85.19 5.50 -8 2 -28 85.29 5.40 -8 2 -28 81.09 6.80 8 2 28 81.29 5.80 -8 -2 28 77.49 5.40 8 -2 -28 66.69 5.60 -8 -2 28 73.79 5.20 -8 2 -28 88.79 5.50 8 -2 -28 76.39 5.50 8 2 28 82.49 5.30 8 2 28 79.99 4.60 8 -2 -28 87.49 5.40 9 2 -28 17.20 3.80 -9 -2 -28 20.50 4.20 9 2 -28 13.70 3.00 -9 -2 -28 19.30 3.70 -9 -2 -28 15.50 3.60 -9 2 28 17.20 3.30 -9 2 28 20.20 3.10 9 -2 28 19.80 3.40 9 2 -28 16.90 3.30 -9 2 -28 18.70 3.30 9 2 28 16.00 3.00 -9 -2 28 22.30 3.60 -9 -2 28 18.10 3.40 9 2 28 18.00 2.70 9 -2 -28 17.80 3.50 9 -2 -28 17.10 3.40 9 2 28 20.70 3.70 -9 2 -28 16.20 3.20 0 -3 28 0.90 1.50 0 -3 28 0.40 1.70 0 3 -28 2.50 2.00 0 -3 -28 1.60 2.20 0 3 28 0.30 1.90 0 3 28 1.20 2.30 0 -3 -28 0.90 3.00 0 3 -28 -0.40 1.80 0 3 28 2.70 1.80 0 -3 -28 -0.30 2.10 0 -3 -28 -1.90 2.10 0 3 -28 -0.30 2.20 0 3 -28 3.00 2.40 -1 -3 -28 1.30 2.20 -1 -3 -28 5.40 3.30 1 -3 28 7.70 2.20 1 3 -28 7.60 2.60 1 3 -28 3.90 2.20 1 -3 28 4.40 2.00 -1 3 28 6.20 2.50 1 3 -28 4.60 2.10 -1 3 28 3.80 2.20 -1 -3 -28 3.30 2.50 1 3 -28 2.10 2.40 -1 3 28 2.30 1.80 -1 -3 -28 -0.10 2.20 1 -3 28 5.70 2.20 -1 3 -28 6.20 2.60 1 3 28 3.70 2.60 1 3 28 4.50 1.90 1 -3 -28 2.10 3.10 -1 3 -28 5.10 2.20 -1 -3 28 5.70 2.10 -1 3 -28 5.20 2.00 1 3 28 3.90 2.10 1 -3 -28 1.10 2.20 -1 -3 28 4.30 1.90 -1 3 -28 5.20 2.50 1 -3 -28 6.50 2.40 -1 -3 28 5.30 2.10 -2 3 28 4.30 2.00 -2 3 28 -0.20 2.00 -2 3 28 3.10 2.50 2 3 -28 7.20 2.80 -2 -3 -28 1.00 3.00 2 3 -28 2.00 2.00 -2 -3 -28 2.00 2.30 -2 -3 -28 0.60 2.40 2 -3 28 -0.70 1.60 2 -3 28 5.30 2.10 -2 -3 -28 4.40 2.40 2 -3 28 2.60 2.00 2 3 -28 4.10 2.10 2 3 -28 1.10 2.20 -2 3 -28 5.10 2.50 -2 -3 28 3.90 1.90 2 -3 -28 1.30 3.00 2 3 28 2.00 1.90 -2 -3 28 1.30 1.90 -2 3 -28 0.30 2.10 -2 3 -28 1.50 2.00 2 -3 -28 1.60 2.20 2 -3 -28 3.40 2.10 2 3 28 1.80 2.30 -2 -3 28 2.20 2.10 2 3 28 1.30 1.60 3 3 -28 65.89 4.50 -3 3 28 68.89 4.90 -3 3 28 75.09 4.80 3 -3 28 72.09 4.70 3 3 -28 79.29 4.80 -3 -3 -28 78.99 6.10 -3 -3 -28 82.09 5.30 3 -3 28 75.59 5.00 -3 3 28 69.89 5.30 3 3 -28 84.99 5.80 3 3 -28 75.49 4.70 -3 -3 -28 71.89 5.10 -3 -3 -28 