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oai:ojs.www.eurjchem.com:article/207 2011-04-06T05:42:05Z eurjchem:ART driver

Synthesis, characterization and crystal structure of ethyl 4-(3-chloro benzamido)benzoate Saeed, Aamer Rafique, Hummera Flörke, Ulrich Ethyl 4-(3-chlorobenzamido)benzoate Crystal structure Synthesis Characterization The title compound was efficiently synthesized in two steps starting from esterification of 4-aminobenzoic acid followed by amidation with 3-chlorobenzoyl chloride in dry tetrahydrofuran. The structure was confirmed by spectroscopic data and elemental analysis. The molecular structure was determined from single crystal X-ray diffraction data. It crystallizes in the triclinic space group P-1 with Z = 2 and unit cell dimensions a = 5.2941(15) Å, b = 8.157(2) Å, c = 16.238(4) Å, α = 82.682(6)°, β = 84.481(6)°, γ = 80.100(6)° and V = 683.2(3) Å3. Atlanta Publishing House LLC 2010-12-22 info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion application/pdf application/octet-stream https://www.eurjchem.com/index.php/eurjchem/article/view/207 10.5155/eurjchem.1.4.289-290.207 European Journal of Chemistry; Vol. 1 No. 4 (2010): December 2010; 289-290 2153-2257 2153-2249 eng https://www.eurjchem.com/index.php/eurjchem/article/view/207/PDF https://www.eurjchem.com/index.php/eurjchem/article/view/207/2523