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Synthesis, characterization and crystal structure of N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide
Riya Datta (1,*)
, Ramya Vittalacharya (2) , Bubbly Shivappa Gudennavar (3) (1) Department of Chemistry, Christ University, Bangalore-560029, India
(2) Department of Chemistry, Christ University, Bangalore-560029, India
(3) Department of Physics, Christ University, Bangalore-560029, India
(*) Corresponding Author
Received: 06 Mar 2014 | Accepted: 07 Mar 2014 | Published: 30 Sep 2014 | Issue Date: September 2014
Abstract
A new compound, N'-[(E)-furan-2-ylmethylidene]furan-2-carbohydrazide was synthesized. Elemental analysis, IR spectrum, 1H NMR and X-ray crystal structure studies were carried out to determine the compositions and molecular structure of the compound. It crystallizes in the orthorhombic space group Pbca with unit cell parameters a = 11.3142(4) Å, b = 7.5526(2) Å and c = 22.9030(9) Å. The crystal structure studies reveal intermolecular N-H···O hydrogen bonding interactions in the solid state.
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European Journal of Chemistry
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DOI: 10.5155/eurjchem.5.3.394-396.1043
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Centre for Research, Christ University, Bangalore, India; Indian Institute of Technology, Madras, India; IISC, Bangalore, India
Citations
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Synthesis of mono and bis-substituted asymmetrical compounds, (1-(pyridin-2-yl)ethylidene)carbonohydrazide and 1-(2'-hydroxybenzylidene)-5-(1'-pyridylethylidene)carbonohydrazone: Structural characterization and antioxidant activity study
European Journal of Chemistry 11(4), 285, 2020
DOI: 10.5155/eurjchem.11.4.285-290.2023
[2]. Alice Prudente Borges, Claudia Cristina Gatto, Victor Marcelo Deflon, Pedro Ivo Da Silva Maia
A dimeric oxidovanadium(V) complex derived from a hydrazonate ligand with an unusual asymmetrically bridged μ-(oxido)μ-(H2O){oxidovanadium(V)}2 core
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DOI: 10.5155/eurjchem.11.1.1-5.1948
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DOI Link: https://doi.org/10.5155/eurjchem.5.3.394-396.1043
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European Journal of Chemistry 2014, 5(3), 394-396 | doi: https://doi.org/10.5155/eurjchem.5.3.394-396.1043 | Get rights and content
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