European Journal of Chemistry 2017, 8(3), 305-309 | doi: https://doi.org/10.5155/eurjchem.8.3.305-309.1587 | Get rights and content






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Flame atomic absorption determination of ultra-trace zinc in environmental samples after pre-concentration by solid phase extraction


Mahmood Payehghadr (1,*)

(1) Department of Chemistry, Payame Noor University, P.O. Box 19395-4697, Tehran, Iran
(*) Corresponding Author

Received: 21 May 2017 | Revised: 30 Jun 2017 | Accepted: 29 Jul 2017 | Published: 30 Sep 2017 | Issue Date: September 2017

Abstract


A simple, reliable and rapid method for pre-concentration and determination of ultra-trace zinc using octadecyl silica membrane disk modified by a new Schiff base ligand, and flame atomic absorption spectrometry is presented. Various parameters including, pH of aqueous solution, flow rates, the amount of ligand and type of stripping solvents were optimized. The breakthrough volume is greater than 1000 mL with an enrichment factor of more than 200 and 120 ng/Ldetection limit. The capacity of the membrane disks modified by 8 mg of the ligand was found to be 260 µg of zinc. The effects of various cationic interferences on percent recovery of zinc ion were studied. The method was successfully applied for the determination of zinc ion in different samples, especially determination of ultra-trace amount of zinc in waters and plants.


Keywords


Zinc; Schiff base; Octadecyl silica disks; Solid phase extraction; Atomic absorption spectrometry; N,N´-Bis(salicylidene)1,8-diamino-3,6-dioxaoctan

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DOI: 10.5155/eurjchem.8.3.305-309.1587

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Funding information


Payame Noor University, P.O. Box 19395-4697, Tehran, Iran

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How to cite


Payehghadr, M. Eur. J. Chem. 2017, 8(3), 305-309. doi:10.5155/eurjchem.8.3.305-309.1587
Payehghadr, M. Flame atomic absorption determination of ultra-trace zinc in environmental samples after pre-concentration by solid phase extraction. Eur. J. Chem. 2017, 8(3), 305-309. doi:10.5155/eurjchem.8.3.305-309.1587
Payehghadr, M. (2017). Flame atomic absorption determination of ultra-trace zinc in environmental samples after pre-concentration by solid phase extraction. European Journal of Chemistry, 8(3), 305-309. doi:10.5155/eurjchem.8.3.305-309.1587
Payehghadr, Mahmood. "Flame atomic absorption determination of ultra-trace zinc in environmental samples after pre-concentration by solid phase extraction." European Journal of Chemistry [Online], 8.3 (2017): 305-309. Web. 25 May. 2020
Payehghadr, Mahmood. "Flame atomic absorption determination of ultra-trace zinc in environmental samples after pre-concentration by solid phase extraction" European Journal of Chemistry [Online], Volume 8 Number 3 (30 September 2017)

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DOI Link: https://doi.org/10.5155/eurjchem.8.3.305-309.1587

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