#============================================================================= data_global loop_ _journal_name_full 'European Journal of Chemistry' _journal_coden_ASTM EJCUA9 _journal_volume 17 _journal_issue 3 _journal_year 2026 _journal_page_first 205 _journal_page_last 209 #============================================================================= data_i1188cucl2_auto _audit_creation_date 2025-01-07 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _shelx_SHELXL_version_number '2018/3' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety '2(C18 H15 S), Cl4 Cu' _chemical_formula_sum 'C36 H30 Cl4 Cu S2' _chemical_formula_weight 732.06 _chemical_absolute_configuration ? _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 7 _space_group_name_H-M_alt 'P 1 n 1' _space_group_name_Hall 'P -2yac' loop_ _space_group_symop_operation_xyz 'x, y, z' 'x+1/2, -y, z+1/2' _cell_length_a 10.44630(10) _cell_length_b 10.01430(10) _cell_length_c 16.07340(10) _cell_angle_alpha 90 _cell_angle_beta 99.0900(10) _cell_angle_gamma 90 _cell_volume 1660.36(3) _cell_formula_units_Z 2 _cell_measurement_reflns_used 13498 _cell_measurement_temperature 296.4(2) _cell_measurement_theta_max 69.3900 _cell_measurement_theta_min 2.8240 _shelx_estimated_absorpt_T_max 0.487 _shelx_estimated_absorpt_T_min 0.451 _exptl_absorpt_coefficient_mu 5.255 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.75037 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.84a (Rigaku Oxford Diffraction, 2023) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'clear light violet' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary violet _exptl_crystal_density_diffrn 1.464 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description irregular _exptl_crystal_F_000 750 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.16 _exptl_crystal_size_min 0.16 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0326 _diffrn_reflns_av_unetI/netI 0.0307 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.991 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 17754 _diffrn_reflns_point_group_measured_fraction_full 0.867 _diffrn_reflns_point_group_measured_fraction_max 0.852 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 69.713 _diffrn_reflns_theta_min 4.415 _diffrn_ambient_temperature 296.15 _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix3000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.991 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 35.00 109.00 0.50 0.54 -- 98.65-117.00 -90.00 148 2 \w 35.00 109.00 0.50 0.54 -- 98.65-117.00-120.00 148 3 \w 30.00 85.00 0.50 0.54 -- 98.65 -69.00-103.00 110 4 \w 31.00 83.00 0.50 0.54 -- 98.65 -68.00 -90.00 104 5 \w 19.00 101.00 0.50 0.20 -- 42.11-138.00 -90.00 164 6 \w -26.00 67.00 0.50 0.20 -- 42.11 -69.00-103.00 186 7 \w -26.00 37.00 0.50 0.20 -- 42.11 -32.00 -60.00 126 8 \w -34.00 24.00 0.50 0.20 -- 42.11 -11.00-180.00 116 9 \w -29.00 28.00 0.50 0.20 -- 42.11 -21.00 -30.00 114 10 \w -29.00 28.00 0.50 0.20 -- 42.11 -21.00 90.00 114 11 \w 19.00 85.00 0.50 0.20 -- 42.11 65.00 -30.00 132 12 \w 15.00 111.00 0.50 0.20 -- 42.11 77.00-120.00 192 13 \w 18.00 111.00 0.50 0.20 -- 42.11 69.00 29.00 186 14 \w 15.00 111.00 0.50 0.20 -- 42.11 77.00 90.00 192 15 \w 15.00 111.00 0.50 0.20 -- 42.11 77.00 150.00 192 16 \w 74.00 168.00 0.50 0.54 -- 98.65 69.00 29.00 188 17 \w 80.00 165.00 0.50 0.54 -- 98.65 50.00 0.00 170 18 \w 77.00 167.00 0.50 0.54 -- 98.65 59.00 -30.00 180 19 \w 77.00 167.00 0.50 0.54 -- 98.65 59.00 -60.00 180 20 \w 64.00 109.00 0.50 0.20 -- 42.11 138.00-150.00 90 21 \w 64.00 109.00 0.50 0.20 -- 42.11 138.00 -30.00 90 22 \w 64.00 109.00 0.50 0.20 -- 42.11 138.00 30.00 90 23 \w -28.00 30.00 0.50 0.20 -- -41.49 21.00 30.00 116 24 \w -28.00 30.00 0.50 0.20 -- -41.49 21.00 0.00 116 25 \w -37.00 27.00 0.50 0.20 -- -41.49 32.00 -30.00 128 26 \w -66.00 28.00 0.50 0.20 -- -41.49 69.00 29.00 188 27 \w -105.00 -29.00 0.50 0.54 -- -98.03 77.00-120.00 152 28 \w -85.00 -29.00 0.50 0.54 -- -98.03 69.00 29.00 112 29 \w -68.00 -30.00 0.50 0.54 -- -98.03 59.00 0.00 76 30 \w -57.00 -31.00 0.50 0.54 -- -98.03 50.00 30.00 52 31 \w -83.00 -30.00 0.50 0.54 -- -98.03 68.00 150.00 106 32 \w -57.00 -31.00 0.50 0.54 -- -98.03 50.00 150.00 52 33 \w -57.00 -31.00 0.50 0.54 -- -98.03 50.00-150.00 52 34 \w -100.00 -19.00 0.50 0.20 -- -41.49 138.00 0.00 162 35 \w -106.00 -25.00 0.50 0.54 -- -98.03 96.00-180.00 162 36 \w -110.00 -14.00 0.50 0.20 -- -41.49 -77.00-150.00 192 37 \w -109.00 -17.00 0.50 0.20 -- -41.49 -69.00-103.00 184 38 \w -109.00 -18.00 0.50 0.20 -- -41.49 -65.00 -60.00 182 39 \w -110.00 -14.00 0.50 0.20 -- -41.49 -77.00 30.00 192 40 \w -110.00 -14.00 0.50 0.20 -- -41.49 -77.00 90.00 192 41 \w -108.00 -21.00 0.50 0.20 -- -41.49 -54.00 120.00 174 42 \w -109.00 -64.00 0.50 0.20 -- -41.49-138.00 30.00 90 43 \w -109.00 -64.00 0.50 0.20 -- -41.49-138.00 -30.00 90 44 \w -166.00 -73.00 0.50 0.54 -- -98.03 -69.00-103.00 186 45 \w -166.00 -74.00 0.50 0.54 -- -98.03 -68.00-120.00 184 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at home/near, HyPix3000' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source ? _reflns_Friedel_coverage 0.716 _reflns_Friedel_fraction_full 0.734 _reflns_Friedel_fraction_max 0.713 _reflns_number_gt 5122 _reflns_number_total 5339 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.42.84a (Rigaku OD, 2023)' _computing_data_collection 'CrysAlisPro 1.171.42.84a (Rigaku OD, 2023)' _computing_data_reduction 'CrysAlisPro 1.171.42.84a (Rigaku OD, 2023)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _refine_diff_density_max 0.248 _refine_diff_density_min -0.244 _refine_diff_density_rms 0.038 _refine_ls_abs_structure_details ; Flack x determined using 2024 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.010(14) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.040 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 388 _refine_ls_number_reflns 5339 _refine_ls_number_restraints 2 _refine_ls_R_factor_all 0.0311 _refine_ls_R_factor_gt 0.0297 _refine_ls_restrained_S_all 1.040 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0457P)^2^+0.1029P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0765 _refine_ls_wR_factor_ref 0.0777 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C4(H4), C5(H5), C6(H6), C8(H8), C9(H9), C10(H10), C11(H11), C12(H12), C14(H14), C15(H15), C16(H16), C17(H17), C18(H18), C20(H20), C21(H21), C22(H22), C23(H23), C24(H24), C26(H26), C27(H27), C28(H28), C29(H29), C30(H30), C32(H32), C33(H33), C34(H34), C35(H35), C36(H36) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.5982(4) 0.0088(4) 0.5498(3) 0.0417(9) Uani 1 1 d . . . . . S1 S 0.46199(10) 0.00875(10) 0.60377(7) 0.0399(2) Uani 1 1 d . . . . . C2 C 0.6693(4) -0.1080(5) 0.5565(3) 0.0527(11) Uani 1 1 d . . . . . H2 H 0.642454 -0.182348 0.583778 0.063 Uiso 1 1 calc R U . . . C3 C 0.7827(5) -0.1109(6) 0.5209(4) 0.0682(15) Uani 1 1 d . . . . . H3 H 0.834042 -0.187167 0.525888 0.082 Uiso 1 1 calc R U . . . C4 C 0.8184(6) -0.0028(7) 0.4790(4) 0.0757(18) Uani 1 1 d . . . . . H4 H 0.894389 -0.006082 0.455722 0.091 Uiso 1 1 calc R U . . . C5 C 0.7444(6) 0.1114(6) 0.4705(4) 0.0732(16) Uani 1 1 d . . . . . H5 H 0.769260 0.183617 0.440317 0.088 Uiso 1 1 calc R U . . . C6 C 0.6333(5) 0.1188(5) 0.5066(3) 0.0618(13) Uani 1 1 d . . . . . H6 H 0.583222 0.195958 0.502027 0.074 Uiso 1 1 calc R U . . . C7 C 0.5156(4) 0.1059(4) 0.6963(3) 0.0404(9) Uani 1 1 d . . . . . C8 C 0.6447(5) 0.1343(5) 0.7228(3) 0.0547(11) Uani 1 1 d . . . . . H8 H 0.706633 0.112231 0.689395 0.066 Uiso 1 1 calc R U . . . C9 C 0.6806(5) 0.1966(5) 0.8003(3) 0.0628(14) Uani 1 1 d . . . . . H9 H 0.767431 0.215561 0.819216 0.075 Uiso 1 1 calc R U . . . C10 C 0.5894(6) 0.2302(5) 0.8490(3) 0.0584(13) Uani 1 1 d . . . . . H10 H 0.614354 0.272650 0.900440 0.070 Uiso 1 1 calc R U . . . C11 C 0.4608(5) 0.2014(5) 0.8219(3) 0.0538(12) Uani 1 1 d . . . . . H11 H 0.399079 0.225532 0.854975 0.065 Uiso 1 1 calc R U . . . C12 C 0.4227(4) 0.1367(5) 0.7460(3) 0.0461(10) Uani 1 1 d . . . . . H12 H 0.336174 0.114282 0.728636 0.055 Uiso 1 1 calc R U . . . C13 C 0.3437(4) 0.1107(4) 0.5409(3) 0.0397(9) Uani 1 1 d . . . . . C14 C 0.2495(4) 0.0402(5) 0.4873(3) 0.0462(10) Uani 1 1 d . . . . . H14 H 0.250123 -0.052620 0.485447 0.055 Uiso 1 1 calc R U . . . C15 C 0.1541(5) 0.1138(6) 0.4366(3) 0.0530(11) Uani 1 1 d . . . . . H15 H 0.090926 0.069991 0.399185 0.064 Uiso 1 1 calc R U . . . C16 C 0.1530(5) 0.2501(5) 0.4416(3) 0.0535(11) Uani 1 1 d . . . . . H16 H 0.087670 0.297820 0.408286 0.064 Uiso 1 1 calc R U . . . C17 C 0.2478(5) 0.3184(5) 0.4956(3) 0.0532(11) Uani 1 1 d . . . . . H17 H 0.246312 0.411190 0.497764 0.064 Uiso 1 1 calc R U . . . C18 C 0.3441(4) 0.2484(5) 0.5459(3) 0.0462(10) Uani 1 1 d . . . . . H18 H 0.407966 0.292859 0.582514 0.055 Uiso 1 1 calc R U . . . S2 S 0.62800(9) 0.47986(10) 0.28711(6) 0.0370(2) Uani 1 1 d . . . . . C19 C 0.6983(4) 0.4827(4) 0.3958(3) 0.0397(9) Uani 1 1 d . . . . . C20 C 0.8315(4) 0.4875(5) 0.4096(3) 0.0483(11) Uani 1 1 d . . . . . H20 H 0.878516 0.482919 0.365174 0.058 Uiso 1 1 calc R U . . . C21 C 0.8931(6) 0.4994(6) 0.4920(3) 0.0655(14) Uani 1 1 d . . . . . H21 H 0.983051 0.504210 0.503702 0.079 Uiso 1 1 calc R U . . . C22 C 0.8204(6) 0.5041(6) 0.5571(3) 0.0671(15) Uani 1 1 d . . . . . H22 H 0.862352 0.513357 0.612262 0.080 Uiso 1 1 calc R U . . . C23 C 0.6876(5) 0.4955(5) 0.5414(3) 0.0589(13) Uani 1 1 d . . . . . H23 H 0.640540 0.496604 0.585910 0.071 Uiso 1 1 calc R U . . . C24 C 0.6239(4) 0.4850(5) 0.4596(3) 0.0468(10) Uani 1 1 d . . . . . H24 H 0.533945 0.479745 0.447885 0.056 Uiso 1 1 calc R U . . . C25 C 0.5961(4) 0.6520(4) 0.2623(3) 0.0388(8) Uani 1 1 d . . . . . C26 C 0.5799(5) 0.7471(5) 0.3213(3) 0.0545(12) Uani 1 1 d . . . . . H26 H 0.584774 0.724553 0.377822 0.065 Uiso 1 1 calc R U . . . C27 C 0.5560(6) 0.8774(5) 0.2946(4) 0.0667(14) Uani 1 1 d . . . . . H27 H 0.545480 0.943292 0.333718 0.080 Uiso 1 1 calc R U . . . C28 C 0.5478(5) 0.9105(5) 0.2114(4) 0.0623(13) Uani 1 1 d . . . . . H28 H 0.531132 0.998335 0.194188 0.075 Uiso 1 1 calc R U . . . C29 C 0.5643(5) 0.8135(5) 0.1530(3) 0.0571(13) Uani 1 1 d . . . . . H29 H 0.557933 0.835901 0.096328 0.069 Uiso 1 1 calc R U . . . C30 C 0.5900(4) 0.6837(5) 0.1783(3) 0.0455(10) Uani 1 1 d . . . . . H30 H 0.603047 0.618381 0.139403 0.055 Uiso 1 1 calc R U . . . C31 C 0.4713(4) 0.4088(4) 0.2843(2) 0.0397(9) Uani 1 1 d . . . . . C32 C 0.4644(5) 0.2733(5) 0.2724(3) 0.0553(12) Uani 1 1 d . . . . . H32 H 0.538827 0.222835 0.271410 0.066 Uiso 1 1 calc R U . . . C33 C 0.3433(6) 0.2138(6) 0.2619(4) 0.0745(17) Uani 1 1 d . . . . . H33 H 0.336139 0.121760 0.254975 0.089 Uiso 1 1 calc R U . . . C34 C 0.2341(5) 0.2891(7) 0.2617(3) 0.0700(17) Uani 1 1 d . . . . . H34 H 0.153188 0.248003 0.252703 0.084 Uiso 1 1 calc R U . . . C35 C 0.2423(5) 0.4244(6) 0.2747(3) 0.0622(14) Uani 1 1 d . . . . . H35 H 0.167548 0.474576 0.275576 0.075 Uiso 1 1 calc R U . . . C36 C 0.3620(4) 0.4856(5) 0.2865(3) 0.0541(12) Uani 1 1 d . . . . . H36 H 0.369053 0.577131 0.295770 0.065 Uiso 1 1 calc R U . . . Cl1 Cl 0.41461(11) 0.50289(11) 0.69152(7) 0.0523(3) Uani 1 1 d . . . . . Cu1 Cu 0.31173(5) 0.68866(5) 0.63908(4) 0.03747(15) Uani 1 1 d . . . . . Cl2 Cl 0.37900(11) 0.69014(11) 0.51137(7) 0.0515(3) Uani 1 1 d . . . . . Cl3 Cl 0.10729(11) 0.75082(19) 0.59269(9) 0.0747(4) Uani 1 1 d . . . . . Cl4 Cl 0.34125(14) 0.80429(12) 0.76115(8) 0.0608(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.043(2) 0.045(2) 0.039(2) -0.0006(18) 0.0090(17) 0.0004(18) S1 0.0443(5) 0.0371(5) 0.0398(5) -0.0010(4) 0.0112(4) -0.0024(4) C2 0.050(2) 0.053(3) 0.056(3) 0.000(2) 0.008(2) 0.008(2) C3 0.047(3) 0.072(4) 0.088(4) -0.014(3) 0.015(3) 0.010(3) C4 0.054(3) 0.091(5) 0.088(4) -0.023(4) 0.031(3) -0.008(3) C5 0.080(4) 0.070(4) 0.080(4) -0.002(3) 0.044(3) -0.017(3) C6 0.073(3) 0.050(3) 0.070(3) 0.008(3) 0.035(3) 0.002(2) C7 0.045(2) 0.034(2) 0.043(2) 0.0025(18) 0.0080(17) -0.0046(18) C8 0.051(2) 0.060(3) 0.053(3) -0.002(2) 0.009(2) -0.007(2) C9 0.062(3) 0.062(3) 0.060(3) 0.001(3) -0.006(3) -0.014(2) C10 0.085(4) 0.048(3) 0.039(2) -0.001(2) 0.001(2) -0.005(2) C11 0.072(3) 0.052(3) 0.039(2) 0.001(2) 0.012(2) 0.010(2) C12 0.049(2) 0.046(2) 0.044(2) 0.003(2) 0.0092(18) 0.001(2) C13 0.040(2) 0.042(2) 0.038(2) -0.0034(17) 0.0093(17) 0.0014(18) C14 0.051(2) 0.043(2) 0.046(2) -0.0033(19) 0.0104(19) -0.005(2) C15 0.048(2) 0.068(3) 0.043(2) -0.004(2) 0.0067(19) -0.003(2) C16 0.055(3) 0.064(3) 0.043(3) 0.005(2) 0.011(2) 0.010(2) C17 0.066(3) 0.045(3) 0.051(3) 0.003(2) 0.017(2) 0.008(2) C18 0.052(2) 0.042(2) 0.045(2) -0.0047(19) 0.009(2) -0.002(2) S2 0.0384(5) 0.0399(5) 0.0329(5) -0.0021(4) 0.0056(4) 0.0029(4) C19 0.046(2) 0.035(2) 0.036(2) -0.0007(16) 0.0002(17) 0.0064(17) C20 0.046(2) 0.055(3) 0.043(2) 0.001(2) 0.0052(19) 0.009(2) C21 0.050(3) 0.089(4) 0.052(3) -0.008(3) -0.007(2) 0.013(3) C22 0.070(3) 0.088(4) 0.038(3) -0.009(2) -0.007(2) 0.020(3) C23 0.071(3) 0.069(3) 0.036(2) -0.001(2) 0.008(2) 0.014(3) C24 0.049(2) 0.054(3) 0.039(2) -0.001(2) 0.0086(18) 0.009(2) C25 0.0342(18) 0.044(2) 0.038(2) 0.0009(18) 0.0054(15) -0.0005(18) C26 0.074(3) 0.049(3) 0.038(2) -0.003(2) 0.001(2) 0.008(2) C27 0.088(4) 0.046(3) 0.065(3) -0.007(2) 0.007(3) 0.011(3) C28 0.067(3) 0.046(3) 0.075(4) 0.015(3) 0.015(3) 0.009(2) C29 0.060(3) 0.060(3) 0.055(3) 0.017(2) 0.017(2) 0.007(2) C30 0.049(2) 0.052(3) 0.037(2) 0.0008(19) 0.0117(18) 0.001(2) C31 0.042(2) 0.047(2) 0.0303(19) -0.0012(17) 0.0071(16) -0.0023(18) C32 0.054(3) 0.049(3) 0.064(3) -0.012(2) 0.016(2) -0.001(2) C33 0.080(4) 0.069(4) 0.080(4) -0.025(3) 0.028(3) -0.031(3) C34 0.055(3) 0.113(5) 0.045(3) -0.013(3) 0.013(2) -0.027(3) C35 0.041(2) 0.087(4) 0.059(3) 0.005(3) 0.010(2) 0.000(3) C36 0.045(2) 