European Journal of Chemistry 2014, 5(3), 394-396 | doi: https://doi.org/10.5155/eurjchem.5.3.394-396.1043 | Get rights and content

Issue cover





  Open Access OPEN ACCESS | Open Access PEER-REVIEWED | RESEARCH ARTICLE | DOWNLOAD PDF | VIEW FULL-TEXT PDF | TOTAL VIEWS

Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide


Riya Datta (1,*) , Ramya Vittalacharya (2) , Bubbly Shivappa Gudennavar (3)

(1) Department of Chemistry, Christ University, Bangalore-560029, India
(2) Department of Chemistry, Christ University, Bangalore-560029, India
(3) Department of Physics, Christ University, Bangalore-560029, India
(*) Corresponding Author

Received: 06 Mar 2014 | Accepted: 07 Mar 2014 | Published: 30 Sep 2014 | Issue Date: September 2014

Abstract


A new compound, N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide was synthesized. Elemental analysis, IR spectrum, 1H NMR and X-ray crystal structure studies were carried out to determine the compositions and molecular structure of the compound. It crystallizes in the orthorhombic space group Pbca with unit cell parameters a = 11.3142(4) Å, b = 7.5526(2) Å and c = 22.9030(9) Å. The crystal structure studies reveal intermolecular N-H···O hydrogen bonding interactions in the solid state.


Keywords


IR; NMR; Furfural; Crystal structure; Acylhydrazone; p-Chlorobenzhydrazide

Full Text:

PDF
PDF    Open Access

DOI: 10.5155/eurjchem.5.3.394-396.1043

Links for Article


| | | | | | |

| | | | | | |

| | | |

Related Articles




Article Metrics

icon graph This Abstract was viewed 974 times | icon graph PDF Article downloaded 365 times

Funding information


Centre for Research, Christ University, Bangalore, India; Indian Institute of Technology, Madras, India; IISC, Bangalore, India

Citations

/


[1]. Thierno Moussa Seck, Fatou Dieng Faye, Aissatou Alioune Gaye, Ibrahima Elhadji Thiam, Ousmane Diouf, Mohamed Gaye, Pascal Retailleau
Synthesis of mono and bis-substituted asymmetrical compounds, (1-(pyridin-2-yl)ethylidene)carbonohydrazide and 1-(2'-hydroxybenzylidene)-5-(1'-pyridylethylidene)carbonohydrazone: Structural characterization and antioxidant activity study
European Journal of Chemistry  11(4), 285, 2020
DOI: 10.5155/eurjchem.11.4.285-290.2023
/


[2]. Alice Prudente Borges, Claudia Cristina Gatto, Victor Marcelo Deflon, Pedro Ivo Da Silva Maia
A dimeric oxidovanadium(V) complex derived from a hydrazonate ligand with an unusual asymmetrically bridged μ-(oxido)μ-(H2O){oxidovanadium(V)}2 core
European Journal of Chemistry  11(1), 1, 2020
DOI: 10.5155/eurjchem.11.1.1-5.1948
/


References


[1]. Mariana-Moldovan, C.; Oniga, O.; Parvu, A.; Tiperciuc, B.; Verite, P.; Pirnau, A.; Crisan, O.; Bojit, M.; Pop, R. Eur. J. Med. Chem. 2011, 46, 526-534.
http://dx.doi.org/10.1016/j.ejmech.2010.11.032

[2]. Rollas, S.; Kucukguzel, S. G. Molecules 2007, 12, 1910-1939.
http://dx.doi.org/10.3390/12081910

[3]. Cocco, M. T.; Congiu, C.; Onnis, V.; Pusceddo, M. C.; Schivo, M. L.; De Logu, A. Eur. J. Med. Chem. 1999, 34, 1071-1076.
http://dx.doi.org/10.1016/S0223-5234(99)00124-5

[4]. Sriram, D.; Yogeeswari, P.; Madhu, K. Bioorg. Med. Chem. Lett. 2005, 15, 4502-4505.
http://dx.doi.org/10.1016/j.bmcl.2005.07.011

[5]. Kucukguzel, S. G.; Rollas, S.; Erdeniz, H.; Kiraz, M.; Ekinci, A. C.; Vidin, A. Eur. J. Med. Chem. 2000, 35, 761-771.
http://dx.doi.org/10.1016/S0223-5234(00)90179-X

[6]. Chornous, V. A.; Bratenko, M. K.; Vovk, M. V.; Sidorchuk, I. I. Pharma. Chem. J. 2001, 35, 26-28.
http://dx.doi.org/10.1023/A:1010432029236

