European Journal of Chemistry 2014, 5(4), 563-569 | doi: https://doi.org/10.5155/eurjchem.5.4.563-569.1083 | Get rights and content






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Synthesis and corrosion inhibition evaluation of novel aminic nitrogen-bearing 1,2,4-triazole Schiff base compounds


Wael Abdel Gayed Ahmed Arafa (1) , Nady Hashem El-Sayed (2,*)

(1) Chemistry Department, Faculty of Science, Fayoum University, Fayoum City, 63514, Egypt
(2) Chemistry Department, Faculty of Science, Fayoum University, Fayoum City, 63514, Egypt
(*) Corresponding Author

Received: 23 Apr 2014 | Revised: 15 Jun 2014 | Accepted: 15 Jun 2014 | Published: 31 Dec 2014 | Issue Date: December 2014

Abstract


Simple, effective, and high yield synthetic procedure for the synthesis of Schiff bases 5a-c is described. The scope of this reaction was investigated and noted that the presence of nickel(II) nitrate hexahydrate gave the corresponding Schiff bases in excellent yields. The inhibition effects of N-((1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-5-yl)methylene)-4H-1,2,4-triazol-3-amine (PTP), 5c, have been investigated against the corrosion of copper in 0.5 M HCl solution. The investigations were accomplished using potentiodynamic polarization and electrochemical impedance measurements. Potentiodynamic polarization measurements indicated that the examined compound is mixed-type inhibitor. The results of electrochemical impedance indicated that the values of the charge transfer resistance and the inhibition efficiency tend to be increased by increasing the inhibitor concentration.


Keywords


EIS; Copper; Inhibitor; Schiff base; Polarization; Heterocycles

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DOI: 10.5155/eurjchem.5.4.563-569.1083

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[2]. A. Espinoza-Vázquez, F. J. Rodríguez-Gómez, R. Mata, A. Madariaga-Mazón, D. Ángeles-Beltrán
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How to cite


Arafa, W.; El-Sayed, N. Eur. J. Chem. 2014, 5(4), 563-569. doi:10.5155/eurjchem.5.4.563-569.1083
Arafa, W.; El-Sayed, N. Synthesis and corrosion inhibition evaluation of novel aminic nitrogen-bearing 1,2,4-triazole Schiff base compounds. Eur. J. Chem. 2014, 5(4), 563-569. doi:10.5155/eurjchem.5.4.563-569.1083
Arafa, W., & El-Sayed, N. (2014). Synthesis and corrosion inhibition evaluation of novel aminic nitrogen-bearing 1,2,4-triazole Schiff base compounds. European Journal of Chemistry, 5(4), 563-569. doi:10.5155/eurjchem.5.4.563-569.1083
Arafa, Wael, & Nady Hashem El-Sayed. "Synthesis and corrosion inhibition evaluation of novel aminic nitrogen-bearing 1,2,4-triazole Schiff base compounds." European Journal of Chemistry [Online], 5.4 (2014): 563-569. Web. 15 Aug. 2020
Arafa, Wael, AND El-Sayed, Nady. "Synthesis and corrosion inhibition evaluation of novel aminic nitrogen-bearing 1,2,4-triazole Schiff base compounds" European Journal of Chemistry [Online], Volume 5 Number 4 (31 December 2014)

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DOI Link: https://doi.org/10.5155/eurjchem.5.4.563-569.1083

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