0.059(3) 0.059(3) 0.004(2) 0.010(2) 0.003(2) Cl1 0.0561(6) 0.0452(6) 0.0549(6) 0.0044(5) 0.0065(5) 0.0101(5) Cu1 0.0382(3) 0.0378(3) 0.0367(3) -0.0011(3) 0.0068(2) -0.0005(3) Cl2 0.0601(6) 0.0553(7) 0.0423(5) -0.0014(5) 0.0183(5) 0.0083(5) Cl3 0.0411(6) 0.1231(12) 0.0599(7) 0.0091(8) 0.0079(5) 0.0187(7) Cl4 0.0901(9) 0.0492(6) 0.0444(6) -0.0117(5) 0.0153(6) -0.0131(6) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 S1 1.780(4) . ? C1 C2 1.381(6) . ? C1 C6 1.382(7) . ? S1 C7 1.792(4) . ? S1 C13 1.788(4) . ? C2 H2 0.9300 . ? C2 C3 1.394(7) . ? C3 H3 0.9300 . ? C3 C4 1.357(9) . ? C4 H4 0.9300 . ? C4 C5 1.375(9) . ? C5 H5 0.9300 . ? C5 C6 1.380(7) . ? C6 H6 0.9300 . ? C7 C8 1.378(6) . ? C7 C12 1.386(6) . ? C8 H8 0.9300 . ? C8 C9 1.392(7) . ? C9 H9 0.9300 . ? C9 C10 1.366(8) . ? C10 H10 0.9300 . ? C10 C11 1.375(7) . ? C11 H11 0.9300 . ? C11 C12 1.384(7) . ? C12 H12 0.9300 . ? C13 C14 1.394(6) . ? C13 C18 1.381(6) . ? C14 H14 0.9300 . ? C14 C15 1.394(7) . ? C15 H15 0.9300 . ? C15 C16 1.367(8) . ? C16 H16 0.9300 . ? C16 C17 1.390(7) . ? C17 H17 0.9300 . ? C17 C18 1.379(7) . ? C18 H18 0.9300 . ? S2 C19 1.786(4) . ? S2 C25 1.789(4) . ? S2 C31 1.779(4) . ? C19 C20 1.375(6) . ? C19 C24 1.382(6) . ? C20 H20 0.9300 . ? C20 C21 1.382(6) . ? C21 H21 0.9300 . ? C21 C22 1.387(8) . ? C22 H22 0.9300 . ? C22 C23 1.373(8) . ? C23 H23 0.9300 . ? C23 C24 1.380(6) . ? C24 H24 0.9300 . ? C25 C26 1.373(6) . ? C25 C30 1.379(6) . ? C26 H26 0.9300 . ? C26 C27 1.384(8) . ? C27 H27 0.9300 . ? C27 C28 1.367(8) . ? C28 H28 0.9300 . ? C28 C29 1.381(8) . ? C29 H29 0.9300 . ? C29 C30 1.375(7) . ? C30 H30 0.9300 . ? C31 C32 1.371(7) . ? C31 C36 1.381(6) . ? C32 H32 0.9300 . ? C32 C33 1.384(8) . ? C33 H33 0.9300 . ? C33 C34 1.367(9) . ? C34 H34 0.9300 . ? C34 C35 1.372(9) . ? C35 H35 0.9300 . ? C35 C36 1.378(7) . ? C36 H36 0.9300 . ? Cl1 Cu1 2.2451(12) . ? Cu1 Cl2 2.2723(11) . ? Cu1 Cl3 2.2364(13) . ? Cu1 Cl4 2.2571(12) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C1 S1 115.1(3) . . ? C2 C1 C6 122.1(4) . . ? C6 C1 S1 122.8(4) . . ? C1 S1 C7 103.6(2) . . ? C1 S1 C13 104.97(19) . . ? C13 S1 C7 104.89(19) . . ? C1 C2 H2 121.1 . . ? C1 C2 C3 117.8(5) . . ? C3 C2 H2 121.1 . . ? C2 C3 H3 119.8 . . ? C4 C3 C2 120.3(5) . . ? C4 C3 H3 119.8 . . ? C3 C4 H4 119.4 . . ? C3 C4 C5 121.2(5) . . ? C5 C4 H4 119.4 . . ? C4 C5 H5 120.0 . . ? C4 C5 C6 120.0(5) . . ? C6 C5 H5 120.0 . . ? C1 C6 H6 120.8 . . ? C5 C6 C1 118.5(5) . . ? C5 C6 H6 120.8 . . ? C8 C7 S1 122.0(4) . . ? C8 C7 C12 121.1(4) . . ? C12 C7 S1 116.4(3) . . ? C7 C8 H8 120.6 . . ? C7 C8 C9 118.7(5) . . ? C9 C8 H8 120.6 . . ? C8 C9 H9 119.7 . . ? C10 C9 C8 120.7(5) . . ? C10 C9 H9 119.7 . . ? C9 C10 H10 119.9 . . ? C9 C10 C11 120.1(5) . . ? C11 C10 H10 119.9 . . ? C10 C11 H11 119.7 . . ? C10 C11 C12 120.5(5) . . ? C12 C11 H11 119.7 . . ? C7 C12 H12 120.6 . . ? C11 C12 C7 118.8(4) . . ? C11 C12 H12 120.6 . . ? C14 C13 S1 114.7(3) . . ? C18 C13 S1 122.8(3) . . ? C18 C13 C14 122.5(4) . . ? C13 C14 H14 121.2 . . ? C13 C14 C15 117.6(4) . . ? C15 C14 H14 121.2 . . ? C14 C15 H15 119.8 . . ? C16 C15 C14 120.4(5) . . ? C16 C15 H15 119.8 . . ? C15 C16 H16 119.5 . . ? C15 C16 C17 121.1(5) . . ? C17 C16 H16 119.5 . . ? C16 C17 H17 120.1 . . ? C18 C17 C16 119.9(5) . . ? C18 C17 H17 120.1 . . ? C13 C18 H18 120.7 . . ? C17 C18 C13 118.6(4) . . ? C17 C18 H18 120.7 . . ? C19 S2 C25 103.66(19) . . ? C31 S2 C19 105.40(19) . . ? C31 S2 C25 103.97(19) . . ? C20 C19 S2 114.1(3) . . ? C20 C19 C24 123.6(4) . . ? C24 C19 S2 122.3(3) . . ? C19 C20 H20 121.2 . . ? C19 C20 C21 117.6(5) . . ? C21 C20 H20 121.2 . . ? C20 C21 H21 120.1 . . ? C20 C21 C22 119.8(5) . . ? C22 C21 H21 120.1 . . ? C21 C22 H22 119.4 . . ? C23 C22 C21 121.1(5) . . ? C23 C22 H22 119.4 . . ? C22 C23 H23 120.0 . . ? C22 C23 C24 120.1(5) . . ? C24 C23 H23 120.0 . . ? C19 C24 H24 121.2 . . ? C23 C24 C19 117.7(4) . . ? C23 C24 H24 121.2 . . ? C26 C25 S2 123.6(3) . . ? C26 C25 C30 121.7(4) . . ? C30 C25 S2 114.7(3) . . ? C25 C26 H26 120.8 . . ? C25 C26 C27 118.4(4) . . ? C27 C26 H26 120.8 . . ? C26 C27 H27 119.6 . . ? C28 C27 C26 120.8(5) . . ? C28 C27 H27 119.6 . . ? C27 C28 H28 120.0 . . ? C27 C28 C29 119.9(5) . . ? C29 C28 H28 120.0 . . ? C28 C29 H29 119.9 . . ? C30 C29 C28 120.2(5) . . ? C30 C29 H29 119.9 . . ? C25 C30 H30 120.5 . . ? C29 C30 C25 118.9(4) . . ? C29 C30 H30 120.5 . . ? C32 C31 S2 115.3(3) . . ? C32 C31 C36 121.9(4) . . ? C36 C31 S2 122.5(4) . . ? C31 C32 H32 121.0 . . ? C31 C32 C33 118.0(5) . . ? C33 C32 H32 121.0 . . ? C32 C33 H33 119.7 . . ? C34 C33 C32 120.6(5) . . ? C34 C33 H33 119.7 . . ? C33 C34 H34 119.6 . . ? C33 C34 C35 120.8(5) . . ? C35 C34 H34 119.6 . . ? C34 C35 H35 120.2 . . ? C34 C35 C36 119.6(5) . . ? C36 C35 H35 120.2 . . ? C31 C36 H36 120.5 . . ? C35 C36 C31 119.0(5) . . ? C35 C36 H36 120.5 . . ? Cl1 Cu1 Cl2 98.43(5) . . ? Cl1 Cu1 Cl4 96.15(5) . . ? Cl3 Cu1 Cl1 136.98(6) . . ? Cl3 Cu1 Cl2 96.45(5) . . ? Cl3 Cu1 Cl4 98.00(6) . . ? Cl4 Cu1 Cl2 139.70(5) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 S1 C7 C8 -15.6(4) . . . . ? C1 S1 C7 C12 172.3(3) . . . . ? C1 S1 C13 C14 98.7(3) . . . . ? C1 S1 C13 C18 -82.5(4) . . . . ? C1 C2 C3 C4 -2.0(8) . . . . ? S1 C1 C2 C3 -175.3(4) . . . . ? S1 C1 C6 C5 176.6(5) . . . . ? S1 C7 C8 C9 -172.5(4) . . . . ? S1 C7 C12 C11 174.4(3) . . . . ? S1 C13 C14 C15 179.9(3) . . . . ? S1 C13 C18 C17 -179.2(3) . . . . ? C2 C1 S1 C7 103.3(4) . . . . ? C2 C1 S1 C13 -147.0(3) . . . . ? C2 C1 C6 C5 -1.1(8) . . . . ? C2 C3 C4 C5 -0.1(10) . . . . ? C3 C4 C5 C6 1.7(10) . . . . ? C4 C5 C6 C1 -1.0(9) . . . . ? C6 C1 S1 C7 -74.7(4) . . . . ? C6 C1 S1 C13 35.1(5) . . . . ? C6 C1 C2 C3 2.6(7) . . . . ? C7 S1 C13 C14 -152.4(3) . . . . ? C7 S1 C13 C18 26.4(4) . . . . ? C7 C8 C9 C10 -0.7(8) . . . . ? C8 C7 C12 C11 2.3(7) . . . . ? C8 C9 C10 C11 0.7(8) . . . . ? C9 C10 C11 C12 0.9(8) . . . . ? C10 C11 C12 C7 -2.3(7) . . . . ? C12 C7 C8 C9 -0.9(7) . . . . ? C13 S1 C7 C8 -125.4(4) . . . . ? C13 S1 C7 C12 62.5(4) . . . . ? C13 C14 C15 C16 -1.5(7) . . . . ? C14 C13 C18 C17 -0.4(7) . . . . ? C14 C15 C16 C17 1.4(7) . . . . ? C15 C16 C17 C18 -0.8(7) . . . . ? C16 C17 C18 C13 0.3(7) . . . . ? C18 C13 C14 C15 1.0(6) . . . . ? S2 C19 C20 C21 175.6(4) . . . . ? S2 C19 C24 C23 -176.0(4) . . . . ? S2 C25 C26 C27 179.8(4) . . . . ? S2 C25 C30 C29 179.2(4) . . . . ? S2 C31 C32 C33 -174.2(4) . . . . ? S2 C31 C36 C35 172.9(4) . . . . ? C19 S2 C25 C26 -23.7(4) . . . . ? C19 S2 C25 C30 155.7(3) . . . . ? C19 S2 C31 C32 -92.8(4) . . . . ? C19 S2 C31 C36 92.7(4) . . . . ? C19 C20 C21 C22 0.9(8) . . . . ? C20 C19 C24 C23 1.3(7) . . . . ? C20 C21 C22 C23 0.9(9) . . . . ? C21 C22 C23 C24 -1.6(8) . . . . ? C22 C23 C24 C19 0.5(7) . . . . ? C24 C19 C20 C21 -2.0(7) . . . . ? C25 S2 C19 C20 -93.5(3) . . . . ? C25 S2 C19 C24 84.1(4) . . . . ? C25 S2 C31 C32 158.4(4) . . . . ? C25 S2 C31 C36 -16.1(4) . . . . ? C25 C26 C27 C28 0.5(8) . . . . ? C26 C25 C30 C29 -1.4(7) . . . . ? C26 C27 C28 C29 -0.5(9) . . . . ? C27 C28 C29 C30 -0.5(8) . . . . ? C28 C29 C30 C25 1.4(7) . . . . ? C30 C25 C26 C27 0.4(7) . . . . ? C31 S2 C19 C20 157.6(3) . . . . ? C31 S2 C19 C24 -24.8(4) . . . . ? C31 S2 C25 C26 86.3(4) . . . . ? C31 S2 C25 C30 -94.3(3) . . . . ? C31 C32 C33 C34 1.4(9) . . . . ? C32 C31 C36 C35 -1.3(7) . . . . ? C32 C33 C34 C35 -2.2(10) . . . . ? C33 C34 C35 C36 1.3(9) . . . . ? C34 C35 C36 C31 0.5(8) . . . . ? C36 C31 C32 C33 0.4(7) . . . . ? _shelx_res_file ; TITL i1188cucl2_auto_a.res in Pn i1188cucl2_auto.res created by SHELXL-2018/3 at 12:16:39 on 07-Jan-2025 REM Old TITL i1188 CuCl2_auto in Pn REM SHELXT solution in Pn: R1 0.081, Rweak 0.025, Alpha 0.001 REM 0.320 for 194 systematic absences, Orientation as input REM Flack x = 0.053 ( 0.011 ) from 2056 Parsons' quotients REM Formula found by SHELXT: Cu Cl6 C36 CELL 1.54184 10.4463 10.0143 16.0734 90 99.09 90 ZERR 2 0.0001 0.0001 0.0001 0 0.001 0 LATT -1 SYMM 0.5+X,-Y,0.5+Z SFAC C H Cl Cu S UNIT 72 60 8 2 4 L.S. 11 0 0 PLAN 7 SIZE 0.16 0.16 0.18 TEMP 23 CONF BOND LIST 6 fmap 2 53 acta MORE -1 BOND $H REM REM REM WGHT 0.045700 0.102900 FVAR 0.74766 C1 1 0.598212 0.008811 0.549779 11.00000 0.04262 0.04458 = 0.03879 -0.00063 0.00899 0.00043 S1 5 0.461992 0.008747 0.603771 11.00000 0.04425 0.03706 = 0.03979 -0.00105 0.01122 -0.00240 C2 1 0.669309 -0.107997 0.556454 11.00000 0.04971 0.05301 = 0.05551 -0.00004 0.00847 0.00792 AFIX 43 H2 2 0.642454 -0.182348 0.583778 11.00000 -1.20000 AFIX 0 C3 1 0.782668 -0.110852 0.520899 11.00000 0.04651 0.07182 = 0.08761 -0.01381 0.01457 0.01043 AFIX 43 H3 2 0.834042 -0.187167 0.525888 11.00000 -1.20000 AFIX 0 C4 1 0.818439 -0.002810 0.479034 11.00000 0.05410 0.09102 = 0.08843 -0.02318 0.03112 -0.00825 AFIX 43 H4 2 0.894389 -0.006082 0.455722 11.00000 -1.20000 AFIX 0 C5 1 0.744429 0.111394 0.470463 11.00000 0.08010 0.06954 = 0.08019 -0.00237 0.04387 -0.01666 AFIX 43 H5 2 0.769260 0.183617 0.440317 11.00000 -1.20000 AFIX 0 C6 1 0.633329 0.118759 0.506611 11.00000 0.07274 0.05031 = 0.07004 0.00847 0.03515 0.00221 AFIX 43 H6 2 0.583222 0.195958 0.502027 11.00000 -1.20000 AFIX 0 C7 1 0.515585 0.105860 0.696341 11.00000 0.04467 0.03403 = 0.04279 0.00255 0.00803 -0.00464 C8 1 0.644676 0.134279 0.722759 11.00000 0.05115 0.06013 = 0.05314 -0.00225 0.00941 -0.00723 AFIX 43 H8 2 0.706633 0.112231 0.689395 11.00000 -1.20000 AFIX 0 C9 1 0.680552 0.196599 0.800315 11.00000 0.06181 0.06193 = 0.05982 0.00149 -0.00559 -0.01408 AFIX 43 H9 2 0.767431 0.215561 0.819216 11.00000 -1.20000 AFIX 0 C10 1 0.589416 0.230205 0.848969 11.00000 0.08520 0.04820 = 0.03891 -0.00066 0.00056 -0.00481 AFIX 43 H10 2 0.614354 0.272650 0.900440 11.00000 -1.20000 AFIX 0 C11 1 0.460843 0.201363 0.821948 11.00000 0.07191 0.05195 = 0.03873 0.00115 0.01198 0.01004 AFIX 43 H11 2 0.399079 0.225532 0.854975 11.00000 -1.20000 AFIX 0 C12 1 0.422663 0.136678 0.746020 11.00000 0.04894 0.04626 = 0.04384 0.00328 0.00923 0.00101 AFIX 43 H12 2 0.336174 0.114282 0.728636 11.00000 -1.20000 AFIX 0 C13 1 0.343739 0.110717 0.540870 11.00000 0.04019 0.04178 = 0.03821 -0.00340 0.00932 0.00143 C14 1 0.249458 0.040194 0.487304 11.00000 0.05095 0.04250 = 0.04613 -0.00326 0.01039 -0.00545 AFIX 43 H14 2 0.250123 -0.052620 0.485447 11.00000 -1.20000 AFIX 0 C15 1 0.154123 0.113825 0.436610 11.00000 0.04759 0.06829 = 0.04287 -0.00396 0.00669 -0.00333 AFIX 43 H15 2 0.090926 0.069991 0.399185 11.00000 -1.20000 AFIX 0 C16 1 0.152968 0.250080 0.441580 11.00000 0.05496 0.06365 = 0.04291 0.00540 0.01065 0.00967 AFIX 43 H16 2 0.087670 0.297820 0.408286 11.00000 -1.20000 AFIX 0 C17 1 0.247799 0.318411 0.495582 11.00000 0.06555 0.04542 = 0.05093 0.00270 0.01673 0.00821 AFIX 43 H17 2 0.246312 0.411190 0.497764 11.00000 -1.20000 AFIX 0 C18 1 0.344139 0.248354 0.545943 11.00000 0.05243 0.04193 = 0.04469 -0.00474 0.00907 -0.00191 AFIX 43 H18 2 0.407966 0.292859 0.582514 11.00000 -1.20000 AFIX 0 S2 5 0.627999 0.479865 0.287111 11.00000 0.03836 0.03991 = 0.03287 -0.00210 0.00564 0.00289 C19 1 0.698334 0.482654 0.395824 11.00000 0.04648 0.03500 = 0.03573 -0.00070 0.00024 0.00637 C20 1 0.831519 0.487492 0.409644 11.00000 0.04559 0.05538 = 0.04347 0.00080 0.00523 0.00859 AFIX 43 H20 2 0.878516 0.482919 0.365174 11.00000 -1.20000 AFIX 0 C21 1 0.893097 0.499393 0.491968 11.00000 0.05030 0.08916 = 0.05210 -0.00847 -0.00672 0.01334 AFIX 43 H21 2 0.983051 0.504210 0.503702 11.00000 -1.20000 AFIX 0 C22 1 0.820407 0.504136 0.557062 11.00000 0.07016 0.08814 = 0.03779 -0.00876 -0.00738 0.02042 AFIX 43 H22 2 0.862352 0.513357 0.612262 11.00000 -1.20000 AFIX 0 C23 1 0.687593 0.495450 0.541391 11.00000 0.07134 0.06906 = 0.03610 -0.00150 0.00811 0.01369 AFIX 43 H23 2 0.640540 0.496604 0.585910 11.00000 -1.20000 AFIX 0 C24 1 0.623874 0.485011 0.459630 11.00000 0.04873 0.05372 = 0.03855 -0.00141 0.00865 0.00917 AFIX 43 H24 2 0.533945 0.479745 0.447885 11.00000 -1.20000 AFIX 0 C25 1 0.596063 0.652048 0.262336 11.00000 0.03420 0.04379 = 0.03819 0.00089 0.00539 -0.00055 C26 1 0.579857 0.747144 0.321285 11.00000 0.07440 0.04867 = 0.03785 -0.00311 0.00070 0.00768 AFIX 43 H26 2 0.584774 0.724553 0.377822 11.00000 -1.20000 AFIX 0 C27 1 0.556029 0.877424 0.294580 11.00000 0.08758 0.04599 = 0.06479 -0.00716 0.00663 0.01128 AFIX 43 H27 2 0.545480 0.943292 0.333718 11.00000 -1.20000 AFIX 0 C28 1 0.547799 0.910532 0.211416 11.00000 0.06678 0.04623 = 0.07524 0.01498 0.01511 0.00856 AFIX 43 H28 2 0.531132 0.998335 0.194188 11.00000 -1.20000 AFIX 0 C29 1 0.564258 0.813462 0.152976 11.00000 0.05979 0.05954 = 0.05451 0.01669 0.01676 0.00735 AFIX 43 H29 2 0.557933 0.835901 0.096328 11.00000 -1.20000 AFIX 0 C30 1 0.589974 0.683713 0.178317 11.00000 0.04883 0.05229 = 0.03687 0.00080 0.01173 0.00104 AFIX 43 H30 2 0.603047 0.618381 0.139403 11.00000 -1.20000 AFIX 0 C31 1 0.471253 0.408796 0.284325 11.00000 0.04223 0.04706 = 0.03033 -0.00119 0.00710 -0.00231 C32 1 0.464356 0.273304 0.272420 11.00000 0.05405 0.04940 = 0.06439 -0.01248 0.01569 -0.00081 AFIX 43 H32 2 0.538827 0.222835 0.271410 11.00000 -1.20000 AFIX 0 C33 1 0.343255 0.213794 0.261943 11.00000 0.07951 0.06887 = 0.08023 -0.02498 0.02814 -0.03082 AFIX 43 H33 2 0.336139 0.121760 0.254975 11.00000 -1.20000 AFIX 0 C34 1 0.234054 0.289051 0.261747 11.00000 0.05452 0.11251 = 0.04490 -0.01345 0.01344 -0.02694 AFIX 43 H34 2 0.153188 0.248003 0.252703 11.00000 -1.20000 AFIX 0 C35 1 0.242259 0.424424 0.274728 11.00000 0.04075 0.08706 = 0.05941 0.00498 0.01015 0.00012 AFIX 43 H35 2 0.167548 0.474576 0.275576 11.00000 -1.20000 AFIX 0 C36 1 0.361964 0.485571 0.286501 11.00000 0.04494 0.05875 = 0.05940 0.00439 0.01024 0.00327 AFIX 43 H36 2 0.369053 0.577131 0.295770 11.00000 -1.20000 AFIX 0 CL1 3 0.414609 0.502886 0.691518 11.00000 0.05610 0.04524 = 0.05488 0.00445 0.00653 0.01012 CU1 4 0.311730 0.688661 0.639079 11.00000 0.03822 0.03778 = 0.03671 -0.00107 0.00683 -0.00053 CL2 3 0.379001 0.690144 0.511370 11.00000 0.06010 0.05534 = 0.04232 -0.00138 0.01835 0.00826 CL3 3 0.107285 0.750820 0.592694 11.00000 0.04107 0.12312 = 0.05992 0.00909 0.00790 0.01872 CL4 3 0.341254 0.804286 0.761150 11.00000 0.09012 0.04922 = 0.04443 -0.01165 0.01530 -0.01311 HKLF 4 REM i1188cucl2_auto_a.res in Pn REM wR2 = 0.0777, GooF = S = 1.040, Restrained GooF = 1.040 for all data REM R1 = 0.0297 for 5122 Fo > 4sig(Fo) and 0.0311 for all 5339 data REM 388 parameters refined using 2 restraints END WGHT 0.0457 0.1029 REM Highest difference peak 0.248, deepest hole -0.244, 1-sigma level 0.038 Q1 1 0.1071 0.6611 0.5828 11.00000 0.05 0.25 Q2 1 0.2139 0.6954 0.6041 11.00000 0.05 0.19 Q3 1 0.2778 0.8201 0.7339 11.00000 0.05 0.17 Q4 1 0.4124 0.5964 0.6685 11.00000 0.05 0.16 Q5 1 0.6231 0.5821 0.2825 11.00000 0.05 0.16 Q6 1 0.5553 -0.3136 0.6156 11.00000 0.05 0.14 Q7 1 0.4565 0.7039 0.5542 11.00000 0.05 0.14 ; _shelx_res_checksum 80984 _shelx_hkl_file ; -12 0 -3 0.54 1.88 -12 0 -2 6.11 2.44 -12 0 -2 4.34 2.12 -12 0 -1 0.67 2.45 -12 0 -1 -0.59 1.98 -12 0 0 18.33 3.76 -12 0 0 7.07 2.91 -12 0 1 2.63 2.27 -12 0 1 -3.68 2.71 -12 0 2 14.08 3.46 -12 0 2 13.53 3.76 -12 0 3 -0.67 2.69 -12 0 3 -0.76 3.31 -12 0 4 189.67 12.38 -12 0 4 174.80 11.42 -12 0 5 -1.46 2.61 -12 0 6 290.08 15.58 -12 0 7 -0.66 2.20 -12 0 8 93.48 7.73 -12 0 9 0.53 1.79 -12 1 -3 13.76 3.01 -12 -1 -3 11.36 2.79 -12 1 -2 54.20 5.77 -12 -1 -2 63.10 6.12 -12 1 -2 55.67 5.88 -12 1 -1 3.82 2.55 -12 1 -1 4.99 2.68 -12 -1 -1 0.64 2.14 -12 1 0 12.61 3.37 -12 -1 0 13.60 3.56 -12 1 0 12.23 3.40 -12 -1 1 63.11 6.84 -12 1 1 64.56 6.79 -12 1 1 73.22 7.07 -12 1 2 42.33 5.56 -12 1 2 39.24 5.57 -12 -1 2 32.67 5.34 -12 1 3 14.17 3.77 -12 1 3 11.70 3.66 -12 -1 3 18.24 4.24 -12 1 4 90.39 8.11 -12 1 4 88.26 8.02 -12 -1 4 76.66 7.66 -12 1 5 4.09 2.66 -12 -1 5 4.23 2.68 -12 1 5 3.53 2.44 -12 1 6 32.53 5.01 -12 1 6 39.08 5.36 -12 -1 6 44.60 5.60 -12 -1 7 77.91 7.14 -12 1 7 63.66 6.53 -12 1 7 71.17 6.77 -12 1 8 55.88 5.66 -12 1 8 49.35 5.36 -12 -1 8 45.66 5.28 -12 2 -2 15.72 3.28 -12 -2 -1 45.73 5.30 -12 2 -1 56.17 5.87 -12 2 0 13.45 3.35 -12 -2 0 7.19 2.58 -12 2 1 30.09 4.76 -12 -2 1 20.76 4.11 -12 2 2 28.10 4.67 -12 2 2 24.93 4.43 -12 -2 2 16.79 3.75 -12 2 3 2.76 2.62 -12 2 3 3.87 2.64 -12 -2 3 1.30 2.18 -12 2 4 25.94 4.49 -12 -2 4 23.23 4.25 -12 2 4 24.89 4.25 -12 2 5 13.94 3.43 -12 -2 5 13.17 3.48 -12 2 6 39.28 5.30 -12 -2 6 28.64 4.40 -12 2 7 20.10 3.83 -12 -2 7 26.02 4.04 -12 2 8 40.80 5.00 -12 3 -1 4.61 2.20 -12 3 0 20.65 3.68 -12 3 1 3.54 2.30 -12 3 2 58.43 6.18 -12 3 3 17.23 3.68 -12 3 4 11.58 3.24 -12 3 5 23.08 4.08 -12 3 6 34.26 4.64 -12 3 7 7.27 2.37 -11 0 -6 0.58 1.86 -11 0 -6 0.62 2.21 -11 0 -5 28.09 4.78 -11 0 -5 22.99 4.33 -11 0 -4 -0.81 2.60 -11 0 -4 1.52 2.88 -11 0 -3 11.56 3.78 -11 0 -3 14.94 4.25 -11 0 -2 -0.88 3.04 -11 0 -2 -0.93 2.89 -11 0 -1 69.33 8.34 -11 0 -1 48.42 6.87 -11 0 0 -3.02 3.71 -11 0 0 0.94 2.90 -11 0 1 194.13 14.46 -11 0 1 196.11 13.98 -11 0 2 -0.96 3.92 -11 0 2 -4.12 4.12 -11 0 3 254.60 16.40 -11 0 3 276.95 17.52 -11 0 4 -0.94 3.26 -11 0 4 1.02 3.53 -11 0 5 201.70 14.47 -11 0 5 185.94 13.58 -11 0 6 0.90 2.66 -11 0 6 -1.96 3.15 -11 0 7 361.59 19.69 -11 0 7 331.40 18.57 -11 0 8 -0.82 2.63 -11 0 8 -0.89 2.39 -11 0 9 185.00 12.83 -11 0 9 194.85 12.59 -11 0 10 0.75 2.23 -11 0 11 157.25 10.65 -11 0 12 -2.21 2.10 -11 1 -6 18.17 3.66 -11 -1 -6 16.11 3.36 -11 1 -6 16.01 3.51 -11 1 -5 17.25 3.97 -11 1 -5 9.73 3.13 -11 -1 -5 17.43 3.96 -11 1 -4 7.01 3.04 -11 1 -4 5.47 2.88 -11 -1 -4 6.26 3.21 -11 1 -3 59.61 7.19 -11 1 -3 56.20 6.98 -11 -1 -3 52.83 6.82 -11 -1 -2 17.27 4.46 -11 1 -2 6.35 3.45 -11 1 -2 16.39 4.39 -11 1 -1 118.20 10.61 -11 -1 -1 92.07 9.62 -11 1 -1 89.54 9.46 -11 -1 0 222.32 14.95 -11 1 0 204.17 14.44 -11 1 1 79.95 9.27 -11 -1 1 77.89 8.90 -11 1 1 85.17 9.45 -11 1 2 272.12 17.36 -11 1 2 272.84 17.26 -11 -1 2 273.54 17.26 -11 1 3 6.92 4.06 -11 -1 3 7.04 4.13 -11 1 3 10.07 4.23 -11 1 4 83.09 9.09 -11 -1 4 71.89 8.52 -11 1 4 63.82 8.32 -11 -1 5 76.76 9.05 -11 1 5 83.40 9.36 -11 1 5 90.23 9.52 -11 1 6 40.98 6.54 -11 -1 6 45.03 6.78 -11 1 6 34.31 6.06 -11 1 7 14.31 4.10 -11 -1 7 15.66 4.75 -11 1 7 17.38 4.50 -11 1 8 60.98 7.34 -11 1 8 64.80 7.44 -11 -1 8 56.67 7.21 -11 1 9 92.07 8.60 -11 -1 9 80.12 8.32 -11 1 9 102.15 8.94 -11 -1 10 103.09 8.80 -11 1 10 103.25 8.75 -11 1 10 95.88 8.51 -11 1 11 50.76 5.84 -11 -1 11 44.72 5.56 -11 1 11 42.18 5.37 -11 -1 12 22.23 3.62 -11 1 12 22.38 3.69 -11 -2 -6 29.88 4.04 -11 2 -6 39.10 4.79 -11 2 -5 146.85 10.12 -11 -2 -5 139.92 9.58 -11 2 -5 120.62 9.05 -11 2 -4 13.11 3.51 -11 -2 -4 10.56 3.52 -11 2 -4 17.90 4.18 -11 2 -3 72.26 7.78 -11 2 -3 75.01 7.72 -11 -2 -3 55.76 6.79 -11 2 -2 29.04 5.39 -11 2 -2 30.54 5.48 -11 -2 -2 24.91 5.09 -11 2 -1 118.66 10.50 -11 2 -1 139.60 11.54 -11 -2 -1 132.10 10.84 -11 2 0 15.26 4.44 -11 -2 0 8.14 3.73 -11 2 0 20.78 4.72 -11 2 1 9.24 3.72 -11 2 1 18.46 5.00 -11 -2 1 19.45 4.84 -11 2 2 70.45 8.57 -11 -2 2 58.13 7.69 -11 2 2 60.69 7.89 -11 2 3 121.32 10.79 -11 -2 3 116.51 10.79 -11 2 3 137.63 11.63 -11 2 4 43.42 6.90 -11 -2 4 24.25 5.28 -11 2 4 36.01 6.19 -11 2 5 14.18 4.58 -11 2 5 19.89 5.01 -11 -2 5 22.00 5.14 -11 2 6 24.75 5.41 -11 -2 6 19.59 4.76 -11 2 6 30.63 5.29 -11 2 7 76.38 8.43 -11 -2 7 85.33 8.42 -11 2 7 83.57 8.43 -11 2 8 90.33 8.90 -11 2 8 86.92 8.44 -11 -2 8 70.61 7.86 -11 -2 9 149.64 11.05 -11 2 9 167.02 11.35 -11 2 9 189.95 12.27 -11 2 10 24.84 4.62 -11 -2 10 23.66 4.25 -11 2 11 28.70 4.37 -11 -2 11 35.36 4.55 -11 3 -5 49.61 5.43 -11 3 -4 1.95 2.47 -11 3 -3 75.10 7.61 -11 3 -2 17.46 4.34 -11 3 -1 181.88 12.85 -11 3 0 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25.32 -10 0 4 469.37 25.67 -10 0 5 -1.09 3.36 -10 0 5 -2.31 4.26 -10 0 6 79.64 9.18 -10 0 6 75.59 9.52 -10 0 7 -1.06 3.54 -10 0 7 -1.13 3.19 -10 0 8 19.61 5.23 -10 0 8 9.90 4.07 -10 0 9 -0.99 3.19 -10 0 9 -1.06 2.67 -10 0 10 76.77 8.92 -10 0 10 82.25 8.96 -10 0 11 -0.86 2.65 -10 0 11 0.92 2.46 -10 0 12 28.83 4.94 -10 0 12 20.46 4.68 -10 0 13 -0.70 2.17 -10 0 14 33.54 4.52 -10 0 14 38.83 4.88 -10 -1 -9 3.53 1.97 -10 -1 -9 3.87 2.16 -10 1 -9 6.98 2.45 -10 1 -9 4.98 2.53 -10 -1 -8 33.97 4.64 -10 1 -8 52.65 6.07 -10 -1 -8 46.85 5.91 -10 1 -8 56.03 6.31 -10 1 -7 11.97 3.85 -10 -1 -7 9.70 3.90 -10 1 -7 8.96 3.65 -10 1 -6 47.81 6.98 -10 -1 -6 42.73 6.61 -10 1 -6 39.73 6.47 -10 -1 -5 257.53 16.78 -10 1 -5 271.93 17.15 -10 1 -5 279.21 17.39 -10 -1 -4 115.73 11.37 -10 1 -4 114.91 11.28 -10 1 -4 108.96 10.88 -10 1 -3 35.26 6.76 -10 1 -3 37.83 7.11 -10 -1 -3 40.59 7.01 -10 -1 -2 10.13 4.17 -10 1 -2 20.36 5.83 -10 -1 -1 37.73 6.98 -10 1 -1 49.59 8.29 -10 1 -1 58.59 8.51 -10 1 0 358.72 21.29 -10 -1 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5 614.29 28.48 0 -2 5 659.80 31.16 0 -2 5 625.92 26.28 0 2 5 657.18 26.55 0 2 5 667.19 28.14 0 -2 5 682.86 28.22 0 -2 5 610.02 27.84 0 2 5 610.13 27.93 0 2 5 664.14 27.54 0 2 6 472.67 24.61 0 2 6 464.50 24.84 0 -2 6 431.64 26.31 0 -2 6 477.39 23.03 0 2 6 518.43 23.77 0 2 6 499.01 24.50 0 -2 6 506.39 24.65 0 -2 6 502.00 25.46 0 2 6 448.82 24.65 0 2 6 509.97 23.54 0 -2 7 541.38 27.67 0 2 7 584.61 30.15 0 -2 7 579.67 29.99 0 -2 7 457.82 29.27 0 2 7 549.73 28.48 0 2 7 556.49 29.17 0 2 7 573.43 27.30 0 -2 7 566.52 27.18 0 2 7 510.16 27.05 0 -2 8 1330.22 53.13 0 -2 8 1290.62 58.08 0 -2 8 1291.10 52.15 0 2 8 1370.45 52.98 0 2 8 1423.08 54.74 0 2 8 1291.59 53.83 0 2 8 1270.71 54.57 0 -2 8 1297.23 55.81 0 2 8 1271.01 55.93 0 -2 9 69.78 12.29 0 2 9 67.71 11.80 0 2 9 67.77 10.43 0 2 9 83.43 12.23 0 -2 9 88.94 12.84 0 2 9 93.06 11.74 0 -2 9 89.57 11.45 0 2 9 70.36 10.59 0 -2 10 1832.49 75.85 0 2 10 1760.09 75.57 0 -2 10 1698.97 56.79 0 -2 10 1700.63 57.18 0 -2 10 1720.93 57.37 0 -2 10 1702.02 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681.26 36.08 0 -4 -6 532.59 29.85 0 -4 -6 515.00 28.18 0 -4 -5 1731.76 63.46 0 -4 -5 1588.81 61.45 0 -4 -4 1108.22 44.16 0 -4 -4 1019.07 43.01 0 -4 -3 1936.85 65.31 0 -4 -3 1791.21 64.94 0 4 -3 1840.28 63.30 0 -4 -3 1746.45 68.29 0 4 -2 77.76 8.84 0 -4 -2 81.66 8.70 0 4 -2 84.03 8.48 0 -4 -2 75.01 9.90 0 4 -1 619.57 29.09 0 -4 -1 726.83 33.20 0 -4 -1 699.40 29.95 0 4 -1 699.15 30.33 0 4 0 6469.85 190.67 0 -4 0 5884.80 190.86 0 -4 0 6545.69 194.13 0 4 0 6271.07 190.92 0 -4 0 6478.53 189.25 0 -4 1 646.86 27.45 0 4 1 682.14 29.89 0 4 1 708.17 30.95 0 -4 1 708.65 28.68 0 -4 1 709.67 30.53 0 4 1 688.36 30.73 0 -4 1 692.70 32.51 0 4 2 39.19 5.96 0 -4 2 41.12 7.09 0 4 2 34.65 6.26 0 -4 2 35.71 6.85 0 -4 2 33.79 5.38 0 4 2 34.78 6.18 0 4 2 31.28 6.13 0 4 3 1936.30 67.13 0 4 3 1866.28 67.03 0 4 3 1920.52 66.68 0 4 3 1902.18 66.44 0 -4 3 1921.98 70.00 0 4 3 1757.37 67.25 0 -4 3 1943.13 65.57 0 4 4 1145.27 44.86 0 4 4 1143.29 45.15 0 4 4 1058.43 44.17 0 4 4 997.81 43.06 0 -4 4 1002.71 42.28 0 -4 4 1067.10 47.19 0 4 4 986.71 44.10 0 4 4 1166.90 43.90 0 4 5 1462.93 56.83 0 4 5 1514.62 57.59 0 4 5 1404.86 56.79 0 4 5 1473.99 55.71 0 -4 5 1424.13 55.13 0 4 5 1469.83 55.63 0 4 5 1269.02 54.93 0 4 5 1369.63 57.80 0 -4 5 1516.75 61.69 0 -4 6 531.54 33.68 0 4 6 555.23 30.06 0 4 6 572.77 31.61 0 4 6 581.55 32.06 0 4 6 598.99 30.85 0 -4 6 569.75 30.24 0 -4 7 555.62 37.49 0 4 7 702.39 35.19 0 -4 7 620.98 33.65 0 4 7 630.45 35.40 0 4 7 609.20 35.13 0 4 8 71.13 12.33 0 4 8 90.63 13.08 0 -4 8 87.32 14.52 0 -4 8 97.04 7.79 0 4 8 85.18 12.46 0 -4 8 94.51 7.80 0 -4 8 100.24 8.15 0 -4 8 114.02 13.63 0 4 9 854.82 47.88 0 4 9 889.24 47.90 0 -4 9 898.21 52.72 0 4 9 867.45 45.57 0 -4 9 928.14 34.14 0 -4 9 868.86 34.11 0 -4 9 919.28 45.92 0 4 10 556.34 37.90 0 4 10 630.07 40.64 0 -4 10 565.79 25.01 0 -4 10 591.56 25.75 0 4 10 487.29 34.65 0 -4 10 586.54 42.69 0 -4 11 565.40 44.58 0 4 11 618.41 40.59 0 4 11 619.29 41.41 0 4 11 549.55 40.20 0 4 11 641.63 29.45 0 4 11 657.21 40.67 0 -4 11 639.71 28.22 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1 -2 3 6467.33 189.25 1 2 3 6892.40 189.64 1 -2 3 6571.58 196.03 1 2 3 6357.96 191.52 1 2 3 6096.43 190.32 1 2 3 6656.77 194.55 1 -2 4 499.94 22.69 1 2 4 477.82 22.35 1 2 4 475.21 21.67 1 2 4 466.71 22.75 1 2 4 482.29 22.99 1 -2 4 484.00 22.10 1 -2 4 478.11 20.62 1 2 4 511.00 21.01 1 -2 4 507.89 25.34 1 2 4 446.49 21.19 1 2 4 466.02 20.79 1 2 4 498.74 24.18 1 2 5 404.97 21.33 1 2 5 388.44 21.32 1 -2 5 414.08 20.69 1 -2 5 370.07 18.94 1 2 5 422.15 19.93 1 2 5 409.17 22.65 1 -2 5 386.25 21.21 1 2 5 397.80 21.49 1 -2 5 382.72 23.12 1 2 5 402.58 19.81 1 -2 6 455.29 22.02 1 2 6 418.71 21.39 1 2 6 406.72 22.02 1 2 6 420.48 23.14 1 2 6 407.32 23.36 1 -2 6 384.51 24.73 1 -2 6 389.95 21.60 1 -2 6 388.95 22.97 1 2 6 392.52 23.19 1 -2 7 1240.08 48.42 1 2 7 1256.68 48.69 1 2 7 1290.34 50.03 1 2 7 1216.67 50.25 1 2 7 1283.69 51.89 1 2 7 1208.42 49.74 1 -2 7 1197.88 54.31 1 -2 7 1269.65 49.42 1 -2 7 1215.95 51.83 1 2 7 1208.71 51.99 1 -2 8 832.47 37.93 1 2 8 826.25 37.96 1 2 8 851.87 38.83 1 2 8 768.27 38.41 1 2 8 831.19 39.02 1 2 8 839.44 40.46 1 -2 8 775.00 42.46 1 -2 8 826.75 41.47 1 2 8 799.19 41.19 1 -2 8 789.36 37.53 1 -2 9 972.99 48.82 1 2 9 944.72 48.39 1 -2 9 950.39 34.52 1 -2 9 927.25 43.92 1 2 9 1017.80 45.11 1 2 9 1029.02 45.75 1 2 9 899.33 43.97 1 2 9 948.63 45.44 1 2 9 951.08 46.34 1 -2 9 844.52 48.46 1 2 9 957.34 36.23 1 -2 9 988.37 44.40 1 2 10 724.91 40.60 1 2 10 656.41 38.06 1 -2 10 696.48 38.15 1 2 10 733.37 39.05 1 2 10 773.32 39.78 1 -2 10 749.03 28.90 1 -2 10 724.34 28.65 1 2 10 672.88 29.80 1 -2 10 691.56 29.74 1 -2 10 719.28 42.51 1 2 10 721.60 43.32 1 -2 10 685.86 28.00 1 2 10 718.75 28.25 1 -2 10 761.26 28.94 1 2 10 697.77 28.22 1 -2 11 408.29 28.80 1 2 11 394.63 28.48 1 -2 11 371.44 19.04 1 -2 11 402.20 19.45 1 -2 11 370.64 20.46 1 2 11 408.47 21.50 1 2 11 396.96 21.17 1 -2 11 429.91 33.07 1 2 11 295.55 28.74 1 -2 11 374.54 18.84 1 2 11 374.57 18.95 1 -2 11 393.86 19.48 1 2 11 410.60 19.47 1 -2 12 84.58 15.60 1 2 12 62.77 14.57 1 -2 12 74.70 8.16 1 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1 -3 -13 497.01 36.88 1 -3 -12 54.85 6.95 1 -3 -12 60.38 12.81 1 -3 -11 20.34 7.89 1 -3 -11 17.68 4.48 1 -3 -11 13.85 6.86 1 -3 -10 11.23 7.26 1 -3 -10 29.08 8.52 1 -3 -10 20.20 4.39 1 -3 -9 1090.56 50.17 1 -3 -9 1061.39 50.43 1 -3 -9 961.73 35.98 1 -3 -8 748.65 38.42 1 3 -8 729.35 34.61 1 -3 -8 774.63 39.08 1 -3 -7 630.99 33.20 1 -3 -7 626.15 32.51 1 -3 -7 667.20 33.61 1 -3 -6 485.88 24.95 1 -3 -6 493.59 27.18 1 -3 -6 507.67 27.11 1 -3 -6 494.82 26.06 1 3 -5 85.88 8.26 1 -3 -5 89.41 9.16 1 -3 -5 86.79 9.56 1 -3 -5 77.22 9.41 1 3 -4 412.66 19.76 1 -3 -4 410.05 21.88 1 -3 -4 416.33 21.88 1 -3 -4 387.98 20.51 1 -3 -3 2897.32 89.39 1 -3 -3 2719.14 86.79 1 3 -3 2705.54 89.79 1 -3 -3 2802.01 90.16 1 -3 -2 655.92 25.79 1 -3 -2 659.00 26.17 1 3 -2 699.32 26.70 1 -3 -2 609.07 29.05 1 -3 -2 696.59 28.00 1 3 -2 640.89 28.11 1 -3 -2 671.92 28.34 1 -3 -1 3893.35 117.56 1 -3 -1 3767.72 116.06 1 3 -1 3867.44 119.00 1 -3 -1 3827.34 115.89 1 3 -1 3904.11 117.27 1 -3 -1 3878.65 120.29 1 3 0 1043.75 37.39 1 -3 0 1054.20 39.36 1 3 0 1022.36 35.96 1 3 0 989.32 34.41 1 -3 0 1009.18 36.32 1 -3 0 990.59 36.04 1 3 0 1007.73 36.42 1 3 0 981.10 38.00 1 -3 0 934.19 36.27 1 -3 0 985.17 35.78 1 3 1 6096.91 175.87 1 3 1 5973.07 178.49 1 -3 1 5968.37 180.73 1 3 1 6074.80 176.66 1 3 1 5767.89 176.24 1 -3 1 6108.53 176.24 1 -3 1 5977.57 177.34 1 -3 1 6080.12 179.62 1 -3 1 5843.44 176.88 1 3 1 5955.76 179.68 1 3 1 6120.91 177.51 1 3 2 545.84 23.77 1 3 2 525.96 23.63 1 3 2 528.99 23.45 1 3 2 544.73 21.67 1 3 2 530.61 24.24 1 -3 2 532.92 25.91 1 3 2 577.39 26.06 1 -3 2 542.39 23.69 1 3 3 2888.92 92.95 1 3 3 2900.82 93.27 1 3 3 2847.15 92.27 1 3 3 2901.81 93.33 1 -3 3 3045.44 97.24 1 3 3 2935.47 95.02 1 -3 3 2820.07 92.24 1 3 4 1030.16 41.19 1 3 4 1034.06 41.53 1 3 4 993.99 39.78 1 -3 4 1014.34 44.10 1 3 4 1025.99 