2024-03-29T10:13:31Z
https://www.eurjchem.com/index.php/eurjchem/oai
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2011-04-06T05:42:05Z
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Synthesis, characterization and crystal structure of ethyl 4-(3-chloro benzamido)benzoate
Saeed, Aamer
Rafique, Hummera
Flörke, Ulrich
Ethyl 4-(3-chlorobenzamido)benzoate
Crystal structure
Synthesis
Characterization
The title compound was efficiently synthesized in two steps starting from esterification of 4-aminobenzoic acid followed by amidation with 3-chlorobenzoyl chloride in dry tetrahydrofuran. The structure was confirmed by spectroscopic data and elemental analysis. The molecular structure was determined from single crystal X-ray diffraction data. It crystallizes in the triclinic space group P-1 with Z = 2 and unit cell dimensions a = 5.2941(15) Å, b = 8.157(2) Å, c = 16.238(4) Å, α = 82.682(6)°, β = 84.481(6)°, γ = 80.100(6)° and V = 683.2(3) Å3.
Atlanta Publishing House LLC
2010-12-22
info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
application/pdf
application/octet-stream
https://www.eurjchem.com/index.php/eurjchem/article/view/207
10.5155/eurjchem.1.4.289-290.207
European Journal of Chemistry; Vol. 1 No. 4 (2010): December 2010; 289-290
2153-2257
2153-2249
eng
https://www.eurjchem.com/index.php/eurjchem/article/view/207/PDF
https://www.eurjchem.com/index.php/eurjchem/article/view/207/2523