67.09 5.00 3 -3 28 76.89 4.70 3 3 28 70.69 5.40 3 -3 -28 77.99 5.00 -3 -3 28 70.59 4.70 -3 3 -28 75.99 4.70 -3 -3 28 76.39 4.80 3 3 28 64.49 4.50 3 3 28 75.69 4.60 3 3 28 71.69 4.50 -3 3 -28 77.09 5.20 3 -3 -28 77.69 5.60 3 -3 -28 74.99 5.20 -3 3 -28 78.79 5.10 -4 -3 -28 25.30 3.60 4 3 -28 22.80 3.20 -4 -3 -28 25.80 3.50 -4 3 28 23.50 3.50 -4 -3 -28 24.40 4.10 -4 -3 -28 24.60 3.50 -4 3 28 23.50 3.10 4 3 -28 30.30 3.50 4 3 -28 31.80 4.30 4 -3 28 23.60 3.20 4 -3 28 25.40 3.30 -4 3 28 27.00 3.50 4 3 -28 28.50 3.30 4 -3 28 27.60 3.80 4 3 28 26.00 3.60 -4 3 -28 24.10 3.10 4 3 28 23.10 2.90 4 -3 -28 24.90 4.00 -4 -3 28 28.10 3.50 -4 3 -28 25.10 3.50 -4 -3 28 22.90 3.30 4 3 28 27.50 3.30 4 -3 -28 25.50 3.30 4 3 28 28.50 3.90 -4 3 -28 21.40 3.40 4 -3 -28 24.60 3.50 5 -3 28 5.90 2.20 5 3 -28 9.30 3.20 -5 -3 -28 6.10 2.70 -5 3 28 9.20 2.60 5 -3 28 6.70 2.40 5 3 -28 4.50 2.40 -5 3 28 5.00 2.10 -5 -3 -28 5.20 3.60 5 3 -28 4.40 2.40 -5 3 28 4.90 2.30 -5 -3 -28 5.70 2.50 -5 -3 -28 7.60 2.80 5 -3 -28 7.90 2.60 -5 3 -28 7.20 2.40 -5 -3 28 5.50 2.20 5 3 28 6.50 2.20 5 3 28 2.80 2.40 -5 3 -28 4.40 2.50 5 3 28 7.90 2.50 5 -3 -28 7.90 3.10 -5 3 -28 4.60 2.60 5 -3 -28 4.60 2.60 -5 -3 28 6.40 2.40 6 3 -28 1.60 2.10 -6 -3 -28 0.70 3.30 6 3 -28 3.50 3.00 6 -3 28 2.30 2.00 6 3 -28 -1.00 2.00 -6 -3 -28 2.30 2.40 6 -3 28 2.60 2.10 -6 3 28 0.80 2.40 -6 3 28 1.50 2.00 -6 3 28 1.60 2.10 -6 -3 -28 4.60 2.50 -6 -3 -28 -2.40 2.50 6 -3 -28 2.20 2.90 -6 3 -28 -0.20 2.20 -6 -3 28 0.70 2.10 6 -3 -28 1.60 2.40 6 3 28 2.40 2.40 -6 -3 28 -0.20 1.80 -6 3 -28 5.60 2.70 6 3 28 -1.60 1.60 6 3 28 3.10 2.00 6 -3 -28 -2.50 2.00 -7 -3 -28 10.50 3.10 7 3 -28 14.40 3.70 7 3 -28 9.10 2.80 -7 -3 -28 8.20 3.70 -7 3 28 10.10 2.70 -7 3 28 13.40 3.10 -7 -3 -28 9.50 2.90 7 3 -28 9.60 2.80 7 -3 28 11.70 2.80 -7 3 28 13.90 3.10 -7 -3 -28 10.60 3.20 -7 3 -28 13.40 3.00 7 -3 -28 9.60 3.00 -7 3 -28 9.00 2.70 7 -3 -28 10.00 2.90 7 3 28 14.00 2.70 -7 -3 28 11.50 2.80 7 3 28 9.60 2.70 7 3 28 11.10 3.00 -7 -3 28 11.10 3.00 7 -3 -28 10.10 2.90 8 3 -28 82.09 5.50 -8 -3 -28 84.29 