42.47 1 -3 4 1066.42 40.70 1 3 4 1031.46 40.52 1 3 5 3120.19 102.81 1 3 5 3269.31 105.23 1 3 5 3219.77 105.64 1 -3 5 3006.93 108.67 1 -3 5 3189.88 103.85 1 3 5 3279.23 107.06 1 3 6 35.18 7.16 1 3 6 31.93 7.18 1 3 6 29.12 6.61 1 -3 6 31.22 7.79 1 -3 6 26.42 5.74 1 3 6 26.12 6.40 1 -3 7 2164.69 87.40 1 3 7 2258.92 82.97 1 3 7 2228.40 83.55 1 -3 7 2315.79 81.60 1 3 7 2296.93 81.79 1 -3 8 131.50 17.36 1 3 8 156.97 15.53 1 -3 8 174.28 15.99 1 3 8 157.45 16.34 1 3 8 143.70 16.25 1 3 8 149.26 15.94 1 3 9 706.20 40.16 1 3 9 728.53 41.32 1 3 9 738.95 40.02 1 -3 9 742.90 45.01 1 3 9 711.22 38.75 1 3 9 747.73 30.35 1 -3 9 748.04 39.18 1 -3 9 747.73 28.92 1 -3 9 722.92 29.03 1 3 10 18.62 7.19 1 3 10 25.28 8.24 1 3 10 19.44 7.50 1 -3 10 22.96 9.27 1 -3 10 17.64 3.93 1 -3 10 33.36 5.41 1 -3 10 19.23 6.90 1 3 10 19.73 4.85 1 3 10 24.22 7.88 1 3 11 644.93 40.44 1 -3 11 647.38 28.19 1 -3 11 700.73 28.98 1 3 11 669.30 40.24 1 3 11 645.35 30.01 1 -3 12 4.46 3.29 1 -3 12 8.75 3.75 1 3 12 11.94 6.04 1 3 12 4.35 4.46 1 -3 13 313.84 18.08 1 -3 13 304.05 17.83 1 3 13 300.40 19.28 1 3 13 329.50 20.25 1 -3 14 10.97 4.11 1 3 14 25.27 6.00 1 3 14 24.36 5.79 1 -3 15 54.59 6.90 1 3 15 53.50 7.82 1 3 16 48.36 7.03 1 3 17 129.53 10.17 1 3 18 32.70 4.54 1 -4 -18 11.28 2.74 1 -4 -17 8.27 2.96 1 -4 -16 98.38 8.64 1 -4 -16 85.59 8.51 1 -4 -15 73.75 8.12 1 -4 -14 276.42 16.78 1 -4 -13 265.83 16.46 1 -4 -12 122.11 10.69 1 -4 -12 124.85 18.31 1 -4 -11 274.35 16.39 1 -4 -11 289.95 27.05 1 -4 -10 180.51 12.49 1 -4 -10 240.55 23.02 1 -4 -9 268.50 15.26 1 -4 -9 312.19 25.36 1 -4 -8 492.70 21.56 1 -4 -8 508.15 32.01 1 -4 -7 76.11 11.28 1 -4 -7 69.11 10.98 1 -4 -7 91.78 11.31 1 4 -6 1132.92 45.77 1 -4 -6 1178.86 48.68 1 -4 -6 1179.41 50.25 1 -4 -6 1157.42 49.62 1 4 -6 1119.85 49.60 1 4 -5 127.95 11.44 1 -4 -5 125.47 12.45 1 -4 -5 116.14 12.20 1 4 -5 108.33 12.00 1 4 -4 900.96 37.95 1 -4 -4 981.35 40.22 1 -4 -4 910.87 40.29 1 4 -4 919.18 40.32 1 4 -3 790.84 34.80 1 -4 -3 752.34 36.81 1 4 -3 759.57 32.87 1 -4 -3 786.55 34.31 1 4 -2 1215.68 47.77 1 4 -2 1225.12 45.78 1 -4 -2 1254.31 50.37 1 -4 -2 1239.87 47.06 1 -4 -1 289.55 16.20 1 4 -1 301.84 18.50 1 4 -1 301.59 17.78 1 4 -1 299.21 17.66 1 -4 -1 314.24 20.15 1 -4 -1 314.56 17.88 1 -4 0 1094.58 42.02 1 -4 0 1195.61 43.63 1 -4 0 1141.47 42.78 1 4 0 1148.61 44.75 1 -4 0 1148.42 47.35 1 4 0 1171.98 43.21 1 4 0 1220.00 44.74 1 4 0 1175.11 45.75 1 -4 1 583.41 26.35 1 -4 1 612.72 26.37 1 4 1 603.25 28.40 1 -4 1 595.54 30.16 1 4 1 587.85 25.95 1 -4 1 574.42 28.06 1 4 1 590.12 28.75 1 4 1 627.29 27.95 1 4 2 1316.53 49.03 1 4 2 1321.28 49.40 1 -4 2 1360.01 49.57 1 4 2 1327.02 47.21 1 4 2 1346.50 51.29 1 -4 2 1336.21 52.50 1 4 2 1367.21 52.35 1 4 2 1346.40 50.64 1 4 3 274.91 17.38 1 4 3 257.75 16.91 1 -4 3 241.36 16.22 1 4 3 257.80 17.53 1 -4 3 246.31 18.60 1 4 3 233.06 17.38 1 4 3 245.80 16.94 1 4 4 1230.47 50.24 1 4 4 1262.31 50.83 1 -4 4 1238.28 49.49 1 4 4 1279.61 50.85 1 -4 4 1278.29 54.59 1 4 4 1300.46 52.35 1 4 4 1280.51 50.46 1 4 5 137.21 13.23 1 4 5 162.12 15.26 1 4 5 124.13 13.06 1 4 5 142.90 14.01 1 -4 5 131.46 12.73 1 -4 5 148.55 16.25 1 4 6 881.61 43.17 1 -4 6 839.92 45.73 1 4 6 861.19 42.27 1 4 6 959.94 43.96 1 -4 6 848.55 40.45 1 4 6 924.17 41.59 1 -4 7 150.72 18.48 1 4 7 141.88 15.55 1 4 7 137.21 15.85 1 -4 7 126.56 13.98 1 4 7 146.19 14.96 1 4 8 147.60 15.86 1 4 8 134.01 15.96 1 4 8 122.99 15.91 1 4 8 165.27 17.80 1 -4 8 138.40 18.72 1 -4 8 112.32 13.89 1 -4 8 136.96 9.84 1 -4 8 111.18 8.93 1 4 9 223.29 20.98 1 4 9 210.73 21.33 1 4 9 177.61 20.13 1 4 9 174.31 19.45 1 -4 9 192.55 23.14 1 -4 9 197.17 19.24 1 -4 9 171.42 11.61 1 -4 9 167.67 11.83 1 4 10 659.05 40.05 1 4 10 668.80 41.08 1 4 10 630.98 40.84 1 4 10 630.91 41.68 1 -4 10 703.73 47.94 1 -4 10 667.73 28.30 1 -4 10 678.41 28.75 1 -4 10 650.92 39.42 1 -4 11 160.12 23.42 1 4 11 176.55 20.34 1 4 11 158.69 13.18 1 -4 11 196.61 13.57 1 -4 11 199.51 13.30 1 4 11 176.66 20.80 1 4 11 189.63 22.04 1 4 12 174.08 14.00 1 4 12 191.64 14.64 1 -4 12 183.00 13.53 1 -4 12 211.32 14.10 1 4 13 108.94 11.14 1 4 13 127.45 12.00 1 -4 13 140.36 11.69 1 -4 13 153.26 11.81 1 4 14 178.36 14.00 1 -4 14 165.76 12.66 1 -4 14 169.95 12.86 1 4 15 56.74 7.65 1 -4 15 39.43 6.27 1 4 16 72.32 8.00 1 4 17 3.22 2.51 1 -5 -17 237.74 12.57 1 -5 -17 245.56 12.41 1 -5 -16 80.21 7.46 1 -5 -16 68.92 7.04 1 -5 -15 94.14 8.98 1 -5 -15 123.10 10.11 1 -5 -14 23.30 5.41 1 -5 -14 22.36 5.03 1 -5 -13 192.28 13.86 1 -5 -12 42.08 6.67 1 -5 -11 447.86 22.87 1 -5 -10 309.10 17.73 1 -5 -9 29.74 5.09 1 -5 -9 14.67 4.22 1 -5 -8 220.94 13.58 1 -5 -8 262.14 21.90 1 -5 -8 237.68 14.29 1 -5 -7 1444.51 49.47 1 -5 -7 1428.37 49.56 1 -5 -7 1480.52 61.94 1 5 -6 21.48 5.92 1 -5 -6 33.83 4.85 1 -5 -6 31.46 7.73 1 -5 -6 28.57 9.25 1 -5 -5 3978.95 129.77 1 5 -5 3945.97 127.32 1 -5 -5 3604.13 133.65 1 -5 -4 552.27 29.98 1 -5 -4 503.72 32.14 1 5 -4 523.74 28.30 1 5 -3 633.94 34.30 1 5 -3 757.84 35.35 1 -5 -3 745.48 35.56 1 -5 -3 765.97 39.60 1 5 -3 745.61 34.64 1 5 -2 190.78 16.05 1 5 -2 172.19 14.43 1 -5 -2 171.42 17.13 1 5 -2 177.60 14.61 1 5 -2 177.59 15.03 1 -5 -2 186.84 15.26 1 5 -1 22.50 5.74 1 -5 -1 16.35 6.41 1 -5 -1 20.23 5.57 1 5 -1 27.76 6.42 1 5 -1 33.38 7.29 1 5 -1 34.26 6.41 1 5 0 819.68 39.15 1 -5 0 898.93 38.04 1 5 0 863.04 39.26 1 -5 0 877.73 42.63 1 5 0 885.65 37.48 1 5 0 848.19 38.70 1 5 1 1641.20 60.09 1 5 1 1698.74 64.29 1 -5 1 1694.66 67.73 1 5 1 1677.68 64.03 1 -5 1 1605.77 59.90 1 5 1 1683.88 63.43 1 5 2 102.59 11.63 1 5 2 90.48 11.50 1 -5 2 94.44 10.23 1 5 2 94.62 11.35 1 5 3 322.91 22.34 1 -5 3 346.33 21.46 1 5 3 327.95 22.77 1 5 3 325.87 22.68 1 -5 3 342.32 24.13 1 5 4 262.82 19.48 1 -5 4 218.65 17.69 1 5 4 251.77 19.60 1 5 4 254.48 19.97 1 5 4 210.87 18.61 1 -5 4 220.48 20.54 1 -5 5 335.30 23.29 1 5 5 361.48 24.87 1 5 5 321.73 23.72 1 5 5 350.30 24.58 1 5 5 358.44 23.80 1 5 5 360.28 25.40 1 -5 5 353.67 27.56 1 5 6 543.54 33.88 1 -5 6 584.78 23.55 1 5 6 535.84 33.64 1 5 6 586.01 34.57 1 5 6 535.15 31.93 1 -5 6 566.87 23.70 1 -5 6 591.52 38.48 1 5 6 582.20 33.58 1 -5 6 566.45 32.78 1 -5 7 155.99 20.45 1 -5 7 194.99 12.03 1 -5 7 178.75 11.60 1 -5 7 180.27 11.48 1 5 7 192.30 18.61 1 5 7 165.05 18.13 1 5 7 163.95 18.36 1 -5 7 194.39 18.39 1 -5 8 29.83 10.69 1 -5 8 25.77 4.73 1 -5 8 34.16 5.15 1 -5 8 27.62 4.89 1 5 8 43.66 9.87 1 5 8 36.99 9.50 1 5 8 22.84 7.95 1 5 8 21.31 7.96 1 -5 8 49.17 9.72 1 -5 9 58.82 14.15 1 -5 9 84.91 8.53 1 -5 9 68.13 7.57 1 5 9 70.41 12.68 1 5 9 63.22 13.14 1 5 9 79.43 13.82 1 -5 9 75.61 12.89 1 -5 10 84.80 17.18 1 -5 10 92.82 14.78 1 5 10 63.70 13.00 1 5 10 125.02 18.01 1 5 10 90.07 15.54 1 -5 10 93.55 9.10 1 -5 10 82.64 8.80 1 -5 11 59.66 7.70 1 -5 11 59.09 7.52 1 -5 12 87.86 8.96 1 -5 12 79.27 8.99 1 -5 13 147.94 12.01 1 -5 13 124.22 10.76 1 -5 14 0.89 2.63 1 -5 14 4.23 2.83 1 -6 -16 7.05 2.66 1 -6 -16 3.89 2.58 1 -6 -15 65.19 6.93 1 -6 -15 59.84 6.80 1 -6 -14 159.45 12.08 1 -6 -14 176.77 12.12 1 -6 -13 102.18 9.78 1 -6 -13 114.82 9.98 1 -6 -12 169.74 13.08 1 -6 -12 161.60 12.30 1 -6 -11 218.45 15.16 1 -6 -11 205.86 14.21 1 -6 -10 249.30 16.19 1 -6 -10 274.89 16.47 1 -6 -9 23.41 5.34 1 -6 -9 30.71 5.60 1 -6 -8 63.35 7.45 1 -6 -8 62.54 7.53 1 -6 -8 59.85 11.85 1 -6 -8 62.16 13.85 1 -6 -7 298.56 16.48 1 -6 -7 278.05 24.13 1 -6 -7 244.54 26.02 1 -6 -7 270.28 15.85 1 -6 -6 866.68 44.49 1 6 -6 748.29 40.30 1 -6 -6 770.35 47.36 1 -6 -6 830.84 32.24 1 6 -6 800.11 42.62 1 -6 -6 780.31 31.42 1 -6 -5 6.53 3.25 1 -6 -5 3.82 4.18 1 6 -5 9.05 5.37 1 -6 -5 7.37 6.21 1 6 -5 10.37 5.57 1 -6 -4 135.50 15.27 1 6 -4 148.63 16.22 1 6 -4 149.44 15.45 1 -6 -4 111.60 16.13 1 -6 -4 131.94 9.94 1 -6 -3 54.98 6.22 1 6 -3 51.01 9.14 1 6 -3 61.33 10.21 1 -6 -3 56.23 9.98 1 -6 -3 46.69 10.05 1 6 -2 164.36 16.63 1 -6 -2 185.04 17.13 1 6 -2 165.38 15.85 1 6 -2 161.41 16.04 1 -6 -2 180.78 19.05 1 6 -1 341.30 24.17 1 -6 -1 348.96 23.30 1 6 -1 346.20 23.19 1 6 -1 330.02 23.70 1 -6 -1 355.70 27.54 1 6 0 195.06 17.93 1 6 0 187.33 16.56 1 6 0 202.83 18.45 1 -6 0 195.97 20.60 1 6 1 2877.24 102.84 1 6 1 2785.10 97.77 1 6 1 2980.70 104.18 1 -6 1 2798.84 107.72 1 -6 2 560.62 23.36 1 6 2 489.87 31.63 1 6 2 541.24 32.71 1 -6 3 562.29 24.12 1 -6 3 595.86 24.31 1 6 3 518.78 33.61 1 6 3 569.85 34.19 1 6 4 862.98 45.45 1 -6 4 830.64 32.55 1 -6 4 853.74 41.93 1 -6 4 856.00 32.50 1 6 4 789.67 43.23 1 -6 5 205.84 19.06 1 -6 5 171.61 20.58 1 -6 5 185.53 12.31 1 -6 5 186.43 12.06 1 6 5 173.20 18.74 1 6 6 248.04 23.35 1 6 6 276.73 22.96 1 -6 6 227.69 20.87 1 -6 6 232.30 14.09 1 -6 6 211.97 23.86 1 -6 6 221.84 13.61 1 6 6 209.24 21.13 1 6 7 1159.39 55.26 1 -6 7 1125.95 54.52 1 -6 7 1081.71 40.31 1 -6 7 1153.11 62.69 1 -6 7 1079.44 41.17 1 6 7 1084.86 55.97 1 6 7 1075.40 56.10 1 6 8 141.45 17.86 1 -6 8 168.16 19.68 1 -6 8 192.25 12.59 1 -6 8 165.68 12.04 1 -6 8 153.03 22.16 1 -6 8 173.48 12.49 1 6 8 159.37 19.80 1 6 8 190.31 22.20 1 6 9 413.23 32.09 1 6 9 401.52 32.88 1 6 9 366.04 31.66 1 -6 9 399.81 20.27 1 -6 9 400.74 20.68 1 -6 9 369.01 30.20 1 -6 9 427.62 38.33 1 -6 9 379.13 20.19 1 -6 10 143.98 11.46 1 -6 10 121.61 10.69 1 -6 10 146.64 11.68 1 -6 11 14.31 4.20 1 -6 11 17.91 4.69 1 -6 12 77.03 8.69 1 -6 12 72.12 8.13 1 -6 13 93.76 8.99 1 -6 13 114.35 10.06 1 -6 14 46.10 6.36 1 -7 -15 27.84 4.35 1 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40.82 2 2 -7 857.46 37.18 2 -2 -7 875.52 39.14 2 -2 -6 588.06 27.30 2 2 -6 548.02 27.18 2 -2 -6 521.86 28.80 2 2 -6 529.22 25.78 2 -2 -6 602.74 28.50 2 -2 -5 1067.41 40.17 2 2 -5 1052.84 40.53 2 -2 -5 1030.59 42.88 2 2 -5 980.75 37.44 2 -2 -5 1089.45 41.65 2 -2 -4 3138.96 97.52 2 2 -4 3212.59 98.15 2 -2 -4 2995.28 100.64 2 2 -4 3103.70 96.24 2 -2 -3 858.94 31.68 2 2 -3 812.01 34.17 2 2 -3 866.45 32.11 2 2 -3 849.82 31.44 2 -2 -3 847.78 34.50 2 -2 -2 3248.38 101.61 2 2 -2 3353.67 101.97 2 2 -2 3311.79 104.86 2 -2 -2 3575.52 105.34 2 2 -2 3468.47 102.38 2 2 -2 3311.73 99.74 2 -2 -2 3272.53 103.33 2 2 -2 3432.89 101.59 2 -2 -1 1223.12 42.52 2 -2 -1 1222.79 41.56 2 2 -1 1162.54 40.58 2 -2 -1 1231.53 41.89 2 2 -1 1176.95 40.33 2 -2 -1 1188.49 39.60 2 2 -1 1202.54 39.71 2 2 -1 1165.93 42.67 2 2 -1 1126.60 38.03 2 2 0 260.98 12.73 2 2 0 272.90 13.24 2 -2 0 254.33 14.22 2 -2 0 303.57 15.23 2 -2 0 272.21 13.63 2 2 0 274.48 13.35 2 -2 0 273.73 14.41 2 2 0 242.95 13.69 2 -2 0 274.52 12.70 2 2 0 282.22 15.57 2 2 0 284.62 12.79 2 2 1 107.17 9.51 2 2 1 120.90 8.40 2 2 1 108.02 8.22 2 -2 1 105.60 8.37 2 -2 1 117.55 8.97 2 2 1 113.45 7.16 2 2 1 99.40 6.95 2 -2 1 126.13 7.95 2 -2 1 101.56 7.14 2 2 1 110.15 7.62 2 2 1 102.64 8.48 2 2 2 1430.48 46.16 2 2 2 1387.21 48.32 2 2 2 1436.08 48.94 2 2 2 1323.59 48.71 2 -2 2 1347.74 48.36 2 -2 2 1363.68 46.31 2 2 2 1467.90 46.59 2 2 2 1445.18 51.24 2 -2 2 1469.49 49.22 2 2 3 2086.11 70.19 2 -2 3 2105.26 69.53 2 2 3 2114.42 72.34 2 2 3 2102.64 70.15 2 2 3 2162.86 70.18 2 -2 3 2116.53 67.77 2 2 3 2099.06 67.58 2 2 4 1431.40 53.09 2 -2 4 1473.49 52.69 2 2 4 1484.38 56.18 2 -2 4 1452.04 57.56 2 2 4 1514.70 55.24 2 2 4 1504.98 54.15 2 2 4 1575.71 54.26 2 2 4 1473.58 51.48 2 -2 4 1470.52 51.30 2 2 5 249.15 16.06 2 -2 5 256.54 19.29 2 -2 5 241.91 15.15 2 2 5 227.71 14.79 2 -2 5 233.27 15.45 2 2 5 268.37 17.36 2 2 5 245.20 16.58 2 2 5 229.22 16.06 2 2 5 244.62 17.81 2 -2 6 215.39 15.08 2 2 6 214.41 14.99 2 2 6 198.27 15.54 2 2 6 181.06 15.01 2 -2 6 184.37 17.49 2 -2 6 181.79 14.29 2 -2 6 191.63 16.26 2 2 6 202.64 16.70 2 -2 7 13.39 6.63 2 2 7 15.33 4.72 2 -2 7 6.16 3.66 2 2 7 14.70 4.52 2 2 7 6.87 4.08 2 2 7 8.43 4.54 2 -2 7 12.72 5.51 2 2 7 14.60 6.16 2 -2 7 13.58 4.56 2 -2 8 1379.19 54.81 2 2 8 1304.55 53.92 2 2 8 1332.37 54.63 2 -2 8 1229.45 52.83 2 -2 8 1298.37 58.33 2 2 8 1259.71 57.93 2 2 8 1316.29 55.34 2 2 8 1355.85 56.27 2 2 9 437.51 28.21 2 2 9 422.84 28.28 2 -2 9 405.14 26.85 2 2 9 454.75 27.99 2 2 9 427.53 27.37 2 -2 9 388.62 29.66 2 2 9 416.49 30.44 2 2 9 423.37 19.26 2 -2 9 437.56 19.42 2 -2 9 442.38 19.50 2 -2 9 416.50 19.42 2 2 9 414.09 20.39 2 -2 9 415.06 20.63 2 2 9 478.40 21.56 2 -2 10 315.54 16.59 2 -2 10 295.07 16.02 2 2 10 326.71 17.72 2 2 10 312.09 17.83 2 -2 10 282.55 17.21 2 2 10 282.68 17.24 2 -2 10 329.26 24.93 2 2 10 331.43 24.75 2 2 10 326.30 16.52 2 -2 10 311.61 16.22 2 2 10 308.14 16.05 2 -2 10 316.14 16.40 2 -2 11 209.36 13.22 2 -2 11 183.81 12.54 2 -2 11 196.81 14.29 2 2 11 178.39 13.79 2 2 11 185.57 13.74 2 2 11 200.72 14.47 2 -2 11 171.14 18.72 2 2 11 179.38 19.61 2 -2 11 216.46 13.36 2 2 11 196.61 12.73 2 -2 11 174.36 12.36 2 2 11 201.87 12.90 2 -2 12 18.78 6.67 2 -2 12 22.83 5.00 2 -2 12 20.76 4.69 2 2 12 32.41 5.69 2 2 12 27.21 5.25 2 -2 12 24.50 5.67 2 2 12 30.57 6.51 2 -2 12 18.49 4.37 2 2 12 20.52 5.91 2 2 12 28.97 6.03 2 2 13 20.52 4.55 2 -2 13 19.55 4.86 2 2 13 25.22 5.07 2 -2 13 22.75 5.42 2 -2 13 13.42 4.83 2 2 13 25.22 6.50 2 -2 13 24.54 5.11 2 2 13 17.38 5.08 2 2 14 96.53 9.18 2 -2 14 82.99 8.69 2 2 14 75.00 8.37 2 -2 14 82.08 8.77 2 2 14 75.79 9.76 2 -2 14 95.29 10.54 2 2 14 99.04 10.30 2 -2 15 19.81 4.64 2 2 15 16.84 4.47 2 -2 15 15.21 4.29 2 2 15 9.02 3.83 2 2 15 15.18 4.96 2 -2 15 14.86 5.21 2 2 15 14.42 4.71 2 -2 16 15.14 4.06 2 2 16 22.99 4.78 2 -2 16 24.61 4.57 2 2 16 33.84 5.19 2 2 16 23.86 5.50 2 -2 16 19.74 5.22 2 2 16 28.26 5.80 2 -2 17 37.18 4.89 2 2 17 39.04 5.03 2 2 17 35.80 5.55 2 2 18 42.25 4.43 2 2 18 45.43 5.18 2 -3 -18 4.81 2.39 2 -3 -17 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255.82 20.10 2 -3 8 225.98 12.82 2 -3 8 222.06 12.87 2 3 8 252.96 20.11 2 3 8 209.92 13.23 2 3 8 230.90 19.93 2 3 8 198.45 18.90 2 -3 9 247.16 20.87 2 -3 9 241.56 13.81 2 -3 9 230.92 13.73 2 3 9 259.25 21.78 2 3 9 240.62 21.52 2 3 9 251.66 22.23 2 3 9 209.45 13.80 2 3 9 236.19 14.73 2 -3 10 646.18 27.35 2 -3 10 608.70 26.56 2 3 10 653.13 38.27 2 3 10 591.90 37.43 2 3 10 616.10 38.98 2 3 10 624.10 27.97 2 3 