[7]. Melnyk, P.; Leroux, V.; Sergheraert, C.; Grellier, P. Bioorg. Med. Chem. Lett. 2006, 16, 31-35.
http://dx.doi.org/10.1016/j.bmcl.2005.09.058

[8]. Krishnamoorthy, P.; Sathyadevi, P.; Senthilkumar K.; Thomas-Muthiah, P.; Ramesh, R.; Dharmaraj, N. Inorg. Chem. Commun. 2011, 14, 1318-1322.
http://dx.doi.org/10.1016/j.inoche.2011.05.004

[9]. Hosseini-Monfared, H.; Kheirabadi, S.; Asghari-Lalami, N.; Mayer, P. Polyhedron 2011, 30, 1375-1384.
http://dx.doi.org/10.1016/j.poly.2011.02.005

[10]. Emmanuel, J.; Sithambarean, M.; Kurup, M. R. P. Acta Cryst. E 2011, 67, o3267-o3267.
http://dx.doi.org/10.1107/S1600536811046381

[11]. Chang, J. G.; He, G. F.; Li, Y. F. Acta Cryst. E 2007, 63, o3997-o3997.
http://dx.doi.org/10.1107/S1600536807043085

[12]. Ali, H. M.; Puvaneswary, S.; Ng, S. W. Acta Cryst. E 2005, 61, o3464-o3464.
http://dx.doi.org/10.1107/S1600536805030497

[13]. Sheldrick, G. M. SHELX97. University of Göttingen, Germany, 1997.

[14]. Song, M. Z.; Fan, C. G. Acta Cryst. E 2009, 65, o2800-o2800.
http://dx.doi.org/10.1107/S1600536809042251

[15]. Nair, Y.; Sithambaresan, M.; Kurup, M. R. P. Acta Cryst. E 2012, 68, o2709-o2709.
http://dx.doi.org/10.1107/S1600536812035179

[16]. Datta, R.; Ramya, V.; Sithambaresan, M.; Kurup, M. R. P. Acta Cryst. E 2013, 69, o1549-o1549.

[17]. Datta, R.; Ramya, V.; Sithambaresan, M.; Kurup, M. R. P. Acta Cryst. E 2014, 70, o242-o242.
http://dx.doi.org/10.1107/S1600536814001822


Supporting information


The Supplementary Material for this article can be found online at: Supplementary files

How to cite


Datta, R.; Vittalacharya, R.; Gudennavar, B. Eur. J. Chem. 2014, 5(3), 394-396. doi:10.5155/eurjchem.5.3.394-396.1043
Datta, R.; Vittalacharya, R.; Gudennavar, B. Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide. Eur. J. Chem. 2014, 5(3), 394-396. doi:10.5155/eurjchem.5.3.394-396.1043
Datta, R., Vittalacharya, R., & Gudennavar, B. (2014). Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide. European Journal of Chemistry, 5(3), 394-396. doi:10.5155/eurjchem.5.3.394-396.1043
Datta, Riya, Ramya Vittalacharya, & Bubbly Shivappa Gudennavar. "Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide." European Journal of Chemistry [Online], 5.3 (2014): 394-396. Web. 1 Dec. 2021
Datta, Riya, Vittalacharya, Ramya, AND Gudennavar, Bubbly. "Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide" European Journal of Chemistry [Online], Volume 5 Number 3 (30 September 2014)

The other citation formats (EndNote | Reference Manager | ProCite | BibTeX | RefWorks) for this article can be found online at: How to cite item



DOI Link: https://doi.org/10.5155/eurjchem.5.3.394-396.1043

CrossRef | Scilit | GrowKudos | Researchgate | Publons | Microsoft | scibey | Scite | Lens | OUCI

WorldCat Paperbuzz | LibKey Citeas | Dimensions | Semanticscholar | Plumx | Kopernio | Zotero | Mendeley

ZoteroSave to Zotero MendeleySave to Mendeley



European Journal of Chemistry 2014, 5(3), 394-396 | doi: https://doi.org/10.5155/eurjchem.5.3.394-396.1043 | Get rights and content

Refbacks

  • There are currently no refbacks.




Copyright (c)





© Copyright 2010 - 2021  Atlanta Publishing House LLC All Right Reserved.

The opinions expressed in all articles published in European Journal of Chemistry are those of the specific author(s), and do not necessarily reflect the views of Atlanta Publishing House LLC, or European Journal of Chemistry, or any of its employees.

Copyright 2010-2021 Atlanta Publishing House LLC. All rights reserved. This site is owned and operated by Atlanta Publishing House LLC whose registered office is 2850 Smith Ridge Trce Peachtree Cor GA 30071-2636, USA. Registered in USA.