5.80 -8 -3 -28 79.29 5.90 -8 -3 -28 92.29 6.20 -8 3 28 88.89 6.00 -8 3 28 77.89 5.60 8 3 -28 100.39 6.80 -8 -3 -28 79.49 6.80 8 3 -28 77.99 5.20 8 -3 28 79.09 5.50 8 3 28 78.09 5.90 -8 3 -28 65.39 7.10 8 -3 -28 93.39 5.80 8 -3 -28 81.99 5.70 8 3 28 82.59 4.90 8 3 28 84.09 5.70 -8 -3 28 86.49 5.60 -8 -3 28 83.39 5.40 -8 3 -28 89.99 5.90 0 -4 28 1.10 1.90 0 4 -28 6.30 2.90 0 -4 28 2.50 1.80 0 -4 -28 5.20 3.70 0 4 -28 2.00 2.70 0 4 28 4.90 2.30 0 4 28 0.00 2.00 0 4 28 2.00 2.60 0 -4 -28 1.20 2.20 1 -4 28 8.60 2.50 -1 4 28 9.60 3.00 -1 -4 -28 3.50 3.60 1 4 -28 7.10 2.80 -1 -4 -28 8.60 2.60 1 4 -28 10.60 2.50 1 -4 28 10.30 2.40 1 4 -28 9.90 3.20 -1 4 28 9.40 2.70 1 -4 28 7.90 2.40 -1 -4 -28 6.00 2.50 -1 4 28 10.10 2.60 1 4 28 8.50 2.50 -1 -4 28 8.90 2.30 -1 -4 28 10.00 2.40 -1 4 -28 13.50 3.30 1 4 28 2.70 2.50 1 4 28 6.00 2.60 1 -4 -28 7.00 3.70 -1 4 -28 8.10 2.90 1 -4 -28 6.40 2.50 -1 -4 28 10.40 2.50 2 -4 28 20.30 3.00 2 4 -28 23.70 3.30 -2 -4 -28 19.60 3.20 -2 4 28 19.10 3.30 -2 4 28 23.70 3.70 2 4 -28 13.20 3.20 2 -4 28 21.90 3.20 2 -4 28 21.90 3.10 -2 4 28 18.70 3.20 -2 -4 -28 22.70 4.40 -2 -4 -28 16.60 3.00 2 4 -28 20.60 3.90 2 -4 -28 18.60 4.10 2 -4 -28 20.60 3.10 -2 -4 28 22.80 3.30 -2 -4 28 24.20 3.40 -2 4 -28 26.10 3.70 2 4 28 13.40 3.00 -2 -4 28 20.00 3.20 -2 4 -28 18.00 3.60 2 4 28 16.50 3.40 2 4 28 21.80 3.20 2 4 28 22.10 3.10 3 -4 28 29.20 3.40 -3 -4 -28 20.00 4.40 -3 -4 -28 19.50 4.30 3 -4 28 28.70 3.50 -3 4 28 24.80 3.60 3 4 -28 26.70 3.80 -3 -4 -28 24.60 3.30 -3 4 28 22.10 3.40 3 -4 28 20.20 3.20 3 4 -28 26.30 3.50 3 4 -28 24.70 4.20 -3 4 28 36.90 4.40 -3 -4 -28 20.40 3.20 -3 -4 28 27.50 3.50 3 4 28 26.60 3.90 -3 -4 28 29.80 3.50 3 4 28 35.10 3.90 3 4 28 25.50 3.50 -3 4 -28 32.00 4.10 3 -4 -28 31.70 4.40 -3 4 -28 27.40 3.90 3 -4 -28 23.10 3.20 -3 -4 28 26.80 3.40 4 -4 28 4.20 2.20 4 -4 28 4.70 2.10 -4 4 28 3.40 2.10 -4 -4 -28 4.80 3.10 4 4 -28 5.60 2.40 -4 -4 -28 1.90 3.50 4 4 -28 5.30 2.90 4 4 -28 7.50 2.80 4 -4 28 4.40 2.20 -4 -4 -28 3.00 2.30 -4 -4 -28 6.60 2.60 -4 4 28 10.10 2.90 -4 4 28 5.90 2.60 