10 621.70 28.35 2 -3 11 127.01 10.49 2 -3 11 109.80 10.00 2 3 11 151.86 18.35 2 3 11 130.08 11.41 2 3 11 134.63 11.83 2 3 11 133.14 17.53 2 -3 12 736.77 31.03 2 -3 12 735.10 31.08 2 3 12 688.63 32.02 2 -3 13 38.93 6.12 2 -3 13 28.32 5.37 2 3 13 31.35 6.40 2 -3 14 203.95 13.65 2 -3 14 203.28 13.72 2 -3 15 31.03 5.35 2 3 15 37.32 6.58 2 3 16 24.60 5.02 2 3 17 33.67 5.05 2 -4 -18 33.51 4.22 2 -4 -17 8.30 3.13 2 -4 -16 59.31 7.13 2 -4 -15 123.71 10.17 2 -4 -15 94.78 9.49 2 -4 -14 19.84 5.37 2 -4 -14 20.49 5.00 2 -4 -13 413.94 21.56 2 4 -12 197.87 24.52 2 -4 -12 222.28 14.73 2 4 -11 85.87 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16.15 2 -4 1 1315.91 48.81 2 -4 1 1234.40 48.35 2 4 1 1260.93 51.38 2 4 1 1288.22 47.61 2 4 1 1192.29 48.69 2 -4 1 1268.61 51.90 2 4 1 1223.63 45.94 2 4 2 1163.57 48.77 2 4 2 1132.78 46.83 2 -4 2 1143.65 45.40 2 4 2 1121.95 44.51 2 4 2 1154.27 44.50 2 4 2 1100.59 44.10 2 4 2 1130.73 42.39 2 4 3 1694.82 64.67 2 4 3 1774.25 67.41 2 -4 3 1717.42 68.20 2 4 3 1755.05 63.62 2 4 3 1708.48 63.11 2 -4 3 1706.30 63.33 2 4 4 1354.37 55.05 2 4 4 1394.28 57.85 2 -4 4 1336.94 59.22 2 4 4 1315.17 54.18 2 4 4 1406.53 54.97 2 -4 4 1409.12 54.71 2 4 5 145.73 14.62 2 4 5 127.15 14.67 2 -4 5 146.95 17.20 2 4 5 139.52 14.31 2 4 5 134.52 13.86 2 -4 5 121.62 13.07 2 4 6 332.25 23.29 2 4 6 289.03 22.60 2 4 6 315.88 23.36 2 4 6 303.08 24.35 2 -4 6 329.16 23.09 2 -4 7 632.46 41.04 2 4 7 693.45 38.00 2 4 7 608.32 36.11 2 -4 7 675.19 36.13 2 -4 7 634.91 25.98 2 -4 7 630.98 25.72 2 4 7 636.51 35.38 2 4 8 245.59 22.29 2 4 8 272.29 23.67 2 -4 8 268.48 22.03 2 -4 8 237.98 14.30 2 -4 8 269.63 14.98 2 4 8 262.83 22.12 2 4 9 303.32 25.31 2 4 9 230.05 23.21 2 -4 9 218.45 20.99 2 -4 9 244.77 14.92 2 -4 9 249.74 14.69 2 4 9 243.22 22.22 2 4 10 34.19 9.57 2 4 10 35.28 9.61 2 -4 10 35.51 9.14 2 -4 10 35.05 5.82 2 -4 10 36.46 5.89 2 4 10 43.66 10.11 2 -4 11 327.97 18.70 2 -4 11 323.13 18.31 2 4 11 338.37 28.58 2 4 11 352.75 29.86 2 4 11 357.75 30.48 2 -4 12 56.93 7.57 2 -4 12 49.49 7.13 2 4 12 43.20 7.31 2 -4 13 27.36 5.53 2 -4 13 38.47 6.38 2 4 13 24.77 5.75 2 -4 14 218.51 14.63 2 -4 14 226.56 14.76 2 -4 15 99.68 8.80 2 4 15 73.82 8.55 2 4 16 77.26 7.87 2 4 17 55.30 5.64 2 -5 -17 18.85 3.73 2 -5 -16 55.86 6.47 2 -5 -16 53.08 6.36 2 -5 -15 38.28 6.03 2 -5 -15 47.81 6.53 2 -5 -14 43.29 6.87 2 -5 -14 49.49 7.00 2 -5 -13 48.25 6.94 2 -5 -13 66.77 8.17 2 -5 -12 290.99 17.04 2 -5 -12 215.61 15.53 2 -5 -11 143.69 11.75 2 -5 -11 122.74 10.99 2 5 -10 241.59 25.49 2 5 -10 214.68 21.36 2 -5 -10 289.43 16.65 2 -5 -10 283.71 16.69 2 5 -9 42.49 10.75 2 -5 -9 37.36 5.76 2 -5 -9 30.79 5.74 2 5 -9 30.56 7.69 2 5 -8 399.51 30.26 2 -5 -8 398.39 29.60 2 -5 -8 397.41 19.87 2 -5 -8 416.91 19.77 2 -5 -7 145.73 10.56 2 -5 -7 134.63 10.00 2 5 -7 117.71 15.73 2 -5 -7 149.03 17.12 2 -5 -7 133.05 17.50 2 -5 -6 2599.25 81.11 2 -5 -6 2477.86 80.46 2 -5 -6 2646.43 99.47 2 5 -6 2605.66 91.30 2 5 -6 2420.37 95.49 2 -5 -6 2737.00 97.36 2 5 -5 112.31 14.08 2 5 -5 109.82 12.20 2 -5 -5 119.89 15.36 2 -5 -5 102.89 12.93 2 5 -4 2507.49 94.05 2 -5 -4 2457.76 95.49 2 5 -4 2539.33 89.82 2 -5 -4 2785.14 93.92 2 -5 -3 1.78 3.89 2 5 -3 4.93 4.87 2 5 -3 9.04 4.47 2 -5 -3 7.23 3.88 2 5 -2 2641.89 96.60 2 5 -2 2747.37 93.87 2 5 -2 2661.32 93.08 2 -5 -2 2832.84 99.37 2 5 -2 2685.54 92.67 2 -5 -2 2760.40 94.78 2 5 -1 822.87 40.61 2 5 -1 839.62 37.91 2 5 -1 797.17 37.88 2 -5 -1 829.68 41.55 2 5 -1 831.49 37.04 2 5 0 693.33 36.88 2 -5 0 669.49 33.14 2 5 0 718.49 34.54 2 5 0 723.93 33.43 2 5 0 755.00 36.11 2 -5 0 774.27 39.46 2 5 1 565.52 31.95 2 -5 1 498.74 27.74 2 5 1 527.81 28.56 2 5 1 539.98 30.19 2 5 1 551.48 27.36 2 -5 1 505.20 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1826.94 58.03 3 -2 -3 1711.95 60.57 3 2 -2 460.34 19.88 3 2 -2 467.99 21.05 3 2 -2 440.86 21.46 3 -2 -2 458.84 21.63 3 2 -2 433.31 22.92 3 2 -2 464.05 21.33 3 -2 -2 464.07 22.78 3 -2 -1 1155.53 43.93 3 -2 -1 1145.25 41.83 3 2 -1 1104.89 41.01 3 2 -1 1140.38 41.89 3 2 -1 1113.93 40.07 3 2 -1 1162.51 41.35 3 -2 -1 1113.19 41.00 3 2 -1 1139.95 43.87 3 2 -1 1146.79 39.20 3 -2 0 1443.55 52.66 3 -2 0 1465.39 49.74 3 2 0 1493.70 50.74 3 2 0 1450.63 51.98 3 -2 0 1503.45 51.32 3 2 0 1453.72 53.53 3 -2 0 1498.56 50.66 3 2 0 1524.81 50.46 3 2 0 1442.84 49.58 3 -2 0 1386.03 50.12 3 2 1 5538.99 163.55 3 -2 1 5571.19 165.25 3 2 1 5576.32 164.30 3 -2 1 5344.10 164.98 3 2 1 5363.07 162.89 3 2 1 5397.98 165.45 3 -2 1 5315.26 162.62 3 2 1 5516.79 162.46 3 -2 1 5544.92 162.74 3 2 1 5551.27 167.54 3 -2 1 5364.54 165.16 3 2 2 800.19 33.35 3 -2 2 819.16 35.12 3 2 2 786.41 33.54 3 -2 2 842.19 34.14 3 2 2 815.70 32.28 3 2 2 789.10 34.40 3 -2 2 871.98 34.65 3 -2 2 862.15 32.79 3 2 2 831.98 32.30 3 2 2 870.84 36.74 3 -2 3 939.33 38.62 3 -2 3 1003.12 38.09 3 2 3 980.37 37.54 3 -2 3 1012.63 39.50 3 2 3 1034.62 42.49 3 2 3 990.53 39.33 3 2 3 922.24 38.94 3 2 3 942.48 39.85 3 2 4 339.93 21.00 3 2 4 405.89 23.88 3 -2 4 378.94 20.12 3 2 4 365.72 19.82 3 -2 4 349.88 20.13 3 2 4 338.89 22.53 3 2 4 340.13 20.98 3 2 4 396.45 21.89 3 2 5 657.84 32.72 3 2 5 713.11 35.63 3 2 5 680.51 31.33 3 -2 5 650.70 31.04 3 -2 5 682.31 31.81 3 2 5 699.05 33.35 3 2 5 733.64 36.07 3 2 5 716.09 33.77 3 2 6 536.48 29.50 3 -2 6 526.35 28.13 3 2 6 564.57 28.78 3 2 6 580.50 30.65 3 2 6 585.00 31.98 3 2 6 574.54 30.69 3 2 6 560.18 32.43 3 -2 6 546.54 28.42 3 -2 7 1721.21 67.59 3 2 7 1765.14 67.72 3 2 7 1880.38 70.55 3 2 7 1826.52 70.61 3 2 8 398.72 27.53 3 2 8 462.04 29.34 3 -2 8 468.69 28.53 3 2 8 468.13 28.33 3 2 8 526.65 29.56 3 2 8 461.47 21.06 3 -2 8 438.41 21.14 3 -2 8 475.47 20.40 3 -2 8 421.98 19.42 3 2 9 271.18 22.98 3 2 9 293.28 23.83 3 -2 9 290.86 15.62 3 -2 9 279.01 22.74 3 2 9 313.39 23.61 3 -2 9 294.95 15.57 3 2 9 293.64 15.37 3 2 9 295.80 16.65 3 -2 9 281.31 16.79 3 2 9 313.44 17.57 3 2 10 327.10 18.47 3 -2 10 351.87 19.43 3 -2 10 288.28 16.58 3 2 10 341.57 17.38 3 2 10 318.80 17.29 3 -2 10 350.48 17.81 3 -2 10 350.11 26.74 3 2 10 352.70 26.73 3 2 10 317.46 18.83 3 -2 11 211.52 21.52 3 2 11 206.45 21.33 3 -2 11 209.69 15.40 3 2 11 230.70 16.00 3 2 11 233.77 15.63 3 -2 11 190.73 13.36 3 2 11 247.87 14.66 3 -2 11 231.54 14.43 3 2 11 212.01 13.92 3 -2 12 73.44 9.00 3 2 12 64.03 8.88 3 2 12 79.75 9.28 3 -2 12 76.89 8.37 3 2 12 80.78 8.34 3 -2 12 73.61 8.27 3 2 12 70.25 8.08 3 2 13 160.56 13.81 3 -2 13 146.40 12.99 3 2 13 138.35 12.53 3 -2 13 178.24 12.57 3 2 13 142.66 11.33 3 2 13 149.51 11.68 3 -2 13 133.13 11.28 3 -2 14 31.45 6.60 3 2 14 30.03 6.70 3 2 14 15.63 5.06 3 -2 14 28.08 5.47 3 -2 14 18.17 4.55 3 2 14 20.92 4.53 3 2 14 24.28 5.06 3 2 15 58.23 7.58 3 2 15 58.51 6.93 3 -2 15 49.40 6.61 3 2 15 42.59 5.87 3 -2 15 56.04 6.81 3 2 16 10.61 4.14 3 -2 16 15.41 3.85 3 2 16 12.73 3.46 3 -2 16 16.06 3.85 3 2 16 12.86 3.47 3 2 17 26.20 4.54 3 2 17 19.14 3.45 3 -3 -18 4.06 2.40 3 -3 -17 22.19 4.21 3 -3 -16 99.12 9.19 3 -3 -15 524.94 25.03 3 -3 -14 70.52 8.42 3 -3 -13 1285.20 48.16 3 -3 -12 102.54 9.83 3 -3 -11 41.97 6.24 3 3 -11 37.90 9.10 3 3 -10 92.98 12.90 3 -3 -10 101.45 15.33 3 -3 -10 109.20 9.11 3 3 -9 20.32 6.46 3 -3 -9 37.01 9.75 3 -3 -9 23.72 4.38 3 -3 -8 53.50 11.14 3 3 -8 43.54 8.16 3 3 -7 524.13 32.93 3 3 -7 559.12 29.41 3 -3 -7 547.33 32.80 3 3 -6 263.39 21.01 3 3 -6 304.00 19.25 3 3 -6 288.37 18.06 3 -3 -6 274.01 21.25 3 3 -5 545.12 30.20 3 3 -5 522.20 26.04 3 -3 -5 565.35 30.89 3 -3 -4 374.11 21.99 3 3 -4 360.86 23.31 3 3 -4 413.28 21.43 3 -3 -4 394.41 23.97 3 -3 -3 169.19 13.60 3 3 -3 167.34 14.89 3 -3 -3 176.45 14.54 3 3 -3 184.83 13.11 3 -3 -3 189.52 15.04 3 -3 -2 71.20 8.42 3 3 -2 81.15 8.45 3 3 -2 66.93 9.18 3 3 -2 73.38 8.14 3 -3 -2 78.94 9.12 3 -3 -2 85.48 9.51 3 -3 -1 568.01 27.92 3 -3 -1 567.05 27.71 3 -3 -1 541.44 26.55 3 3 -1 624.88 27.31 3 -3 -1 568.48 26.66 3 3 -1 562.33 25.76 3 3 -1 537.85 28.78 3 -3 0 451.69 23.45 3 -3 0 473.49 24.19 3 -3 0 446.53 23.16 3 3 0 463.93 23.28 3 3 0 381.06 20.18 3 3 0 437.68 21.53 3 3 0 418.71 24.44 3 -3 1 895.63 36.78 3 -3 1 847.27 36.58 3 3 1 807.44 35.80 3 3 1 866.18 34.14 3 3 1 785.80 33.82 3 3 1 822.11 33.57 3 3 1 852.22 38.42 3 -3 2 199.93 15.20 3 -3 2 236.67 16.45 3 3 2 213.13 16.06 3 3 2 234.61 15.40 3 3 2 238.93 15.87 3 3 2 233.10 14.39 3 3 2 222.75 17.67 3 3 3 486.06 27.01 3 3 3 514.37 26.50 3 3 3 552.23 27.43 3 -3 3 547.81 27.29 3 3 3 500.34 28.96 3 3 4 114.24 13.03 3 3 4 97.61 11.52 3 -3 4 92.72 10.46 3 3 4 94.92 10.80 3 3 4 81.01 10.30 3 3 4 94.80 11.81 3 -3 5 399.71 24.37 3 3 5 416.66 25.38 3 3 5 412.91 25.35 3 3 5 441.55 27.97 3 3 5 368.75 24.28 3 -3 6 461.45 27.47 3 3 6 513.62 29.74 3 3 6 493.26 29.52 3 3 6 488.26 31.33 3 3 6 465.64 28.36 3 -3 7 1588.26 64.33 3 -3 7 1595.33 53.03 3 -3 7 1621.83 53.50 3 3 7 1508.20 65.02 3 3 7 1611.54 66.88 3 3 8 890.99 43.83 3 -3 8 841.94 42.42 3 3 8 843.54 44.18 3 3 8 824.41 44.18 3 -3 8 859.27 32.26 3 -3 8 797.89 32.19 3 3 9 731.69 41.68 3 3 9 745.52 42.40 3 -3 9 725.57 29.37 3 -3 9 690.66 29.33 3 3 9 708.30 40.10 3 3 10 83.54 9.01 3 -3 10 86.66 8.41 3 -3 10 86.68 9.00 3 3 10 83.15 13.80 3 3 10 92.65 14.98 3 -3 11 210.83 13.90 3 -3 11 218.76 14.31 3 3 11 186.68 14.19 3 -3 12 106.41 9.84 3 -3 12 120.51 10.30 3 3 12 94.66 10.11 3 -3 13 186.77 12.94 3 -3 13 160.41 12.30 3 3 13 161.78 13.25 3 -3 14 3.30 2.76 3 -3 14 5.78 3.22 3 3 14 3.97 4.07 3 3 15 87.15 9.18 3 3 16 11.10 3.64 3 3 17 22.88 3.91 3 -4 -18 9.88 2.55 3 -4 -17 89.39 7.68 3 -4 -16 1.52 2.63 3 -4 -15 73.28 8.13 3 -4 -14 392.00 21.09 3 -4 -13 31.75 5.91 3 -4 -13 35.96 6.03 3 -4 -12 465.06 22.86 3 -4 -12 446.02 23.21 3 4 -11 592.03 37.02 3 -4 -11 579.45 26.30 3 -4 -11 597.15 26.81 3 4 -10 22.22 7.05 3 -4 -10 24.75 8.61 3 4 -10 27.38 9.20 3 -4 -10 40.18 6.10 3 -4 -10 39.14 6.03 3 4 -9 521.53 31.97 3 -4 -9 549.24 35.99 3 -4 -9 536.29 23.63 3 -4 -9 511.98 23.40 3 4 -8 208.41 18.15 3 -4 -8 181.63 11.71 3 -4 -8 164.70 11.32 3 4 -8 190.03 20.38 3 -4 -7 385.11 27.41 3 4 -7 338.80 23.19 3 4 -7 324.11 26.13 3 -4 -7 345.85 17.04 3 -4 -7 347.06 16.99 3 4 -6 1449.94 65.41 3 -4 -6 1544.98 64.99 3 -4 -6 1580.21 66.53 3 4 -6 1705.08 61.74 3 4 -5 399.41 27.24 3 -4 -5 445.75 28.00 3 4 -5 428.46 24.38 3 -4 -5 413.66 26.56 3 4 -4 607.55 34.03 3 -4 -4 668.64 34.14 3 4 -4 625.75 30.45 3 -4 -4 599.71 32.51 3 -4 -4 581.45 31.30 3 4 -3 212.62 18.38 3 -4 -3 218.52 17.64 3 4 -3 236.10 16.71 3 -4 -3 228.55 17.92 3 -4 -3 238.49 17.83 3 -4 -2 3.72 3.51 3 4 -2 4.64 4.37 3 4 -2 -1.09 3.39 3 -4 -2 1.28 3.43 3 4 -2 1.11 2.63 3 -4 -2 5.40 3.41 3 -4 -2 2.57 3.44 3 -4 -1 705.88 34.50 3 -4 -1 748.53 36.22 3 4 -1 738.86 34.38 3 4 -1 781.79 38.17 3 4 -1 752.98 33.53 3 -4 -1 794.69 36.17 3 -4 0 1181.41 47.72 3 -4 0 1140.04 48.80 3 4 0 1186.76 47.80 3 4 0 1164.93 50.67 3 4 0 1144.31 44.55 3 4 0 1103.92 44.81 3 -4 0 1162.42 47.94 3 -4 1 1360.77 53.41 3 -4 1 1314.68 52.51 3 4 1 1323.18 53.29 3 4 1 1298.57 49.58 3 4 1 1278.27 55.64 3 -4 2 2641.56 92.02 3 4 2 2637.39 89.79 3 4 2 2663.24 90.62 3 4 2 2724.69 96.70 3 4 2 2655.00 93.23 3 -4 3 715.06 36.27 3 4 3 777.67 36.39 3 4 3 824.12 37.57 3 4 3 846.54 41.62 3 4 3 760.94 38.02 3 -4 4 722.42 36.78 3 4 4 781.40 37.48 3 4 4 742.33 37.22 3 4 4 723.60 39.88 3 4 4 764.90 38.54 3 -4 5 659.37 34.94 3 4 5 624.26 34.42 3 4 5 665.81 35.53 3 4 5 625.02 37.51 3 4 5 634.48 35.29 3 -4 6 94.96 7.79 3 -4 6 74.28 7.14 3 -4 6 80.16 11.56 3 4 6 87.07 12.70 3 4 6 59.61 10.70 3 4 6 76.50 12.70 3 4 6 82.75 12.39 3 4 7 65.64 11.45 3 4 7 78.10 12.41 3 -4 7 62.22 10.69 3 4 7 63.95 12.83 3 -4 7 56.09 6.68 3 -4 7 79.59 7.57 3 4 8 251.57 22.61 3 -4 8 264.62 23.08 3 -4 8 279.01 15.72 3 -4 8 272.75 15.79 3 4 8 294.61 25.04 3 4 8 301.97 25.52 3 4 9 406.24 30.04 3 -4 9 401.28 29.64 3 4 9 345.85 29.30 3 4 9 389.32 30.76 3 -4 9 400.50 20.51 3 -4 9 409.39 20.33 3 4 10 190.21 21.93 3 4 10 226.94 24.02 3 -4 10 249.86 15.48 3 -4 10 249.26 15.73 3 4 10 247.98 24.27 3 -4 11 397.91 21.09 3 -4 11 379.65 20.48 3 -4 12 54.86 7.67 3 -4 12 55.57 7.31 3 -4 13 56.06 7.52 3 -4 13 55.25 7.22 3 -4 14 41.78 6.15 3 -4 14 46.48 6.36 3 4 14 40.09 6.38 3 -4 15 31.21 4.85 3 4 15 38.43 5.78 3 4 16 37.77 5.13 3 -5 -17 8.29 2.90 3 -5 -16 2.01 2.75 3 -5 -15 4.79 3.35 3 -5 -15 2.98 2.98 3 -5 -14 16.95 4.94 3 -5 -14 23.03 5.31 3 -5 -13 41.57 6.62 3 -5 -13 31.29 6.01 3 -5 -12 23.93 5.52 3 -5 -12 27.43 5.52 3 -5 -11 179.08 13.35 3 -5 -11 169.36 13.03 3 5 -10 98.83 16.81 3 5 -10 89.33 13.57 3 -5 -10 72.29 13.28 3 -5 -10 89.65 9.20 3 -5 -10 89.97 9.13 3 5 -9 548.01 39.47 3 -5 -9 579.14 38.75 3 5 -9 554.01 35.21 3 -5 -9 590.88 26.33 3 -5 -9 578.84 26.08 3 5 -8 88.51 14.68 3 -5 -8 78.56 8.19 3 -5 -8 99.94 9.16 3 5 -8 83.21 12.43 3 -5 -8 93.60 14.69 3 5 -7 951.50 51.22 3 -5 -7 934.47 50.27 3 -5 -7 961.21 36.09 3 -5 -7 961.12 36.65 3 -5 -7 991.77 50.68 3 5 -7 953.77 45.25 3 -5 -6 238.85 13.88 3 -5 -6 212.98 20.94 3 5 -6 237.80 22.48 3 -5 -6 231.30 13.39 3 -5 -6 215.13 21.04 3 5 -6 213.55 18.45 3 -5 -5 1853.82 61.45 3 -5 -5 1836.31 61.04 3 5 -5 1840.55 77.18 3 -5 -5 1868.03 76.42 3 5 -5 2030.89 73.05 3 -5 -5 1820.19 75.21 3 5 -4 55.75 10.47 3 -5 -4 41.18 9.12 3 5 -4 55.52 9.25 3 5 -3 1386.58 62.15 3 -5 -3 1424.69 61.45 3 5 -3 1469.78 58.09 3 5 -2 83.00 10.42 3 -5 -2 84.02 10.82 3 -5 -2 69.49 9.98 3 5 -2 62.59 11.15 3 -5 -2 44.25 9.93 3 -5 -1 1585.15 66.63 3 5 -1 1576.62 63.57 3 5 -1 1620.52 61.97 3 -5 -1 1637.90 63.55 3 -5 -1 1620.96 64.02 3 5 -1 1663.84 68.49 3 5 -1 1615.10 62.21 3 -5 0 601.02 32.27 3 5 0 630.20 33.72 3 -5 0 555.21 34.04 3 5 0 642.18 31.48 3 -5 0 618.44 32.98 3 5 0 617.84 35.89 3 5 1 534.59 31.72 3 5 1 596.60 30.12 3 5 1 581.86 35.21 3 -5 1 608.70 32.48 3 5 2 326.37 26.13 3 5 2 390.26 26.20 3 -5 2 372.26 24.84 3 5 3 1783.94 72.22 3 -5 3 1788.21 58.45 3 -5 3 1772.73 58.87 3 -5 3 1756.14 70.21 3 5 3 1739.31 74.50 3 5 4 29.32 7.74 3 5 4 15.09 5.45 3 -5 4 28.62 4.67 3 5 4 30.91 8.63 3 -5 4 29.74 4.89 3 -5 4 28.78 4.71 3 -5 4 19.69 6.24 