European Journal of Chemistry

Flame atomic absorption determination of ultra-trace zinc in environmental samples after pre-concentration by solid phase extraction

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Published: Sep 30, 2017
DOI: https://doi.org/10.5155/eurjchem.8.3.305-309.1587
Keywords:
Zinc, Schiff base, Octadecyl silica disks, Solid phase extraction, Atomic absorption spectrometry, N, N´-Bis(salicylidene)1, 8-diamino-3, 6-dioxaoctan
Section
Research Article
Issue
Vol. 8 No. 3 (2017): September 2017
Dates
Received 2017-05-21
Accepted 2017-07-29
Published 2017-09-30


Main Article Content

Mahmood Payehghadr
Department of Chemistry, Payame Noor University, P.O. Box 19395-4697, Tehran, Iran

Abstract

A simple, reliable and rapid method for pre-concentration and determination of ultra-trace zinc using octadecyl silica membrane disk modified by a new Schiff base ligand, and flame atomic absorption spectrometry is presented. Various parameters including, pH of aqueous solution, flow rates, the amount of ligand and type of stripping solvents were optimized. The breakthrough volume is greater than 1000 mL with an enrichment factor of more than 200 and 120 ng/Ldetection limit. The capacity of the membrane disks modified by 8 mg of the ligand was found to be 260 µg of zinc. The effects of various cationic interferences on percent recovery of zinc ion were studied. The method was successfully applied for the determination of zinc ion in different samples, especially determination of ultra-trace amount of zinc in waters and plants.


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Payehghadr, M. Flame Atomic Absorption Determination of Ultra-Trace Zinc in Environmental Samples After Pre-Concentration by Solid Phase Extraction. Eur. J. Chem. 2017, 8, 305-309.

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Supporting Agencies

Payame Noor University, P.O. Box 19395-4697, Tehran, Iran
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