4 4 28 7.10 2.50 -4 -4 28 4.90 2.20 4 4 28 3.60 2.70 -4 4 -28 7.50 4.40 4 4 28 2.90 2.20 -4 -4 28 2.70 2.00 -4 4 -28 10.10 3.20 4 -4 -28 4.70 3.20 4 -4 -28 9.50 2.70 -4 -4 28 4.70 2.30 0 0 29 1.30 1.70 0 0 -29 3.90 2.60 0 0 -29 5.90 2.50 0 0 -29 1.60 2.30 0 0 29 1.00 1.70 0 0 29 1.20 1.90 -1 0 -29 -0.90 2.40 1 0 -29 -2.00 2.00 -1 0 29 -1.20 1.70 1 0 29 -3.40 1.40 1 0 -29 -0.90 2.10 -1 0 -29 -2.70 2.00 -1 0 29 2.90 1.80 -1 0 -29 -1.50 2.10 1 0 29 3.60 1.90 1 0 -29 2.00 2.50 1 0 29 0.30 1.80 -1 0 29 -2.40 1.40 2 0 -29 58.89 4.90 -2 0 29 53.89 4.00 -2 0 -29 48.80 4.10 2 0 29 52.89 4.20 2 0 -29 52.19 4.40 -2 0 29 52.69 3.90 2 0 -29 46.80 4.40 -2 0 29 58.09 4.20 -2 0 -29 68.69 5.00 2 0 29 51.19 4.00 -2 0 -29 48.30 4.40 -2 0 -29 56.69 3.70 3 0 -29 1.80 2.40 -3 0 29 -1.30 1.50 -3 0 -29 0.10 2.30 -3 0 -29 -0.50 2.00 -3 0 -29 3.40 2.00 -3 0 29 -1.50 1.60 -3 0 -29 0.80 2.40 -3 0 29 1.30 1.60 3 0 29 0.30 1.60 3 0 29 0.60 1.70 3 0 29 0.00 1.90 3 0 -29 -4.60 2.00 4 0 29 4.80 2.30 4 0 -29 2.90 2.40 -4 0 -29 8.80 2.40 -4 0 29 3.70 2.10 4 0 -29 4.30 2.80 4 0 29 0.90 1.50 -4 0 -29 3.50 2.50 -4 0 29 0.40 1.80 4 0 29 0.40 1.70 -4 0 29 5.50 1.90 -4 0 -29 1.70 2.40 -4 0 -29 3.30 2.70 -5 0 -29 -0.90 2.00 5 0 29 1.40 1.80 -5 0 -29 -1.00 2.40 -5 0 29 0.10 2.20 5 0 29 0.70 2.20 -5 0 29 -0.70 1.40 5 0 -29 2.90 2.40 5 0 -29 0.40 2.20 -5 0 -29 -3.40 2.20 -5 0 29 0.60 1.80 -5 0 -29 0.50 2.50 -5 0 29 -3.70 1.50 -6 0 29 12.90 2.70 -6 0 -29 16.60 3.20 6 0 -29 20.40 3.40 6 0 29 14.80 3.10 6 0 -29 18.80 3.60 -6 0 -29 16.20 2.90 6 0 29 15.80 2.80 -6 0 29 13.40 2.70 -6 0 -29 11.50 3.10 -6 0 29 15.90 3.00 -6 0 -29 15.00 3.30 -7 0 29 -0.30 1.70 -7 0 29 2.20 2.40 7 0 29 -1.70 1.60 7 0 -29 -0.80 2.40 -7 0 29 -1.60 1.60 -7 0 -29 -2.90 2.40 7 0 29 -0.60 2.50 -7 0 -29 -0.80 2.50 7 0 -29 -0.40 2.40 -7 0 -29 2.60 2.70 -7 0 -29 -0.20 2.40 8 0 -29 6.90 3.00 -8 0 -29 4.00 2.80 8 0 -29 3.00 2.70 -8 0 29 7.20 2.60 8 0 29 8.20 2.40 -8 0 -29 2.40 2.70 8 0 29 5.80 2.00 -8 0 -29 8.80 3.00 -8 0 29 3.90 2.10 -8 0 -29 5.00 2.80 -8 0 29 1.30 2.20 -9 0 -29 -3.00 2.60 9 0 -29 1.00 2.50 -9 0 -29 -4.60 2.60 -9 0 29 2.20 2.30 -9 0 29 0.60 2.20 -9 0 -29 1.50 2.60 9 0 29 1.20 1.90 -9 0 -29 3.80 3.00 9 0 29 1.00 1.80 -9 0 29 3.70 2.30 9 0 -29 -6.50 2.30 -10 0 29 34.70 4.10 10 0 29 39.50 4.30 -10 0 -29 40.40 4.30 10 0 -29 30.20 4.10 -10 0 -29 25.00 4.10 -10 0 -29 35.20 4.40 -10 0 29 35.40 3.90 10 0 29 36.30 3.80 -10 0 29 37.50 3.90 10 0 -29 34.80 4.40 -10 0 -29 32.20 4.50 0 1 -29 30.70 3.60 0 -1 -29 28.20 3.40 0 1 29 34.70 3.70 0 1 29 29.10 3.10 0 -1 29 36.20 3.60 0 1 -29 34.50 3.10 0 -1 -29 34.30 4.30 0 1 29 38.70 3.70 0 -1 29 34.50 3.40 0 -1 29 28.40 3.50 0 1 -29 29.50 3.70 0 1 -29 27.20 3.50 0 -1 -29 28.40 3.50 1 -1 29 20.40 2.90 1 1 -29 13.40 2.90 -1 1 29 14.60 2.50 -1 1 29 19.70 2.90 1 1 -29 13.80 3.10 -1 -1 -29 18.50 3.60 1 1 -29 18.20 3.30 -1 -1 -29 21.50 3.20 -1 -1 -29 14.00 3.20 -1 1 29 17.50 2.90 -1 1 29 16.90 2.60 1 -1 29 15.70 2.70 1 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-32 10.40 3.40 -6 -1 -32 8.90 3.30 -6 1 -32 11.10 3.10 6 -1 -32 7.90 3.20 6 1 32 10.10 3.10 6 -1 -32 11.20 3.30 -6 -1 32 12.90 2.90 -6 1 -32 6.40 3.10 6 1 32 8.20 2.30 -6 1 -32 8.40 3.10 -6 -1 32 8.90 2.70 -6 1 -32 10.20 2.80 -7 -1 -32 19.00 3.60 -7 1 -32 23.00 3.50 0 2 -32 116.69 6.20 0 2 32 118.19 6.20 0 -2 32 119.39 6.10 0 2 -32 124.69 6.90 0 -2 -32 114.19 7.10 0 2 32 118.19 5.40 0 -2 32 122.29 6.40 0 2 32 116.39 6.70 0 -2 -32 129.49 6.70 0 2 -32 108.39 6.50 0 -2 -32 120.09 6.60 0 -2 32 116.09 6.10 1 -2 32 9.90 2.80 -1 2 32 8.60 2.30 -1 2 32 4.10 2.50 -1 -2 -32 8.40 3.00 -1 2 32 8.30 2.80 1 -2 32 7.40 2.70 1 -2 32 3.30 2.30 1 2 -32 11.10 3.30 1 2 -32 2.20 2.60 -1 -2 -32 8.50 3.60 -1 -2 -32 2.80 2.90 1 2 -32 10.00 3.20 1 2 32 4.10 2.50 -1 -2 32 0.90 2.10 1 -2 -32 6.80 3.00 1 -2 -32 7.80 3.50 -1 -2 32 6.70 2.50 1 -2 -32 4.40 2.80 1 2 32 3.80 2.40 -1 2 -32 8.70 3.00 -1 2 -32 1.60 2.70 -1 2 -32 9.00 2.80 1 2 32 7.20 2.10 1 2 32 5.30 2.00 -1 2 -32 5.50 2.90 2 -2 32 -1.70 2.20 2 2 -32 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4 2 32 0.80 2.30 -4 2 -32 0.50 3.00 -4 -2 32 2.50 2.40 4 2 