3 5 4 21.38 7.80 3 5 5 74.54 11.71 3 5 5 102.53 13.85 3 -5 5 88.39 8.09 3 -5 5 82.55 7.76 3 5 5 95.81 14.96 3 -5 5 86.29 7.98 3 -5 5 96.72 8.65 3 -5 5 70.55 11.68 3 5 5 78.29 12.85 3 5 6 84.27 13.47 3 5 6 100.80 14.15 3 -5 6 95.49 8.60 3 -5 6 107.24 9.12 3 5 6 116.55 16.81 3 -5 6 95.26 8.54 3 -5 6 102.12 14.05 3 -5 6 97.28 8.71 3 5 6 104.34 15.05 3 5 7 336.78 26.42 3 -5 7 285.19 16.55 3 -5 7 288.89 16.62 3 5 7 353.06 29.89 3 5 7 315.53 26.57 3 5 7 343.55 27.59 3 -5 7 313.85 25.57 3 -5 8 39.36 6.30 3 -5 8 35.77 5.95 3 5 8 47.44 10.98 3 5 8 51.22 11.38 3 -5 8 30.11 8.35 3 5 8 46.05 10.35 3 -5 9 616.10 27.33 3 -5 9 630.61 27.89 3 5 9 579.65 39.78 3 5 9 533.18 38.83 3 5 9 531.82 37.33 3 -5 9 600.46 39.20 3 -5 10 119.36 10.80 3 -5 10 124.01 10.78 3 -5 11 485.22 23.75 3 -5 11 469.74 23.96 3 -5 12 11.30 3.95 3 -5 12 3.61 3.02 3 -5 13 13.97 4.31 3 -5 13 29.31 5.32 3 -5 14 6.12 2.99 3 -5 14 11.07 3.56 3 -5 15 5.64 2.69 3 -6 -16 81.28 6.68 3 -6 -16 76.87 6.71 3 -6 -15 71.19 7.01 3 -6 -15 85.48 7.58 3 -6 -14 182.90 12.60 3 -6 -14 207.76 13.34 3 -6 -13 257.35 15.79 3 -6 -13 256.99 15.94 3 -6 -12 124.61 11.22 3 -6 -12 117.34 10.45 3 -6 -11 461.16 23.43 3 -6 -11 432.62 22.29 3 -6 -10 16.25 4.99 3 -6 -10 8.68 4.14 3 -6 -9 257.12 16.15 3 6 -9 203.37 24.31 3 6 -9 233.91 22.75 3 -6 -8 46.81 6.82 3 6 -8 61.00 13.18 3 -6 -8 55.95 7.16 3 6 -8 38.62 9.10 3 -6 -7 162.67 12.28 3 6 -7 183.67 18.68 3 6 -7 163.86 20.73 3 -6 -7 174.02 12.48 3 -6 -6 220.32 13.83 3 -6 -6 205.72 22.46 3 6 -6 194.37 18.88 3 6 -6 171.58 20.82 3 -6 -6 198.32 13.21 3 -6 -5 479.02 22.47 3 -6 -5 466.05 33.84 3 6 -5 527.67 31.96 3 6 -5 502.35 35.42 3 -6 -5 487.60 22.75 3 -6 -4 577.34 25.01 3 -6 -4 586.77 37.83 3 6 -4 609.10 34.53 3 6 -4 606.73 34.87 3 6 -4 552.55 37.26 3 -6 -4 566.64 25.20 3 -6 -3 540.13 23.62 3 -6 -3 536.31 23.16 3 -6 -3 503.15 34.72 3 6 -3 454.12 33.41 3 6 -3 523.02 31.86 3 6 -3 477.38 30.30 3 6 -2 174.54 17.31 3 6 -2 201.29 18.12 3 -6 -2 184.59 20.49 3 -6 -2 191.44 12.31 3 6 -2 174.68 19.93 3 6 -1 419.29 27.38 3 6 -1 422.97 28.28 3 -6 -1 368.60 29.30 3 6 -1 376.61 25.56 3 -6 -1 419.39 19.36 3 -6 -1 400.88 19.52 3 6 -1 385.74 29.91 3 6 0 11.56 5.46 3 6 0 15.91 5.88 3 6 0 9.12 7.90 3 -6 0 17.58 3.95 3 -6 0 14.66 4.11 3 -6 0 17.17 3.86 3 -6 1 42.32 5.72 3 -6 1 44.33 5.78 3 -6 1 32.42 7.78 3 6 1 41.59 10.16 3 -6 1 36.82 5.26 3 -6 1 22.04 4.70 3 6 1 40.46 9.09 3 -6 2 418.33 20.65 3 -6 2 424.14 20.15 3 -6 2 452.70 29.72 3 -6 2 414.82 20.43 3 6 2 447.10 32.61 3 -6 2 464.43 21.13 3 6 2 454.64 31.24 3 -6 3 52.82 6.46 3 6 3 68.55 12.66 3 -6 3 63.10 7.20 3 -6 3 45.70 9.85 3 6 3 55.58 11.52 3 -6 3 53.17 6.71 3 -6 4 503.90 22.81 3 6 4 518.38 36.56 3 -6 4 492.60 23.32 3 -6 4 516.57 33.38 3 6 4 452.90 33.39 3 -6 4 491.25 23.11 3 -6 5 88.03 8.71 3 6 5 87.22 14.98 3 -6 5 91.11 8.96 3 -6 5 106.22 15.02 3 -6 5 92.76 9.01 3 6 5 107.45 15.80 3 -6 6 92.26 8.94 3 6 6 53.92 11.13 3 6 6 110.08 15.78 3 -6 6 77.49 8.53 3 -6 6 84.01 8.45 3 6 6 104.68 16.49 3 -6 6 87.04 8.86 3 -6 6 88.84 14.20 3 6 6 65.92 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439.18 31.83 3 -7 -4 437.13 35.34 3 -7 -4 490.79 23.35 3 7 -4 455.38 31.96 3 7 -3 286.13 24.15 3 7 -3 291.65 27.50 3 7 -3 273.74 24.37 3 -7 -3 286.23 16.82 3 -7 -3 254.17 26.25 3 7 -2 341.17 26.63 3 7 -2 384.00 31.37 3 7 -2 371.03 28.66 3 -7 -2 388.19 19.96 3 -7 -2 342.65 30.70 3 7 -1 117.92 15.14 3 7 -1 154.33 19.70 3 -7 -1 143.38 11.40 3 -7 -1 164.26 20.76 3 7 -1 166.69 18.39 3 -7 0 258.35 15.87 3 -7 0 272.52 16.23 3 7 0 273.45 25.03 3 7 0 285.30 27.16 3 -7 0 294.85 16.55 3 -7 1 193.95 13.19 3 7 1 148.65 19.91 3 -7 1 174.76 12.69 3 7 1 172.24 20.14 3 -7 1 182.51 12.82 3 7 2 874.53 51.05 3 -7 2 918.11 36.05 3 7 2 836.93 49.27 3 -7 2 851.68 35.14 3 7 3 78.50 13.96 3 -7 3 62.82 7.97 3 7 3 63.31 14.26 3 -7 3 76.46 8.11 3 -7 3 63.37 7.82 3 -7 4 485.63 34.54 3 7 4 441.86 35.32 3 -7 4 545.28 25.35 3 7 4 452.51 36.33 3 -7 4 524.93 24.35 3 -7 4 520.85 25.08 3 -7 5 12.31 6.24 3 -7 5 19.01 4.90 3 -7 5 11.45 4.41 3 -7 5 15.29 4.54 3 7 5 25.09 8.64 3 7 5 22.97 9.26 3 -7 6 22.98 5.38 3 -7 6 19.94 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52.34 10.44 4 2 5 63.73 11.57 4 -2 5 66.03 9.13 4 2 5 44.52 7.90 4 2 6 359.38 25.21 4 2 6 391.02 28.27 4 2 6 413.65 26.61 4 -2 6 376.98 24.62 4 2 6 420.53 25.45 4 -2 7 145.03 9.96 4 -2 7 129.21 14.49 4 2 7 122.36 13.81 4 2 7 155.30 17.60 4 2 7 120.98 14.83 4 2 7 149.98 16.13 4 -2 7 143.70 11.07 4 -2 7 131.44 9.57 4 2 7 132.00 9.97 4 -2 7 130.31 10.06 4 2 8 1028.14 38.71 4 -2 8 1029.50 38.74 4 -2 8 995.25 37.58 4 -2 8 1036.05 49.57 4 2 8 1014.99 48.58 4 2 8 1016.58 50.35 4 2 8 980.29 49.77 4 -2 8 987.14 39.43 4 2 8 1023.80 39.68 4 -2 8 1059.52 38.22 4 2 8 1059.79 38.00 4 -2 8 1010.84 37.35 4 2 8 975.59 36.96 4 -2 9 208.73 13.40 4 -2 9 197.09 20.07 4 2 9 233.67 21.28 4 2 9 216.58 21.30 4 2 9 249.07 22.68 4 2 9 225.71 14.49 4 -2 9 227.38 14.47 4 -2 9 176.11 13.90 4 2 9 213.36 14.88 4 -2 9 241.45 14.00 4 2 9 185.26 12.52 4 -2 10 39.04 7.28 4 2 10 47.36 7.57 4 -2 10 47.50 10.39 4 2 10 46.06 9.88 4 2 10 43.61 6.23 4 -2 10 38.44 5.99 4 2 10 49.55 6.64 4 2 10 54.48 7.51 4 -2 10 50.12 7.01 4 -2 11 450.33 22.12 4 2 11 429.09 21.54 4 -2 11 419.87 21.61 4 2 11 453.93 22.22 4 2 11 453.31 23.50 4 -2 11 454.82 23.11 4 -2 12 510.22 24.08 4 2 12 492.02 23.47 4 -2 12 500.87 23.88 4 2 12 476.52 23.53 4 2 12 463.37 24.84 4 -2 12 502.86 24.80 4 -2 13 16.63 4.18 4 -2 13 16.57 4.31 4 2 13 25.48 5.18 4 2 13 29.43 5.35 4 2 13 21.69 5.57 4 -2 14 191.01 13.03 4 2 14 204.08 13.25 4 2 14 217.11 13.76 4 -2 14 191.94 13.10 4 2 14 217.33 14.78 4 2 15 10.67 3.31 4 -2 15 4.93 2.90 4 2 15 14.21 3.64 4 2 15 9.33 3.40 4 2 16 33.75 4.76 4 -2 16 44.47 5.15 4 2 16 41.61 4.98 4 -3 -17 25.57 4.41 4 -3 -16 194.92 12.77 4 -3 -15 65.12 7.74 4 -3 -14 220.77 14.98 4 -3 -13 225.41 15.21 4 -3 -12 847.33 34.78 4 3 -12 911.37 49.69 4 -3 -12 808.00 50.06 4 3 -12 741.52 50.60 4 3 -11 48.27 10.77 4 -3 -11 78.78 14.84 4 -3 -11 46.45 6.93 4 3 -11 52.56 13.88 4 -3 -10 198.66 13.52 4 3 -10 238.44 21.73 4 -3 -10 232.43 24.24 4 3 -10 217.09 23.85 4 3 -9 62.16 10.76 4 -3 -9 57.00 11.92 4 -3 -9 52.81 6.79 4 3 -9 58.50 12.03 4 3 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290.05 15.02 4 4 4 271.49 22.59 4 -4 4 277.16 22.12 4 4 5 105.43 13.85 4 4 5 151.01 16.56 4 -4 5 132.23 9.96 4 4 5 163.71 19.25 4 -4 5 118.22 9.38 4 -4 5 126.63 9.55 4 4 5 120.69 15.45 4 -4 5 116.75 14.48 4 4 6 10.34 6.92 4 4 6 2.00 4.00 4 -4 6 6.83 3.18 4 -4 6 1.96 4.64 4 -4 6 0.73 2.26 4 -4 6 2.28 2.88 4 4 6 4.28 5.06 4 4 6 -2.49 4.45 4 -4 7 54.05 6.60 4 -4 7 53.21 6.89 4 -4 7 54.31 10.82 4 4 7 33.78 9.33 4 4 7 50.31 10.62 4 -4 8 147.55 11.41 4 -4 8 165.36 12.20 4 -4 8 152.08 17.91 4 4 8 145.81 18.53 4 4 8 142.02 18.32 4 4 8 149.27 18.09 4 4 9 412.67 32.90 4 4 9 454.64 34.50 4 -4 9 466.96 22.79 4 -4 9 470.56 23.22 4 4 9 490.90 34.24 4 -4 10 93.25 9.50 4 -4 10 69.61 8.10 4 -4 11 194.62 13.73 4 -4 11 216.32 14.70 4 -4 12 232.93 15.46 4 -4 12 275.87 16.05 4 -4 13 41.81 6.06 4 -4 13 50.44 6.84 4 -4 14 60.91 6.91 4 -4 14 60.02 6.70 4 -4 15 57.76 6.06 4 -5 -17 7.57 2.51 4 -5 -16 60.67 6.43 4 -5 -15 23.50 5.20 4 -5 -14 198.11 13.77 4 -5 -14 221.38 13.89 4 -5 -13 12.33 4.03 4 -5 -13 16.70 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5 5 93.23 13.47 4 -5 5 114.44 15.32 4 5 5 81.25 14.19 4 -5 6 247.70 15.29 4 -5 6 261.98 15.74 4 -5 6 308.44 16.80 4 5 6 276.13 27.03 4 5 6 212.30 21.62 4 5 6 235.97 23.32 4 -5 6 296.52 25.19 4 5 6 238.69 23.97 4 -5 7 17.02 4.54 4 -5 7 9.61 3.84 4 -5 7 21.68 4.91 4 5 7 23.31 8.64 4 5 7 9.86 7.31 4 5 7 4.77 4.78 4 -5 7 4.75 5.62 4 -5 8 4.71 3.67 4 -5 8 0.91 3.26 4 5 8 10.48 5.74 4 5 8 2.54 3.94 4 5 8 12.19 6.17 4 -5 8 14.76 7.29 4 -5 9 35.98 6.55 4 -5 9 49.47 6.88 4 -5 10 701.64 30.98 4 -5 10 728.61 31.89 4 -5 11 70.49 8.34 4 -5 11 66.23 8.05 4 -5 12 279.52 16.32 4 -5 12 230.94 14.99 4 -5 13 33.11 5.24 4 -5 13 28.47 5.22 4 -5 14 48.21 5.86 4 -5 14 62.34 6.38 4 -5 15 42.99 4.89 4 -6 -16 62.33 5.79 4 -6 -15 122.50 9.08 4 -6 -15 122.20 8.87 4 -6 -14 115.92 9.62 4 -6 -14 121.88 9.69 4 -6 -13 111.10 10.11 4 -6 -13 131.76 10.79 4 -6 -12 49.11 7.01 4 -6 -12 42.84 6.56 4 -6 -11 73.49 8.55 4 -6 -11 63.71 8.06 4 -6 -10 921.19 36.68 4 -6 -10 831.35 35.37 4 -6 -9 158.41 12.73 4 -6 -9 174.20 12.67 4 6 -8 870.35 48.23 4 -6 -8 980.94 38.40 4 6 -8 893.47 55.09 4 -6 -7 316.15 17.17 4 6 -7 254.81 23.21 4 6 -7 279.35 24.18 4 -6 -7 281.50 16.97 4 6 -7 251.81 27.22 4 -6 -6 580.36 25.71 4 6 -6 523.55 34.09 4 -6 -6 581.38 26.15 4 -6 -5 294.70 16.70 4 6 -5 286.69 23.83 4 -6 -5 299.75 16.97 4 6 -5 280.68 27.29 4 -6 -4 1048.18 38.09 4 6 -4 953.28 47.74 4 6 -4 979.09 54.89 4 6 -4 863.84 46.22 4 -6 -4 920.88 36.85 4 -6 -3 137.90 10.84 4 -6 -3 166.01 11.79 4 6 -3 123.53 15.41 4 6 -3 161.81 17.24 4 6 -3 131.89 18.86 4 6 -2 332.55 25.10 4 -6 -2 355.00 18.49 4 6 -2 298.73 27.99 4 -6 -2 354.73 18.26 4 -6 -1 37.14 9.10 4 -6 -1 41.84 6.07 4 6 -1 34.52 8.96 4 -6 -1 41.98 5.94 4 -6 -1 39.93 5.79 4 6 -1 42.02 11.79 4 -6 -1 29.84 8.60 4 6 -1 45.42 9.11 4 6 0 231.57 22.22 4 -6 0 240.72 22.04 4 -6 0 260.82 15.32 4 -6 0 251.23 14.94 4 6 0 281.87 26.95 4 -6 0 253.32 15.27 4 6 0 266.38 21.78 4 -6 1 111.26 9.64 4 -6 1 103.05 14.61 4 -6 1 101.30 9.26 4 -6 1 92.04 8.66 4 -6 1 106.12 9.49 4 6 1 122.76 16.35 4 -6 2 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212.29 12.35 5 2 5 171.92 17.29 5 2 5 152.05 18.50 5 -2 5 173.53 16.93 5 2 5 214.86 18.36 5 -2 5 195.08 12.00 5 2 6 213.63 22.15 5 2 6 166.45 18.02 5 -2 6 211.35 12.72 5 2 6 221.92 12.72 5 -2 6 177.86 18.00 5 2 6 154.55 16.61 5 -2 6 186.32 12.09 5 2 7 51.92 11.02 5 2 7 71.04 13.19 5 -2 7 83.64 8.01 5 -2 7 81.08 12.67 5 2 7 47.81 9.59 5 -2 7 81.97 8.15 5 2 7 84.07 7.94 5 -2 8 111.55 9.35 5 2 8 106.27 8.96 5 -2 8 95.49 9.06 5 2 8 100.67 9.15 5 2 8 113.94 15.73 5 2 8 91.11 9.28 5 -2 8 113.67 9.70 5 -2 8 85.99 13.48 5 2 8 103.90 14.43 5 2 9 136.89 17.74 5 -2 9 138.55 10.83 5 2 9 129.75 10.38 5 -2 9 92.33 14.42 5 2 9 109.25 15.57 5 2 9 127.78 11.10 5 -2 10 4.38 3.03 5 2 10 12.67 4.34 5 2 10 3.00 3.35 5 -2 11 64.07 7.64 5 2 11 55.44 7.89 5 2 11 75.50 8.14 5 2 11 67.60 8.02 5 -2 12 169.18 12.49 5 2 12 174.75 12.54 5 2 12 167.80 12.63 5 2 13 62.03 8.06 5 -2 13 64.21 7.40 5 2 13 61.83 7.24 5 2 13 62.76 7.58 5 2 14 51.02 6.26 5 -2 14 44.28 6.04 5 2 14 53.70 6.12 5 2 15 85.73 7.24 5 -2 15 83.96 7.10 5 2 15 68.54 6.49 5 2 16 8.00 2.40 5 -2 16 10.98 2.46 5 -3 -16 6.96 3.36 5 -3 -15 236.14 14.59 5 -3 -14 12.52 4.46 5 -3 -13 133.55 11.47 5 -3 -12 14.05 4.83 5 3 -11 145.73 20.25 5 -3 -11 162.37 12.51 5 3 -11 182.39 20.98 5 -3 -11 186.04 22.49 5 -3 -10 31.33 5.66 5 3 -10 22.33 8.67 5 3 -10 16.13 6.87 5 3 -9 182.29 21.34 5 3 -9 159.57 17.73 5 -3 -9 173.47 20.55 5 -3 -9 165.73 12.07 5 3 -8 86.84 14.32 5 3 -8 79.73 12.33 5 -3 -8 75.57 13.37 5 -3 -8 83.06 8.16 5 3 -7 307.92 26.13 5 3 -7 322.86 23.72 5 -3 -7 254.01 23.72 5 -3 -7 320.76 16.57 5 3 -6 86.30 13.52 5 3 -6 101.41 12.43 5 -3 -6 89.44 13.40 5 3 -6 109.20 13.01 5 -3 -6 113.93 9.06 5 -3 -6 126.14 9.20 5 3 -5 1568.57 59.43 5 3 -5 1561.50 61.36 5 -3 -5 1502.13 63.65 5 3 -5 1350.90 63.23 5 -3 -5 1414.62 63.64 5 -3 -4 406.50 26.83 5 3 -4 399.86 25.36 5 -3 -4 443.37 27.48 5 3 -4 376.87 27.29 5 -3 -4 359.53 26.28 5 -3 -3 2393.36 85.39 5 3 -3 2472.10 85.71 5 -3 -3 2463.74 87.18 5 3 -3 2176.89 87.87 5 -3 -3 2211.25 87.43 5 3 -2 268.19 19.74 5 -3 -2 269.18 21.74 5 -3 -2 270.71 20.12 5 3 -2 250.38 21.62 5 -3 -1 420.91 26.90 5 3 -1 448.50 26.51 5 3 -1 410.49 25.36 5 -3 -1 404.39 27.02 5 -3 -1 403.13 24.94 5 3 -1 403.50 27.89 5 -3 0 165.03 16.29 5 3 0 174.39 16.40 5 3 0 203.63 16.78 5 -3 0 159.35 15.79 5 -3 0 186.49 15.69 5 3 0 141.10 16.26 5 -3 1 523.97 30.66 5 -3 1 512.86 30.49 5 3 1 553.00 29.67 5 3 1 506.69 30.44 5 3 1 489.74 27.44 5 3 1 504.00 32.29 5 3 2 414.76 28.46 5 -3 2 383.79 25.63 5 -3 2 365.66 25.09 5 3 2 370.96 23.77 5 3 2 348.85 25.54 5 -3 3 1275.21 56.13 5 3 3 1313.54 58.29 5 3 3 1185.88 58.37 5 3 3 1409.02 56.62 5 3 3 1334.65 62.56 5 3 4 404.83 29.82 5 3 4 391.67 30.69 5 3 4 383.24 26.17 5 -3 4 368.32 18.33 5 -3 4 392.22 26.58 5 3 5 150.14 18.89 5 3 5 138.87 17.80 5 3 5 113.24 14.48 5 -3 5 138.72 10.37 5 -3 5 113.29 14.42 5 3 6 24.69 8.28 5 3 6 20.37 8.83 5 3 6 26.72 8.64 5 -3 6 21.99 4.59 5 3 7 489.18 34.00 5 -3 7 519.82 24.04 5 3 8 30.93 9.31 5 -3 8 31.65 5.62 5 3 9 77.33 13.88 5 -3 9 69.34 8.03 5 3 10 21.44 4.82 5 -3 10 18.47 4.77 5 3 11 213.08 13.94 5 -3 11 194.51 13.73 5 3 12 39.88 6.69 5 3 12 32.82 5.61 5 -3 12 29.66 5.33 5 3 13 46.40 6.85 5 3 13 31.41 5.19 5 3 14 24.34 4.22 5 -4 -17 95.33 7.24 5 -4 -16 4.53 2.95 5 -4 -15 3.11 3.03 5 -4 -14 178.32 12.88 5 -4 -13 7.48 4.01 5 -4 -12 530.84 25.71 5 -4 -11 54.20 7.37 5 -4 -10 24.00 5.41 5 4 -10 30.74 8.99 5 -4 -10 16.71 9.00 5 4 -10 27.35 9.82 5 -4 -10 26.72 6.03 5 -4 -9 346.77 18.66 5 -4 -9 339.27 18.79 5 -4 -9 329.34 29.56 5 4 -9 377.47 28.32 5 4 -9 299.57 29.20 5 -4 -8 43.16 6.31 5 4 -8 40.89 11.23 5 -4 -8 44.89 6.47 5 4 -8 64.56 11.18 5 -4 -8 37.49 10.07 5 4 -7 330.29 29.30 5 -4 -7 390.72 29.87 5 -4 -7 364.03 18.95 5 -4 -7 403.79 19.84 5 -4 -7 352.02 28.74 5 4 -7 451.59 28.77 5 4 -6 776.34 47.51 5 -4 -6 905.08 48.28 5 -4 -6 899.65 34.78 5 -4 -6 955.86 35.25 5 -4 -6 895.77 47.82 5 4 -6 898.65 43.85 5 4 -6 913.88 45.29 5 4 -5 169.01 19.70 5 -4 -5 170.54 18.67 5 -4 -5 186.26 12.11 5 -4 -5 184.05 12.00 5 -4 -5 171.64 18.84 5 4 -5 214.16 17.64 5 4 -5 211.61 18.55 5 4 -4 1091.96 57.81 5 -4 -4 1243.82 56.48 5 4 -4 1314.87 55.60 5 -4 -4 1304.94 59.16 5 -4 -4 1250.87 44.06 5 -4 -4 1273.41 44.52 5 -4 -3 13.54 3.71 5 -4 -3 14.91 3.80 5 4 -3 15.55 7.69 5 -4 -3 7.58 5.09 5 4 -3 19.58 6.37 5 -4 -3 5.07 4.55 5 -4 -3 11.70 5.79 5 -4 -3 17.45 6.25 5 -4 -2 72.37 7.25 5 -4 -2 95.00 13.16 5 4 -2 56.96 12.08 5 4 -2 71.98 10.70 5 -4 -2 66.83 11.63 5 -4 -2 78.85 11.27 5 -4 -1 287.76 23.40 5 -4 -1 306.02 15.68 5 -4 -1 249.01 21.95 5 4 -1 291.33 21.77 5 4 -1 310.01 25.84 5 4 -1 344.73 23.80 5 4 0 8.87 5.50 5 -4 0 8.73 3.07 5 -4 0 11.08 5.48 5 -4 0 9.85 3.33 5 4 0 12.63 5.29 5 -4 0 13.21 5.85 5 4 0 11.09 6.28 5 4 1 207.88 19.40 5 -4 1 179.67 11.70 5 -4 1 185.00 18.70 5 -4 1 192.61 12.14 5 4 1 185.18 17.12 5 4 1 219.22 22.04 5 -4 1 217.73 19.75 5 -4 2 1091.52 40.69 5 -4 2 1114.49 40.33 5 -4 2 1151.40 53.38 5 -4 2 1102.47 40.43 5 4 2 1166.24 57.41 5 -4 2 1160.85 53.75 5 4 2 1161.22 54.17 5 -4 3 456.25 20.09 5 4 3 446.75 28.09 5 -4 3 394.12 19.95 5 4 3 489.70 33.94 5 -4 3 428.51 20.22 5 -4 3 360.74 18.84 5 4 3 371.73 28.46 5 -4 3 444.35 29.73 5 4 4 327.40 24.84 5 4 4 337.68 29.45 5 -4 4 331.91 17.97 5 4 4 405.17 31.26 5 -4 4 347.55 17.69 5 -4 4 345.26 18.01 5 4 4 326.61 27.02 5 -4 4 332.77 26.08 5 -4 5 1066.18 39.68 5 -4 5 1059.66 40.18 5 -4 5 1043.32 40.27 5 -4 5 1019.64 51.96 5 4 5 1084.76 52.54 5 4 5 1073.51 57.61 5 -4 6 -1.73 3.28 5 -4 6 5.71 3.42 5 -4 6 6.93 3.55 5 -4 6 2.20 3.94 5 4 6 2.78 6.57 5 4 6 4.44 5.25 5 -4 7 103.89 9.95 5 -4 7 106.74 9.59 5 -4 7 90.91 9.10 5 4 7 126.32 17.15 5 4 8 174.04 19.78 5 4 8 135.64 18.60 5 -4 8 191.33 13.23 5 -4 8 173.53 13.09 5 -4 9 110.31 10.28 5 -4 9 99.98 9.57 5 -4 10 308.82 17.76 5 -4 10 321.27 18.51 5 -4 11 37.65 5.99 5 -4 11 28.58 5.66 5 -4 12 148.02 11.59 5 -4 13 127.83 9.95 5 -4 14 14.83 3.46 5 -5 -17 28.21 3.62 5 -5 -16 52.21 5.59 5 -5 -15 81.58 7.90 5 -5 -14 12.06 4.33 5 -5 -13 458.64 21.88 5 -5 -13 432.02 22.18 5 -5 -12 143.22 12.07 5 -5 -12 145.46 11.48 5 -5 -11 33.87 6.11 5 -5 -11 43.84 6.84 5 -5 -10 186.92 14.24 5 -5 -10 250.13 15.61 5 -5 -9 66.93 8.23 5 5 -9 67.05 12.38 5 -5 -9 73.93 14.61 5 5 -9 69.04 14.71 5 -5 -9 76.59 8.54 5 -5 -8 45.73 6.99 5 5 -8 33.30 10.88 5 -5 -8 42.69 6.75 5 5 -8 30.36 8.52 5 -5 -8 52.60 12.04 5 5 -7 203.90 24.51 5 -5 -7 236.12 14.88 5 -5 -7 230.40 14.55 5 -5 -7 232.42 23.82 5 5 -7 204.02 20.09 5 5 -7 201.39 20.07 5 5 -6 140.61 19.88 5 -5 -6 175.32 12.23 5 -5 -6 177.69 12.59 5 -5 -6 186.31 20.66 5 5 -6 170.61 17.74 5 5 -6 159.17 17.92 5 5 -5 727.83 45.64 5 -5 -5 684.02 28.76 5 -5 -5 676.57 29.19 5 -5 -5 670.28 40.62 5 -5 -5 776.14 43.31 5 5 -5 750.43 38.77 5 5 -5 671.31 38.84 5 -5 -4 214.17 21.04 5 5 -4 199.65 22.58 5 -5 -4 208.22 13.71 5 -5 -4 225.07 13.62 5 -5 -4 186.71 20.08 5 5 -4 204.42 19.67 5 -5 -3 37.42 8.96 5 5 -3 18.37 8.51 5 -5 -3 34.80 5.48 5 -5 -3 49.25 10.70 5 -5 -3 38.39 5.75 5 5 -3 29.88 8.06 5 -5 -2 2.07 5.23 5 -5 -2 8.40 3.61 5 5 -2 2.59 5.68 5 -5 -2 2.13 4.66 5 -5 -2 2.28 2.63 5 5 -2 5.52 4.36 5 -5 -1 12.46 6.17 5 -5 -1 18.21 4.41 5 5 -1 5.85 4.62 5 5 -1 5.21 6.59 5 -5 -1 17.09 7.15 5 -5 -1 29.25 5.07 5 5 -1 5.44 3.98 5 -5 0 33.02 5.24 5 -5 0 29.41 8.86 5 -5 0 35.67 5.76 5 5 0 34.82 8.45 5 5 0 36.63 10.50 5 -5 0 49.66 10.61 5 5 0 37.75 8.56 5 5 1 288.36 24.84 5 -5 1 297.80 24.82 5 -5 1 320.66 16.80 5 -5 1 295.27 16.66 5 -5 1 255.15 23.43 5 5 1 319.97 28.42 5 -5 2 61.56 7.34 5 -5 2 71.62 7.37 5 -5 2 68.35 7.46 5 -5 2 48.68 6.59 5 -5 2 70.21 12.38 5 -5 2 79.63 7.95 5 5 2 68.04 12.30 5 5 2 81.62 15.10 5 5 3 392.93 31.12 5 -5 3 435.49 21.43 5 -5 3 459.58 21.78 5 5 3 441.15 35.25 5 -5 3 431.52 21.75 5 -5 3 463.63 32.50 5 -5 3 458.22 21.70 5 -5 4 27.06 5.40 5 -5 4 33.72 5.99 5 -5 4 25.80 5.33 5 5 4 17.31 7.77 5 -5 4 34.22 5.56 5 -5 4 25.71 8.65 5 5 4 35.04 10.28 5 5 5 279.26 28.67 5 5 5 269.27 24.21 5 -5 5 293.76 17.26 5 -5 5 257.71 24.37 5 -5 5 279.69 16.66 5 -5 5 283.99 16.85 5 5 5 266.30 26.42 5 5 6 37.86 9.53 5 -5 6 44.02 6.69 5 -5 6 44.67 11.15 5 -5 6 34.48 5.96 5 -5 6 41.98 6.67 5 -5 7 324.07 18.27 5 -5 7 289.44 17.78 5 -5 7 296.11 27.16 5 -5 7 307.48 17.94 5 -5 8 44.48 6.85 5 -5 8 27.36 5.61 5 -5 9 256.80 16.28 5 -5 9 278.09 17.24 5 -5 10 107.79 9.89 5 -5 10 112.73 10.52 5 -5 11 306.22 17.31 5 -5 11 302.06 17.54 5 -5 12 21.45 4.43 5 -5 12 25.43 4.96 5 -5 13 95.02 8.19 5 -5 13 103.32 8.22 5 -5 14 6.25 2.33 5 -6 -16 2.93 2.02 5 -6 -15 11.15 3.24 5 -6 -14 197.93 11.90 5 -6 -14 183.96 12.00 5 -6 -13 198.02 12.80 5 -6 -13 197.76 13.09 5 -6 -12 82.30 8.54 5 -6 -12 88.53 8.99 5 -6 -11 58.21 7.60 5 -6 -11 51.03 7.23 5 -6 -10 16.98 5.29 5 -6 -10 18.25 5.12 5 -6 -9 195.82 14.17 5 -6 -9 217.17 14.47 5 -6 -8 142.61 11.79 5 -6 -8 120.90 10.72 5 6 -7 695.05 48.98 5 6 -7 786.62 44.76 5 6 -7 781.20 45.23 5 -6 -7 812.48 33.79 5 -6 -7 814.69 33.14 5 -6 -6 690.08 28.98 5 6 -6 668.38 46.62 5 6 -6 600.29 37.70 5 6 -6 621.70 39.49 5 -6 -6 656.49 29.13 5 -6 -5 272.41 15.85 5 6 -5 230.80 22.32 5 -6 -5 243.83 15.51 5 -6 -4 99.93 9.46 5 6 -4 93.65 17.29 5 6 -4 108.99 15.71 5 -6 -4 95.67 9.62 5 -6 -3 66.54 7.89 5 6 -3 80.83 15.72 5 6 -3 72.75 12.40 5 -6 -3 68.12 8.13 5 -6 -2 225.45 14.94 5 -6 -2 263.36 16.04 5 -6 -2 268.02 24.61 5 6 -2 244.75 26.54 5 -6 -2 288.03 24.91 5 6 -2 262.04 23.35 5 -6 -1 441.67 22.14 5 -6 -1 446.78 32.70 5 -6 -1 477.07 22.89 5 -6 -1 476.37 33.85 5 6 -1 452.09 37.11 5 6 -1 498.80 32.73 5 -6 0 113.96 9.83 5 6 0 80.13 13.66 5 -6 0 114.71 10.03 5 -6 0 99.23 9.52 5 -6 0 126.80 17.05 5 6 0 128.85 19.54 5 6 1 18.21 9.82 5 -6 1 34.88 5.91 5 6 1 29.55 9.12 5 -6 1 43.28 6.58 5 -6 1 32.39 5.71 5 -6 1 31.22 8.64 5 -6 1 35.95 5.72 5 6 2 101.25 18.13 5 -6 2 96.18 9.31 5 6 2 64.21 13.20 5 -6 2 95.62 9.37 5 -6 2 71.43 13.42 5 -6 2 89.79 9.31 5 -6 2 74.39 8.29 5 -6 3 1.83 2.94 5 6 3 2.68 5.86 5 -6 3 -1.89 3.38 5 -6 3 3.68 3.19 5 -6 3 2.53 4.52 5 6 3 9.37 7.39 5 -6 4 60.68 7.74 5 -6 4 58.90 7.82 5 6 4 83.39 15.01 5 -6 4 83.32 8.94 5 6 4 50.72 13.11 5 -6 4 51.68 11.46 5 -6 4 68.85 8.55 5 6 5 205.52 23.96 5 -6 5 241.17 15.79 5 -6 5 213.70 14.59 5 6 5 231.19 26.60 5 -6 5 240.91 15.60 5 -6 5 226.98 15.05 5 -6 5 224.40 24.09 5 -6 6 97.37 10.03 5 -6 6 116.23 10.69 5 -6 6 118.11 10.68 5 -6 6 129.38 10.94 5 -6 7 197.04 14.39 5 -6 7 213.73 14.77 5 -6 7 215.42 14.76 5 -6 8 73.89 8.73 5 -6 8 92.45 9.38 5 -6 8 80.21 8.58 5 -6 9 202.11 13.71 5 -6 9 159.41 12.73 5 -6 10 52.64 7.13 5 -6 10 60.18 7.54 5 -6 11 37.93 5.57 5 -6 11 40.73 6.03 5 -6 12 48.72 6.15 5 -6 12 55.59 6.07 5 -6 13 9.39 2.97 5 -6 13 11.83 2.99 5 -7 -14 40.87 4.83 5 -7 -14 41.78 4.99 5 -7 -13 42.43 5.37 5 -7 -13 36.53 5.21 5 -7 -12 136.05 10.09 5 -7 -12 127.73 10.09 5 -7 -11 45.61 6.27 5 -7 -11 42.41 6.42 5 -7 -10 121.37 10.73 5 -7 -9 16.76 4.87 5 -7 -8 78.91 8.94 5 -7 -7 17.11 4.51 5 -7 -7 20.09 5.36 5 -7 -6 226.05 15.10 5 -7 -6 228.53 15.26 5 -7 -5 456.55 22.91 5 -7 -5 451.62 23.08 5 -7 -4 39.65 6.45 5 -7 -4 33.50 6.14 5 -7 -3 451.57 23.21 5 -7 -3 485.18 23.66 5 -7 -3 482.35 23.86 5 7 -3 488.05 34.75 5 7 -3 477.52 39.39 5 -7 -2 54.33 7.38 5 -7 -2 57.27 7.62 5 7 -2 38.97 13.06 5 -7 -2 43.29 7.08 5 7 -2 58.92 11.81 5 -7 -1 12.46 4.37 5 7 -1 3.25 9.65 5 -7 -1 11.62 4.73 5 -7 0 561.03 26.85 5 -7 0 572.05 26.38 5 -7 0 524.26 25.76 5 7 0 529.49 42.29 5 -7 1 44.45 6.80 5 7 1 38.20 10.40 5 7 1 29.59 11.43 5 -7 1 28.67 5.96 5 -7 1 66.16 8.16 5 -7 1 35.95 9.80 5 -7 2 303.54 18.06 5 -7 2 300.08 18.00 5 -7 2 253.30 16.63 5 -7 3 148.13 12.22 5 -7 3 138.13 11.96 5 -7 3 140.94 12.07 5 -7 4 16.14 5.11 5 -7 4 7.83 4.21 5 -7 4 18.93 4.89 5 -7 5 37.07 6.56 5 -7 5 39.18 6.59 5 -7 5 49.90 7.30 5 -7 6 176.60 13.28 5 -7 6 163.36 13.00 5 -7 6 182.36 13.33 5 -7 7 225.02 14.75 5 -7 7 197.29 14.08 5 -7 7 179.76 13.26 5 -7 7 194.54 13.60 5 -7 8 159.57 12.31 5 -7 8 167.61 12.32 5 -7 8 163.66 12.11 5 -7 9 17.30 4.70 5 -7 9 27.85 5.16 5 -7 10 52.91 6.45 5 -7 10 57.05 6.76 5 -7 11 5.65 2.58 5 -7 11 11.51 3.29 5 -7 12 81.52 6.63 5 -7 12 75.24 6.44 5 -8 -13 23.07 3.68 5 -8 -12 18.64 3.72 5 -8 -11 135.01 9.99 5 -8 -10 30.28 5.22 5 -8 -9 12.27 4.21 5 -8 -8 6.89 3.70 5 -8 -8 10.60 3.79 5 -8 -7 13.32 4.44 5 -8 -7 13.94 4.42 5 -8 -6 31.61 5.87 5 -8 -6 53.78 7.14 5 -8 -5 95.35 9.56 5 -8 -5 95.77 9.72 5 -8 -4 15.40 4.37 5 -8 -4 7.66 3.74 5 -8 -3 177.82 13.22 5 -8 -3 217.80 14.73 5 -8 -2 15.15 4.34 5 -8 -2 15.45 4.24 5 -8 -1 145.10 11.96 5 -8 -1 132.90 11.28 5 -8 0 2.80 3.64 5 -8 0 1.99 3.32 5 -8 0 10.27 4.17 5 -8 1 338.07 19.05 5 -8 1 292.52 17.58 5 -8 1 333.55 19.12 5 -8 2 51.07 7.30 5 -8 2 41.39 7.17 5 -8 2 51.82 7.22 5 -8 3 298.17 17.87 5 -8 3 311.71 18.60 5 -8 3 308.97 18.37 5 -8 4 28.91 5.63 5 -8 4 31.40 6.05 5 -8 4 15.50 4.79 5 -8 5 128.97 11.03 5 -8 5 98.16 9.93 5 -8 5 136.04 11.27 5 -8 6 20.04 4.58 5 -8 6 22.16 4.99 5 -8 6 26.63 5.42 5 -8 7 80.21 8.28 5 -8 7 68.67 7.69 5 -8 7 63.44 7.53 5 -8 8 17.94 4.30 5 -8 8 12.12 3.57 5 -8 9 203.69 12.41 5 -8 10 15.12 3.31 5 -8 11 38.29 4.33 5 -9 -11 26.16 3.78 5 -9 -10 152.10 9.63 5 -9 -9 1.86 2.29 5 -9 -8 86.65 7.85 5 -9 -8 94.50 8.17 5 -9 -7 19.22 4.22 5 -9 -7 26.60 4.94 5 -9 -7 26.80 4.98 5 -9 -6 51.48 6.59 5 -9 -6 50.85 6.51 5 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536.19 24.72 6 -4 6 537.81 25.56 6 -4 7 34.30 6.38 6 -4 7 31.38 5.71 6 -4 8 195.00 14.25 6 -4 9 75.27 8.75 6 -4 10 147.44 11.87 6 -4 11 261.69 15.61 6 -4 12 28.83 4.76 6 -4 13 44.19 5.31 6 -5 -16 55.76 5.34 6 -5 -15 15.56 3.65 6 -5 -14 302.58 16.37 6 -5 -13 0.82 3.42 6 -5 -12 350.68 19.21 6 -5 -11 168.72 12.80 6 -5 -11 151.47 11.84 6 -5 -10 82.99 8.89 6 -5 -10 59.39 7.49 6 -5 -9 74.03 8.51 6 -5 -9 64.83 8.20 6 -5 -8 355.98 19.75 6 -5 -8 368.99 19.96 6 -5 -7 45.39 10.87 6 5 -7 32.35 8.84 6 -5 -7 38.61 10.60 6 -5 -7 45.77 6.76 6 -5 -7 38.91 6.47 6 5 -7 47.27 12.33 6 5 -6 206.76 25.26 6 -5 -6 171.25 20.31 6 5 -6 185.82 20.20 6 -5 -6 194.41 21.54 6 -5 -6 220.72 23.54 6 -5 -6 206.98 13.98 6 -5 -6 190.03 13.63 6 -5 -5 37.08 6.08 6 -5 -5 25.51 5.34 6 5 -5 18.18 9.02 6 -5 -5 31.53 9.73 6 -5 -5 39.62 9.80 6 -5 -5 27.54 8.99 6 5 -5 36.24 9.74 6 -5 -4 139.91 10.97 6 -5 -4 131.32 11.10 6 5 -4 110.49 18.50 6 -5 -4 134.68 18.00 6 -5 -4 113.80 16.39 6 5 -4 153.95 18.35 6 -5 -3 172.14 19.93 6 5 -3 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7 -4 8 12.43 4.06 7 -4 9 38.13 6.08 7 -4 10 74.00 7.74 7 -4 11 56.39 6.30 7 -5 -15 54.75 5.29 7 -5 -14 4.23 2.75 7 -5 -13 370.44 18.49 7 -5 -12 17.55 4.59 7 -5 -11 287.13 16.91 7 -5 -10 32.55 5.79 7 -5 -9 39.37 6.25 7 -5 -9 36.14 6.34 7 -5 -8 30.81 5.96 7 -5 -8 28.83 5.58 7 -5 -7 143.21 12.11 7 -5 -7 162.91 12.36 7 -5 -6 126.96 11.11 7 -5 -6 133.81 11.35 7 -5 -5 819.71 48.41 7 -5 -5 752.73 47.11 7 5 -5 682.29 48.82 7 -5 -5 756.67 32.44 7 -5 -5 796.06 33.10 7 -5 -5 738.13 45.02 7 5 -4 -2.54 5.57 7 -5 -4 5.37 3.39 7 -5 -4 15.80 5.06 7 5 -4 9.60 7.57 7 -5 -4 -2.64 5.78 7 -5 -4 10.84 6.41 7 5 -3 127.29 17.82 7 -5 -3 125.36 10.58 7 -5 -3 136.28 11.46 7 5 -3 98.94 18.60 7 -5 -3 129.28 18.60 7 -5 -3 118.99 17.61 7 5 -2 184.31 21.59 7 -5 -2 211.29 13.86 7 -5 -2 184.03 13.51 7 5 -2 181.72 24.26 7 -5 -2 190.18 22.28 7 -5 -2 167.87 21.21 7 5 -1 300.24 27.44 7 5 -1 309.59 31.89 7 -5 -1 257.99 26.41 7 -5 -1 286.11 27.41 7 -5 -1 318.51 17.78 7 -5 -1 322.75 18.50 7 -5 0 196.29 22.94 7 -5 0 231.72 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51.45 7.45 8 -2 4 59.25 7.96 8 -2 5 204.69 14.60 8 -2 5 184.99 13.91 8 2 6 251.74 16.08 8 -2 6 272.07 16.78 8 -2 6 238.61 15.56 8 -2 7 6.69 4.10 8 2 7 8.43 3.75 8 -2 7 0.93 3.23 8 -2 8 57.03 7.06 8 2 8 36.88 5.91 8 -2 8 50.36 7.17 8 2 8 58.22 7.55 8 -2 9 11.84 3.75 8 2 9 10.91 3.56 8 -2 10 1.41 2.44 8 2 10 0.70 2.78 8 2 10 6.72 2.75 8 -2 11 59.34 6.07 8 2 11 69.37 6.42 8 2 11 68.03 6.91 8 -2 12 106.15 7.35 8 2 12 113.01 7.51 8 2 12 102.70 7.61 8 -3 -13 26.06 4.76 8 -3 -12 27.67 5.25 8 -3 -11 73.49 8.27 8 -3 -10 149.01 11.71 8 -3 -9 118.13 10.66 8 -3 -8 58.89 7.83 8 -3 -7 6.56 3.93 8 -3 -6 551.10 39.95 8 3 -6 532.67 38.40 8 -3 -6 603.17 39.58 8 -3 -6 541.12 25.96 8 -3 -5 37.62 10.05 8 -3 -5 16.79 4.99 8 -3 -5 49.89 12.65 8 -3 -5 40.67 10.86 8 3 -5 43.20 11.08 8 -3 -4 226.73 22.93 8 -3 -4 240.87 15.30 8 -3 -4 205.91 23.61 8 -3 -4 173.04 21.45 8 3 -4 191.46 22.50 8 -3 -3 36.28 9.69 8 -3 -3 22.30 5.16 8 -3 -3 21.22 8.24 8 -3 -3 18.30 8.45 8 3 -3 24.42 9.41 8 -3 -2 104.20 15.22 8 3 -2 72.33 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278.97 16.65 8 -5 2 260.57 16.49 8 -5 2 256.88 16.59 8 -5 2 279.46 17.05 8 -5 3 0.98 3.02 8 -5 3 3.86 3.55 8 -5 4 346.66 19.39 8 -5 4 298.87 18.21 8 -5 5 67.38 8.26 8 -5 5 73.58 8.53 8 -5 6 14.26 4.23 8 -5 6 16.41 4.45 8 -5 7 11.58 3.63 8 -5 7 7.83 3.44 8 -5 8 9.65 3.39 8 -5 8 5.40 3.08 8 -5 9 21.10 4.08 8 -5 10 67.51 6.06 8 -6 -13 8.42 2.58 8 -6 -12 38.37 4.92 8 -6 -11 64.29 6.56 8 -6 -10 11.10 3.78 8 -6 -10 7.17 3.20 8 -6 -9 2.99 3.41 8 -6 -9 0.73 2.75 8 -6 -8 26.83 5.06 8 -6 -8 36.14 5.72 8 -6 -7 18.31 4.62 8 -6 -7 20.44 4.93 8 -6 -6 48.62 6.70 8 -6 -6 41.76 6.33 8 -6 -5 66.73 7.94 8 -6 -5 60.87 7.96 8 -6 -4 216.11 13.96 8 -6 -4 178.54 13.47 8 -6 -3 246.46 15.81 8 -6 -2 70.48 8.41 8 -6 -2 57.26 7.50 8 -6 -1 42.16 6.73 8 -6 -1 65.69 8.10 8 -6 0 49.15 7.42 8 -6 0 57.19 7.47 8 -6 1 20.51 4.92 8 -6 1 18.44 4.67 8 -6 1 4.43 3.28 8 -6 1 12.79 4.33 8 -6 2 243.74 15.29 8 -6 2 197.24 14.08 8 -6 2 218.47 14.59 8 -6 2 229.23 14.65 8 -6 3 158.93 11.93 8 -6 3 160.70 12.14 8 -6 3 147.94 11.66 8 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52.21 7.39 9 -2 3 43.42 6.93 9 -2 4 115.63 10.49 9 2 4 98.45 9.81 9 -2 4 101.20 9.77 9 -2 5 218.97 14.67 9 2 5 206.79 14.26 9 -2 5 202.26 13.98 9 -2 6 16.88 4.85 9 -2 6 15.20 4.55 9 2 6 21.37 5.24 9 -2 7 214.47 13.67 9 -2 7 200.61 13.08 9 2 7 192.28 12.75 9 -2 7 223.46 14.07 9 2 7 194.72 13.34 9 -2 8 35.73 5.21 9 2 8 32.27 4.99 9 2 9 7.92 3.29 9 -2 9 7.30 2.93 9 2 9 7.93 2.89 9 2 10 17.65 3.54 9 2 10 10.57 2.76 9 -2 10 11.49 2.85 9 2 11 9.86 2.47 9 -3 -12 27.11 4.61 9 -3 -11 89.80 8.30 9 -3 -10 37.53 5.98 9 -3 -9 252.83 15.52 9 -3 -8 19.59 5.06 9 -3 -7 119.39 10.69 9 -3 -6 23.46 5.41 9 -3 -5 821.45 34.54 9 -3 -4 73.26 8.90 9 -3 -3 176.06 13.35 9 -3 -2 38.22 6.58 9 -3 -1 52.23 7.72 9 -3 0 35.60 6.51 9 -3 1 48.43 7.30 9 -3 2 56.50 7.88 9 -3 3 219.54 15.21 9 -3 3 226.95 15.48 9 -3 4 87.02 9.37 9 -3 4 82.21 8.97 9 -3 5 62.67 7.81 9 -3 