32 4.00 2.00 4 -2 -32 4.50 3.00 4 2 32 9.40 2.40 -4 -2 32 1.50 2.30 4 -2 -32 8.00 3.40 -4 2 -32 2.80 2.60 -4 2 -32 7.90 2.70 -5 2 32 -2.00 2.00 -5 -2 -32 2.30 3.00 5 -2 32 -3.00 1.70 -5 -2 -32 0.60 3.40 5 2 -32 2.10 2.70 5 2 -32 2.20 3.00 5 -2 32 -1.70 1.90 -5 -2 -32 -3.50 2.60 -5 2 32 1.70 2.20 -5 -2 32 -0.50 2.10 -5 -2 32 0.60 2.20 -5 2 -32 2.10 2.50 -5 2 -32 0.00 4.30 5 2 32 4.90 2.80 5 2 32 2.40 2.10 5 2 32 0.70 1.80 5 -2 -32 3.10 2.80 5 -2 -32 3.60 2.90 -5 2 -32 3.00 2.60 -5 2 -32 -1.60 2.60 0 0 33 1.90 2.30 0 0 -33 -1.20 2.50 0 0 33 3.60 2.10 0 0 -33 -0.80 2.60 0 0 33 3.30 2.20 0 0 -33 5.50 2.90 -1 0 -33 -1.00 2.80 1 0 33 -2.00 1.70 1 0 -33 2.20 3.00 -1 0 33 -0.60 1.90 1 0 -33 -0.60 2.70 -1 0 -33 -0.20 2.60 1 0 -33 -5.20 2.30 1 0 33 -0.80 1.90 -1 0 33 -0.70 1.90 -1 0 -33 1.00 2.90 1 0 33 3.90 2.30 -1 0 33 0.20 1.80 2 0 -33 16.20 3.70 -2 0 33 15.60 2.90 2 0 33 12.90 3.00 -2 0 -33 8.40 3.30 -2 0 33 21.40 3.30 2 0 -33 18.20 3.90 2 0 -33 21.30 3.70 -2 0 -33 15.60 3.70 -2 0 33 17.30 3.00 2 0 33 12.80 2.70 -2 0 -33 13.50 3.30 2 0 33 21.30 3.40 -3 0 33 -1.20 1.90 3 0 -33 4.20 3.00 -3 0 -33 -1.00 2.60 3 0 33 -1.00 2.20 -3 0 33 -0.20 1.90 -3 0 33 1.80 2.00 3 0 33 -1.10 1.90 3 0 -33 2.80 2.80 -3 0 -33 -1.80 2.70 3 0 33 -0.30 2.00 -3 0 -33 2.60 2.90 -4 0 33 282.97 9.60 4 0 -33 290.17 10.50 -4 0 33 267.07 9.10 -4 0 -33 258.57 9.90 4 0 33 287.77 9.50 4 0 33 283.37 10.00 -4 0 -33 271.17 9.80 -4 0 -33 272.47 10.20 4 0 -33 257.07 9.50 -4 0 33 256.97 9.20 4 0 33 263.87 9.50 5 0 33 -1.30 1.80 -5 0 33 0.00 2.60 -5 0 33 -0.10 2.00 -5 0 -33 3.80 3.10 -5 0 -33 6.40 3.20 5 0 -33 2.60 2.90 5 0 33 -3.10 2.30 -5 0 -33 -3.90 2.50 5 0 33 2.80 2.30 5 0 -33 -0.20 2.70 -5 0 33 -0.60 2.00 6 0 33 11.50 3.30 6 0 33 13.30 3.00 -6 0 -33 3.90 3.00 -6 0 33 8.90 3.10 -6 0 -33 13.80 3.20 -6 0 -33 21.20 4.00 -6 0 -33 12.40 3.50 6 0 33 17.60 3.30 6 0 -33 16.20 3.50 -6 0 33 7.60 2.70 0 1 33 4.10 2.10 0 1 -33 5.90 3.00 0 1 -33 4.20 2.90 0 -1 -33 2.70 2.80 0 -1 33 4.30 2.40 0 1 -33 6.40 3.20 0 -1 33 7.90 2.60 0 -1 33 9.60 2.50 0 1 33 6.00 2.60 0 -1 -33 7.40 3.50 0 -1 -33 7.70 3.10 0 1 33 4.80 2.60 1 1 -33 6.50 3.00 -1 1 33 6.10 2.30 1 -1 33 7.60 2.50 1 1 -33 12.90 3.30 -1 -1 -33 9.60 2.90 1 -1 33 11.80 2.80 -1 1 33 3.10 2.30 -1 -1 -33 5.40 3.40 -1 -1 -33 7.60 3.20 -1 1 33 4.30 2.60 1 -1 33 13.40 2.80 1 1 -33 9.70 3.20 1 -1 -33 12.90 3.40 1 -1 -33 11.30 3.30 1 1 33 4.70 2.60 -1 1 -33 7.60 3.10 -1 1 -33 6.00 2.90 1 1 33 13.40 2.70 1 1 33 10.60 2.90 1 -1 -33 11.80 3.60 -1 -1 33 3.10 2.40 -1 -1 33 10.80 2.70 -1 -1 33 11.50 2.80 -1 1 -33 10.50 3.30 -2 1 33 5.30 2.40 2 -1 33 10.00 2.90 2 1 -33 8.50 3.00 2 1 -33 10.10 2.90 -2 -1 -33 12.10 3.50 -2 -1 -33 5.40 3.00 2 -1 33 12.30 3.00 2 -1 33 9.50 2.70 -2 1 33 6.20 2.30 -2 -1 -33 4.20 3.30 -2 1 33 4.10 2.50 2 1 -33 11.60 3.40 -2 -1 33 4.80 2.40 -2 1 -33 4.50 2.90 2 -1 -33 9.60 3.30 -2 1 -33 6.50 3.00 2 1 33 10.00 2.80 -2 -1 33 7.50 2.50 2 -1 -33 5.90 3.30 2 1 33 8.20 2.30 -2 1 -33 11.60 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-2 2 -33 4.00 2.90 -2 2 -33 1.50 2.40 2 -2 -33 1.40 3.30 -2 -2 33 -0.20 2.20 2 2 33 -0.40 2.10 3 -2 33 1.60 2.20 -3 -2 -33 4.70 3.30 3 2 -33 3.10 3.00 -3 -2 -33 -1.30 2.80 -3 2 33 0.70 2.30 -3 -2 -33 -0.10 2.70 -3 2 33 -2.60 2.20 3 -2 33 5.40 2.40 3 2 -33 -3.60 2.40 3 -2 -33 -1.50 3.20 3 2 33 -3.20 2.40 3 2 33 2.50 2.10 -3 2 -33 6.60 3.00 -3 -2 33 1.00 2.20 -3 -2 33 -1.60 2.10 3 2 33 -0.30 2.20 3 -2 -33 6.50 3.10 -3 2 -33 2.20 3.70 -3 2 -33 -0.70 2.60 -3 2 -33 8.60 2.80 0 0 -34 374.06 12.30 0 0 34 379.86 11.20 0 0 -34 369.16 12.10 0 0 34 360.96 11.40 0 0 -34 377.26 11.80 0 0 34 384.36 11.60 -1 0 34 -0.80 2.00 -1 0 -34 7.20 3.30 1 0 -34 2.70 3.00 -1 0 -34 -3.20 2.60 -1 0 -34 -1.00 3.00 -1 0 34 -3.00 1.80 1 0 34 1.00 2.30 -1 0 34 -2.00 1.80 1 0 34 2.10 2.20 1 0 34 0.80 2.10 1 0 -34 -3.70 2.50 1 0 -34 1.00 2.90 2 0 34 67.59 5.20 2 0 -34 58.69 5.20 2 0 -34 59.49 5.50 -2 0 34 66.19 5.10 -2 0 -34 69.09 5.60 -2 0 -34 79.49 6.10 -2 0 34 66.29 5.10 -2 0 34 77.89 5.30 2 0 34 59.19 4.70 2 0 34 64.49 5.40 -2 0 -34 54.29 5.30 -3 0 34 -1.70 2.00 -3 0 -34 -4.10 2.90 3 0 34 1.10 2.00 3 0 34 -1.50 2.00 3 0 -34 6.30 3.10 -3 0 34 0.60 2.10 -3 0 -34 -0.90 2.80 -3 0 -34 2.70 3.00 3 0 34 1.40 2.50 -3 0 34 -0.70 1.70 3 0 -34 2.80 2.90 4 0 -34 35.90 4.40 4 0 34 47.80 5.00 -4 0 -34 54.99 5.40 -4 0 -34 37.00 4.40 -4 0 34 54.59 5.00 -4 0 34 50.79 4.70 -4 0 34 40.70 4.50 -4 0 -34 35.20 4.60 4 0 34 45.40 4.60 4 0 -34 51.99 5.40 0 1 34 -0.20 2.20 0 1 -34 4.60 3.00 0 -1 -34 0.90 2.70 0 -1 -34 -2.60 3.00 0 1 34 -1.00 1.80 0 1 -34 -2.70 2.60 0 1 34 -0.90 2.50 0 -1 -34 -2.70 2.90 0 -1 34 2.10 2.30 0 -1 34 -1.70 2.00 0 1 -34 0.00 2.70 0 -1 34 0.10 2.20 1 -1 34 24.30 3.60 1 1 -34 28.00 4.10 -1 1 34 24.80 3.30 -1 1 34 21.00 3.50 -1 -1 -34 25.60 4.10 -1 -1 -34 23.30 4.40 -1 -1 -34 16.30 3.70 1 1 -34 24.80 4.30 -1 1 34 25.20 3.70 1 1 -34 24.70 3.90 1 -1 34 21.60 3.40 1 -1 34 22.20 3.50 -1 1 -34 22.10 3.80 -1 1 -34 18.20 3.60 -1 -1 34 29.10 3.70 -1 1 -34 25.50 3.90 1 1 34 26.00 3.70 -1 -1 34 23.50 3.40 1 1 34 21.10 3.10 1 -1 -34 23.00 3.90 1 -1 -34 24.70 4.40 1 1 34 20.20 3.40 -1 -1 34 18.80 3.30 1 -1 -34 24.10 3.90 2 1 -34 6.60 3.30 -2 1 34 0.80 2.70 2 -1 34 5.40 2.40 -2 1 34 6.80 2.30 -2 -1 -34 4.10 3.20 -2 -1 -34 14.30 4.00 -2 1 34 0.90 2.40 2 -1 34 5.40 2.60 2 -1 34 7.10 2.60 2 1 -34 3.10 2.90 -2 -1 -34 14.40 3.60 2 -1 -34 -0.70 2.70 -2 1 -34 2.10 2.90 2 -1 -34 18.50 4.00 -2 1 -34 10.20 3.20 -2 -1 34 3.50 2.40 -2 -1 34 6.50 2.70 -2 1 -34 9.90 3.20 2 1 34 9.60 3.00 2 1 34 7.60 2.40 -3 1 34 16.80 2.90 -3 -1 -34 11.50 3.40 -3 -1 -34 8.20 3.60 -3 -1 -34 15.40 3.80 -3 1 34 12.00 3.40 -3 1 34 13.40 3.10 3 -1 34 11.50 2.90 3 -1 34 8.60 3.00 3 1 -34 14.70 3.80 3 1 -34 5.90 3.00 3 1 34 9.50 2.60 -3 -1 34 13.00 3.10 -3 -1 34 10.00 2.70 -3 1 -34 8.30 3.30 -3 1 -34 15.50 3.40 3 -1 -34 10.50 3.20 3 -1 -34 14.00 3.60 -3 1 -34 6.20 3.30 3 1 34 11.20 3.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 43411 _olex2_exptl_crystal_mounting_method 'The crystal was mounted on a mylar loop oil' _olex2_submission_special_instructions 'No special instructions were received' loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 1.34163 2 -0.34163