5 60.39 7.62 9 -3 6 78.76 8.33 9 -3 6 74.76 8.12 9 -3 7 141.29 10.56 9 -3 7 133.73 10.25 9 3 9 135.89 9.28 9 3 10 0.94 1.83 9 -4 -14 17.20 2.88 9 -4 -13 11.44 2.93 9 -4 -12 113.65 8.51 9 -4 -11 53.43 6.36 9 -4 -10 56.78 6.82 9 -4 -9 123.02 10.15 9 -4 -8 54.10 7.11 9 -4 -7 144.38 11.72 9 -4 -6 131.70 11.12 9 -4 -5 69.82 8.30 9 -4 -4 153.54 12.30 9 -4 -4 156.61 11.88 9 -4 -3 10.44 4.42 9 -4 -2 134.30 11.56 9 -4 -1 22.86 5.29 9 -4 0 91.95 9.50 9 -4 0 77.87 8.45 9 -4 1 118.37 10.62 9 -4 1 114.36 10.40 9 -4 1 107.01 10.33 9 -4 2 89.83 9.11 9 -4 2 101.15 10.35 9 -4 3 79.93 8.60 9 -4 3 83.04 9.13 9 -4 4 118.77 10.36 9 -4 4 88.32 9.21 9 -4 5 226.88 14.47 9 -4 5 212.14 14.28 9 -4 6 54.44 6.68 9 -4 6 49.41 6.53 9 -4 7 47.29 5.81 9 -4 7 40.68 5.69 9 -4 8 44.36 5.22 9 -4 8 41.65 5.27 9 -4 9 27.17 3.90 9 -5 -13 140.26 8.22 9 -5 -12 57.51 5.67 9 -5 -11 70.35 6.77 9 -5 -10 22.80 4.37 9 -5 -9 56.36 6.66 9 -5 -8 3.90 3.04 9 -5 -7 87.50 8.68 9 -5 -6 71.80 8.11 9 -5 -6 65.93 7.52 9 -5 -5 120.83 10.58 9 -5 -5 140.50 10.87 9 -5 -4 18.94 4.84 9 -5 -4 20.11 4.85 9 -5 -3 174.17 12.73 9 -5 -2 0.88 2.94 9 -5 -2 0.85 2.83 9 -5 -1 272.91 16.37 9 -5 -1 267.95 16.37 9 -5 0 32.19 5.94 9 -5 0 37.77 6.39 9 -5 0 27.89 5.81 9 -5 1 180.49 13.25 9 -5 1 209.13 13.70 9 -5 2 3.54 2.86 9 -5 2 0.86 2.96 9 -5 3 276.84 16.50 9 -5 3 285.80 16.57 9 -5 4 8.25 3.62 9 -5 4 5.64 3.31 9 -5 5 71.06 7.67 9 -5 5 64.70 7.11 9 -5 6 8.44 3.27 9 -5 6 5.42 2.91 9 -5 7 3.09 2.35 9 -5 7 9.29 2.89 9 -5 8 23.83 3.79 9 -5 8 25.41 3.64 9 -6 -11 44.11 4.80 9 -6 -10 56.01 5.71 9 -6 -9 49.28 5.77 9 -6 -8 76.25 7.37 9 -6 -8 98.62 7.97 9 -6 -7 72.58 7.29 9 -6 -7 75.35 7.32 9 -6 -6 69.86 7.28 9 -6 -6 53.75 6.58 9 -6 -5 49.55 6.56 9 -6 -5 51.19 6.56 9 -6 -4 80.07 8.20 9 -6 -4 81.75 7.99 9 -6 -4 68.01 7.50 9 -6 -3 295.00 16.08 9 -6 -3 283.36 16.23 9 -6 -3 289.22 16.68 9 -6 -2 52.41 6.69 9 -6 -2 47.76 6.55 9 -6 -1 55.22 6.99 9 -6 -1 60.27 7.11 9 -6 0 13.02 4.40 9 -6 0 18.61 4.40 9 -6 0 9.61 3.52 9 -6 1 27.65 5.03 9 -6 1 25.97 4.81 9 -6 1 42.89 6.01 9 -6 1 37.35 5.61 9 -6 2 8.25 3.42 9 -6 2 6.47 3.28 9 -6 2 4.46 2.98 9 -6 3 29.69 4.97 9 -6 3 34.64 5.39 9 -6 4 78.66 7.55 9 -6 4 76.31 7.45 9 -6 5 149.75 10.03 9 -6 5 138.07 9.76 9 -6 6 7.84 2.65 9 -6 6 5.98 2.58 9 -6 7 39.48 4.44 9 -6 7 35.22 4.12 9 -7 -9 19.80 3.23 9 -7 -9 15.08 2.95 9 -7 -8 115.02 7.86 9 -7 -8 134.16 8.55 9 -7 -7 54.16 5.78 9 -7 -6 0.60 2.16 9 -7 -6 3.67 2.74 9 -7 -6 3.63 2.59 9 -7 -5 74.86 7.22 9 -7 -5 76.33 7.12 9 -7 -4 88.90 8.22 9 -7 -4 95.79 8.26 9 -7 -3 41.45 5.72 9 -7 -3 48.16 5.92 9 -7 -2 154.42 10.87 9 -7 -2 158.96 10.86 9 -7 -1 12.60 3.45 9 -7 -1 16.92 3.89 9 -7 0 13.56 3.45 9 -7 0 12.57 3.71 9 -7 1 16.66 3.92 9 -7 1 19.71 4.05 9 -7 2 7.65 2.93 9 -7 2 1.76 2.35 9 -7 2 4.18 2.45 9 -7 3 75.51 6.65 9 -7 3 75.71 6.62 9 -7 4 32.27 4.36 9 -7 4 25.88 3.91 9 -7 4 29.72 4.05 9 -7 5 5.52 2.10 9 -7 5 3.04 1.82 9 -8 -7 22.54 3.18 9 -8 -7 18.92 3.00 9 -8 -6 42.57 4.44 9 -8 -6 40.78 4.41 9 -8 -5 211.59 10.83 9 -8 -5 190.35 10.56 9 -8 -4 45.72 5.02 9 -8 -4 38.77 4.55 9 -8 -3 171.81 10.13 9 -8 -3 179.11 9.97 9 -8 -3 172.60 10.13 9 -8 -2 10.62 3.04 9 -8 -2 4.51 2.06 9 -8 -2 8.25 2.61 9 -8 -1 31.06 4.29 9 -8 -1 38.26 4.52 9 -8 0 60.34 5.75 9 -8 0 66.21 5.89 9 -8 1 18.88 3.29 9 -8 1 21.02 3.36 9 -8 2 6.72 2.10 9 -8 2 8.58 2.46 10 0 -14 39.65 4.52 10 0 -13 0.57 2.74 10 0 -12 18.77 4.35 10 0 -11 -0.76 3.10 10 0 -10 92.21 9.03 10 0 -9 2.67 3.47 10 0 -8 14.00 4.95 10 0 -7 2.91 3.87 10 0 -6 82.34 9.24 10 0 -5 3.03 4.23 10 0 -4 450.88 23.63 10 0 -3 -1.03 4.21 10 0 -2 548.18 26.85 10 0 -1 -1.03 4.01 10 0 0 124.99 11.64 10 0 1 1.01 3.13 10 0 2 3.97 3.44 10 0 3 -1.93 3.76 10 0 4 37.79 6.14 10 0 5 1.73 3.20 10 0 6 86.10 8.53 10 0 7 -0.66 2.45 10 0 8 1.71 1.91 10 0 8 2.72 2.33 10 0 9 0.47 1.67 10 0 9 0.44 1.61 10 -1 -14 24.29 3.46 10 1 -14 18.49 3.27 10 -1 -13 24.29 4.07 10 1 -13 14.99 3.51 10 -1 -12 57.11 6.32 10 1 -12 61.71 6.61 10 -1 -11 166.14 11.57 10 1 -11 169.03 11.63 10 -1 -10 -0.80 3.20 10 1 -10 9.83 4.21 10 1 -9 69.33 8.08 10 -1 -9 70.39 8.10 10 -1 -8 27.13 5.65 10 1 -8 29.61 6.01 10 -1 -7 24.37 5.60 10 1 -7 23.99 5.40 10 -1 -6 50.08 7.40 10 1 -6 37.49 6.82 10 -1 -5 109.76 10.74 10 1 -5 120.50 11.27 10 -1 -4 9.92 4.17 10 1 -4 8.13 4.27 10 -1 -4 20.48 4.92 10 -1 -3 451.54 23.36 10 1 -3 464.09 23.93 10 -1 -3 437.82 22.49 10 -1 -2 230.63 15.81 10 1 -2 231.56 16.07 10 -1 -2 238.89 15.47 10 -1 -1 527.32 25.94 10 1 -1 553.17 26.58 10 -1 -1 522.05 25.41 10 -1 0 272.76 17.06 10 1 0 240.65 16.36 10 -1 1 41.36 6.62 10 1 1 37.00 6.66 10 -1 2 8.70 3.87 10 1 2 6.85 4.02 10 -1 3 37.51 6.28 10 1 3 29.40 5.76 10 -1 4 92.22 9.22 10 1 4 95.82 9.37 10 -1 5 243.07 14.99 10 1 5 230.62 14.81 10 -1 6 29.76 5.04 10 -1 6 38.55 5.60 10 1 6 41.14 5.89 10 -1 7 9.58 2.92 10 1 7 16.77 3.84 10 -1 7 8.72 3.11 10 -1 8 41.47 4.88 10 1 8 35.31 4.65 10 1 8 30.26 4.42 10 -1 9 7.92 2.37 10 1 9 7.13 2.30 10 1 9 7.27 2.41 10 -2 -13 4.18 2.16 10 2 -13 5.42 2.38 10 -2 -12 1.70 2.27 10 2 -12 2.38 2.55 10 -2 -11 17.68 4.00 10 2 -11 21.24 4.49 10 -2 -10 201.16 12.75 10 2 -10 182.02 12.41 10 -2 -9 62.35 7.36 10 2 -9 61.02 7.53 10 -2 -8 176.12 11.99 10 -2 -8 162.84 12.14 10 2 -8 165.89 12.40 10 -2 -7 23.76 5.05 10 -2 -7 15.69 4.64 10 2 -7 22.80 5.37 10 -2 -6 27.42 5.31 10 -2 -6 35.00 6.26 10 2 -6 23.48 5.37 10 -2 -5 32.83 5.70 10 -2 -5 21.06 5.02 10 2 -5 20.12 5.52 10 -2 -4 407.21 20.97 10 -2 -4 382.44 20.70 10 2 -4 380.18 21.13 10 -2 -3 147.77 11.96 10 -2 -3 118.90 10.94 10 2 -3 139.57 11.94 10 -2 -2 164.03 12.94 10 -2 -2 179.52 13.31 10 2 -2 185.60 13.66 10 -2 -1 52.28 7.39 10 -2 -1 37.57 6.65 10 2 -1 33.06 6.36 10 -2 0 60.65 7.54 10 2 0 70.25 8.53 10 -2 1 21.18 5.25 10 2 1 32.15 5.90 10 -2 2 251.61 15.91 10 2 2 263.77 16.26 10 -2 2 267.54 16.26 10 -2 3 21.70 5.05 10 2 3 17.69 4.50 10 -2 3 15.23 4.56 10 -2 4 132.62 10.63 10 -2 4 151.47 11.44 10 -2 4 152.41 11.51 10 2 4 157.58 11.76 10 -2 5 8.51 3.46 10 -2 5 3.84 2.66 10 2 5 10.11 3.41 10 -2 6 177.65 11.52 10 2 6 204.79 12.13 10 -2 6 205.18 12.54 10 -2 6 178.37 11.81 10 2 6 208.75 12.63 10 -2 7 4.72 2.43 10 -2 7 7.36 2.69 10 2 7 9.24 2.74 10 2 8 72.20 6.40 10 -2 8 67.54 5.82 10 2 8 63.73 5.79 10 2 9 0.85 1.69 10 -3 -11 13.25 3.33 10 -3 -10 240.11 13.39 10 -3 -9 3.51 2.74 10 -3 -8 79.82 8.00 10 -3 -7 7.26 3.54 10 -3 -6 112.25 9.99 10 -3 -5 53.25 7.13 10 -3 -4 112.72 10.19 10 -3 -3 63.68 8.04 10 -3 -2 7.35 3.86 10 -3 -1 80.14 8.77 10 -3 0 180.34 12.70 10 -3 1 39.80 6.01 10 -3 1 36.81 5.94 10 -3 2 59.77 7.43 10 -3 2 56.50 7.13 10 -3 3 28.68 5.26 10 -3 3 40.58 6.13 10 -3 4 40.45 5.81 10 -3 4 30.16 5.03 10 -3 5 14.33 3.92 10 -3 5 16.88 3.90 10 -3 6 3.18 2.78 10 -3 6 0.62 2.14 10 -3 7 5.33 2.13 10 3 8 84.77 6.45 10 -4 -12 0.41 1.71 10 -4 -11 64.08 5.94 10 -4 -10 33.67 4.71 10 -4 -9 70.09 7.02 10 -4 -8 13.42 3.91 10 -4 -7 27.86 4.91 10 -4 -6 40.27 5.93 10 -4 -5 98.09 9.30 10 -4 -4 30.13 5.56 10 -4 -3 103.53 9.64 10 -4 -2 36.67 6.04 10 -4 -1 84.03 8.60 10 -4 0 35.74 5.93 10 -4 1 80.93 8.40 10 -4 1 97.57 8.86 10 -4 2 24.99 4.82 10 -4 2 20.70 4.48 10 -4 3 61.26 7.26 10 -4 3 62.97 7.13 10 -4 4 -0.71 2.38 10 -4 4 1.39 2.57 10 -4 5 32.80 4.85 10 -4 5 17.73 3.94 10 -4 6 23.51 4.07 10 -4 6 29.75 4.24 10 -4 7 50.18 4.99 10 -4 7 62.29 5.46 10 -5 -11 38.04 4.08 10 -5 -10 3.41 2.35 10 -5 -9 25.47 4.26 10 -5 -8 69.48 6.82 10 -5 -7 19.65 4.09 10 -5 -6 54.55 6.36 10 -5 -5 14.33 4.26 10 -5 -4 92.36 8.48 10 -5 -3 0.72 2.32 10 -5 -3 2.22 2.89 10 -5 -2 319.11 17.15 10 -5 -2 355.79 17.92 10 -5 -2 347.25 17.82 10 -5 -1 36.51 5.55 10 -5 -1 32.70 5.19 10 -5 0 214.39 13.27 10 -5 1 0.72 2.67 10 -5 1 0.67 2.32 10 -5 2 44.61 5.78 10 -5 2 46.26 5.71 10 -5 3 49.96 5.82 10 -5 3 45.54 5.61 10 -5 4 64.06 6.40 10 -5 4 65.63 6.41 10 -5 5 14.52 3.14 10 -5 5 15.65 3.26 10 -5 6 53.41 5.16 10 -5 6 54.87 5.08 10 -6 -9 125.32 7.66 10 -6 -8 96.82 6.89 10 -6 -8 94.26 6.78 10 -6 -7 40.53 4.82 10 -6 -7 40.83 4.83 10 -6 -7 36.13 4.73 10 -6 -6 -1.09 2.18 10 -6 -6 4.30 2.40 10 -6 -6 3.48 2.38 10 -6 -5 23.31 4.05 10 -6 -5 25.31 4.20 10 -6 -5 22.74 4.23 10 -6 -4 41.01 5.05 10 -6 -4 43.60 5.29 10 -6 -4 51.43 5.89 10 -6 -3 26.29 4.30 10 -6 -3 26.29 4.38 10 -6 -3 21.00 3.89 10 -6 -2 56.45 6.15 10 -6 -1 65.01 6.53 10 -6 0 32.33 4.49 10 -6 0 30.65 4.44 10 -6 1 -0.57 1.89 10 -6 2 29.25 4.07 10 -6 2 29.21 4.15 10 -6 3 11.85 2.88 10 -6 3 11.58 2.68 10 -6 4 28.60 3.83 10 -6 4 30.30 3.90 10 -7 -6 14.59 2.70 10 -7 -6 16.53 2.87 10 -7 -5 3.46 1.93 10 -7 -5 2.27 1.77 10 -7 -4 0.45 1.75 10 -7 -4 0.96 2.01 10 -7 -3 75.20 6.24 10 -7 -3 47.56 4.95 10 -7 -2 5.00 2.19 10 -7 -2 0.98 1.95 10 -7 -1 53.85 5.10 10 -7 -1 60.33 5.45 10 -7 0 26.31 3.52 11 0 -12 2.67 2.18 11 0 -11 169.02 10.26 11 0 -10 -0.61 2.52 11 0 -9 202.91 12.55 11 0 -8 -0.74 2.80 11 0 -7 374.11 19.16 11 0 -6 0.82 3.04 11 0 -5 202.90 13.62 11 0 -4 -2.61 4.04 11 0 -3 250.15 15.58 11 0 -2 -0.88 3.78 11 0 -1 195.27 13.64 11 0 0 -2.58 3.69 11 0 1 58.38 7.18 11 0 2 1.59 3.02 11 0 3 21.70 4.53 11 0 4 0.69 2.46 11 0 5 19.71 3.97 11 0 5 22.31 4.10 11 0 6 -0.48 1.72 11 0 6 -1.48 1.65 11 0 7 17.77 2.89 11 -1 -12 24.94 3.46 11 1 -12 20.96 3.35 11 -1 -11 40.01 4.72 11 1 -11 36.85 4.67 11 -1 -10 69.70 6.69 11 1 -10 72.50 6.75 11 -1 -9 98.09 8.16 11 1 -9 88.28 8.02 11 -1 -8 47.57 6.18 11 1 -8 53.02 6.51 11 -1 -7 22.71 5.01 11 1 -7 19.37 4.47 11 -1 -6 49.15 6.78 11 1 -6 33.29 5.73 11 -1 -5 93.40 8.95 11 1 -5 91.67 9.05 11 -1 -4 61.25 7.61 11 1 -4 72.20 8.09 11 -1 -3 8.49 4.43 11 1 -3 5.22 3.65 11 -1 -2 249.18 15.38 11 1 -2 228.04 14.93 11 1 -1 81.08 8.82 11 -1 -1 56.53 7.54 11 -1 0 154.02 11.89 11 1 0 178.43 12.61 11 -1 1 82.52 8.35 11 1 1 87.43 8.66 11 -1 2 21.43 4.71 11 1 2 13.25 4.03 11 -1 3 46.66 5.97 11 1 3 51.11 6.20 11 -1 4 6.98 2.73 11 -1 4 3.29 2.50 11 1 4 7.35 2.80 11 -1 5 8.16 2.72 11 1 5 6.65 2.59 11 -1 5 15.19 3.38 11 -1 5 17.60 3.68 11 1 5 10.72 3.21 11 -1 6 12.71 2.89 11 -1 6 18.17 3.15 11 1 6 16.63 3.18 11 -2 -11 22.39 3.37 11 2 -11 15.47 3.17 11 -2 -10 28.10 4.13 11 2 -10 18.78 3.80 11 -2 -9 173.78 10.69 11 2 -9 170.46 10.73 11 -2 -8 92.76 7.91 11 2 -8 97.93 8.42 11 -2 -7 75.04 7.67 11 2 -7 99.93 8.70 11 -2 -6 18.43 3.95 11 -2 -6 23.69 4.48 11 2 -6 24.09 4.75 11 -2 -5 18.01 4.35 11 -2 -5 20.88 4.55 11 2 -5 20.29 4.50 11 -2 -4 35.24 5.30 11 -2 -4 24.43 5.26 11 2 -4 30.35 5.64 11 -2 -3 130.92 10.29 11 -2 -3 118.24 10.07 11 2 -3 134.06 10.69 11 -2 -2 57.27 6.98 11 2 -2 61.37 7.30 11 -2 -1 18.40 4.31 11 2 -1 15.97 4.19 11 -2 0 16.59 4.08 11 -2 0 16.13 3.80 11 -2 0 25.52 4.63 11 2 0 21.83 4.55 11 -2 1 136.61 10.19 11 -2 1 130.51 9.88 11 -2 1 147.82 10.56 11 2 1 114.10 9.67 11 -2 2 30.22 4.79 11 -2 2 30.79 5.10 11 -2 2 27.47 4.89 11 2 2 23.42 4.55 11 -2 3 65.53 6.71 11 2 3 61.29 6.60 11 -2 3 69.05 6.76 11 -2 4 13.70 3.34 11 -2 4 11.60 3.13 11 2 4 12.53 3.17 11 -2 5 120.19 7.89 11 -2 5 134.76 8.54 11 -2 5 117.96 8.10 11 2 5 108.59 7.91 11 -2 6 40.37 4.52 11 -3 -9 169.81 9.82 11 -3 -8 21.19 3.87 11 -3 -7 21.40 4.02 11 -3 -6 16.39 3.96 11 -3 -5 30.36 5.08 11 -3 -4 87.28 8.10 11 -3 -3 48.27 6.28 11 -3 -1 8.05 3.28 11 -3 0 13.53 3.73 11 -3 1 188.79 11.94 11 -3 1 172.21 11.10 11 -3 2 12.77 3.40 11 -3 2 15.46 3.52 11 -3 3 57.68 5.98 11 -3 3 60.68 6.17 11 -3 4 -0.51 1.83 11 -3 4 2.12 2.12 11 -3 5 59.03 5.39 11 -4 -9 35.33 4.19 11 -4 -8 38.74 4.70 11 -4 -7 99.00 7.60 11 -4 -6 0.59 2.10 11 -4 -5 28.43 4.46 11 -4 -4 44.74 5.76 11 -4 -3 55.44 6.22 11 -4 -3 56.59 6.29 11 -4 -2 91.74 7.98 11 -4 -1 96.23 8.24 11 -4 0 32.77 4.80 11 -4 1 0.60 2.09 11 -4 1 5.97 2.38 11 -4 2 12.39 3.08 11 -4 2 13.70 2.92 11 -4 3 41.43 4.78 11 -4 3 47.82 5.04 11 -4 4 62.90 5.45 11 -4 4 64.87 5.43 11 -5 -8 -0.40 1.64 11 -5 -8 -0.79 1.73 11 -5 -7 47.54 4.87 11 -5 -7 44.30 4.64 11 -5 -6 29.72 3.96 11 -5 -6 19.60 3.54 11 -5 -5 54.63 5.47 11 -5 -5 40.48 4.80 11 -5 -4 18.28 3.55 11 -5 -4 15.62 3.39 11 -5 -4 16.07 3.17 11 -5 -3 26.76 3.96 11 -5 -3 21.89 3.53 11 -5 -2 6.42 2.42 11 -5 -2 2.60 2.03 11 -5 -1 82.05 6.72 11 -5 0 14.20 3.00 11 -5 1 103.94 7.41 11 -5 2 11.19 2.58 11 -5 2 9.79 2.26 12 0 -9 -0.43 1.94 12 0 -8 107.68 7.51 12 0 -7 1.06 2.18 12 0 -6 320.41 15.47 12 0 -5 1.20 2.57 12 0 -4 168.37 10.71 12 0 -3 -1.87 2.95 12 0 -2 13.08 3.79 12 0 -1 -0.61 2.73 12 0 0 18.81 3.86 12 0 1 1.11 1.98 12 0 2 1.42 2.03 12 0 2 9.69 2.81 12 0 3 -0.86 1.76 12 0 3 -0.45 1.72 12 -1 -8 51.95 5.06 12 1 -8 46.70 4.95 12 -1 -7 64.98 5.94 12 1 -7 69.65 6.13 12 -1 -6 30.82 4.26 12 1 -6 26.58 4.10 12 -1 -5 1.14 2.27 12 1 -5 0.58 2.55 12 -1 -4 83.86 7.40 12 1 -4 84.72 7.33 12 -1 -3 17.23 3.89 12 1 -3 12.18 3.67 12 -1 -2 23.91 3.97 12 -1 -2 30.79 4.71 12 1 -2 33.96 4.97 12 -1 -1 62.05 6.11 12 1 -1 54.63 5.94 12 -1 0 8.92 2.87 12 1 0 6.28 2.75 12 -1 1 6.22 2.23 12 -1 1 2.10 2.15 12 1 1 3.75 2.25 12 -1 2 46.74 4.82 12 -1 2 55.71 5.32 12 1 2 50.07 5.14 12 -1 3 10.19 2.34 12 1 3 8.05 2.05 12 -1 3 12.34 2.67 12 -1 3 11.46 2.62 12 1 3 11.70 2.56 12 -2 -7 23.08 3.42 12 2 -7 24.27 3.74 12 -2 -6 37.16 4.47 12 2 -6 36.65 4.44 12 -2 -5 12.80 2.98 12 2 -5 17.56 3.42 12 -2 -4 24.46 3.83 12 2 -4 20.29 3.69 12 -2 -3 -2.07 2.61 12 2 -3 1.08 2.27 12 -2 -2 18.09 3.44 12 -2 -2 23.65 3.89 12 2 -2 21.57 3.78 12 -2 -1 19.97 3.41 12 -2 -1 20.56 3.49 12 2 -1 20.49 3.62 12 -2 0 8.16 2.40 12 -2 0 9.57 2.71 12 2 0 6.50 2.46 12 -2 1 47.06 4.73 12 2 1 42.26 4.60 12 -2 1 38.28 4.37 12 -2 2 8.59 2.21 12 -3 -4 9.06 2.67 12 -3 -3 15.98 3.15 12 -3 -2 54.80 5.27 12 -3 -1 4.19 2.24 12 -3 0 33.34 3.97 0 0 0 0.00 0.00 TITL i1188 CuCl2_auto in Pn REM Pn (#7 in standard setting) CELL 1.54184 10.446327 10.014317 16.073370 90.0000 99.0905 90.0000 ZERR 28.00 0.000084 0.000086 0.000130 0.0000 0.0008 0.0000 LATT -1 SYMM x+1/2,-y, z+1/2 SFAC Cl Cu UNIT 28.00 28.00 REM CrysAlisPro recorded range (K): Min=296.3; max=296.6; aver:296.4 TEMP 23 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 47486 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ;