

Crystal structure of (2E)-1-(4-hydroxyphenyl)-3-(4-methoxyphenyl)prop-2-en-1-one
Fatma Yesilyurt (1)





(1) Department of Pharmaceutical Chemistry, Faculty of Pharmacy, Ataturk University, 25240 Erzurum, Turkey
(2) Department of Mathematics and Science Education, Faculty of Education, Kastamonu University, 37200 Kastamonu, Turkey
(3) Department of Pharmaceutical Chemistry, Faculty of Pharmacy, Ataturk University, 25240 Erzurum, Turkey
(4) Department of Physics, Faculty of Sciences, Erciyes University, 38039 Kayseri, Turkey
(5) Department of Physics, Arts and Sciences Faculty, Aksaray University, 68100 Aksaray, Turkey
(*) Corresponding Author
Received: 11 May 2018 | Revised: 25 May 2018 | Accepted: 25 May 2018 | Published: 30 Jun 2018 | Issue Date: June 2018
Abstract
The compound, C16H14O3, (except H atoms) is almost planar [r.m.s. deviations for all non-H atoms = 0.001 Å] and the dihedral angle between the aromatic rings is 9.35 (7)°. In the crystal, molecules are linked by intermolecular O—H···O and C—H···O hydrogen bonds, forming a three-dimensional network structure. Furthermore, a weak π-π stacking interactions [centroid-to-centroid distance = 3.7055 (9) Å] contributes to the stabilization of the molecular packing. Crystal Data for C16H14O3 (M = 254.27 g/mol): Orthorhombic, space group Pbca (no. 61), a = 13.4563(16) Å, b = 11.4986(14) Å, c = 16.720(2) Å, V = 2587.1(5) Å3, Z = 8, T = 296(2) K, μ(MoKα) = 0.090 mm-1, Dcalc = 1.306 g/cm3, 61402 reflections measured (4.88° ≤ 2Θ ≤ 56.76°), 3240 unique (Rint = 0.0334, Rsigma = 0.0120) which were used in all calculations. The final R1 was 0.0438 (I≥2σ(I)) and wR2 was 0.1228 (all data).
Announcements
Our editors have decided to support scientists to publish their manuscripts in European Journal of Chemistry without any financial constraints.
1- The article processing fee will not be charged from the articles containing the single-crystal structure characterization between July 1, 2022 and August 15, 2022 (Voucher code: SINGLE2022).
2. Young writers will not be charged for the article processing fee between July 1, 2022 and August 15, 2022 (Voucher code: YOUNG2022).
3. The article processing fee will not be charged from the articles containing a part of the PhD thesis between July 1, 2022 and August 15, 2022 (Voucher code: PhD2022).
Editor-in-Chief
European Journal of Chemistry
Keywords
Full Text:
PDF

DOI: 10.5155/eurjchem.9.2.147-150.1733
Links for Article
| | | | | | |
| | | | | | |
| | | |
Related Articles
Article Metrics


Funding information
Aksaray University, Science and Technology Application and Research Center, Aksaray, Turkey, for the use of the Bruker SMART BREEZE CCD diffractometer (Grant No. 2010K120480 of the State of Planning Organization)
Citations
[1]. Zhiyin Yu, Hao Jiang, Li Wang, Feng-Xian Yang, Jian-Ping Huang, Chongxi Liu, Xiaowei Guo, Wensheng Xiang, Sheng-Xiong Huang
Dimeric Pimprinine Alkaloids From Soil-Derived Streptomyces sp. NEAU-C99
Frontiers in Chemistry 8, , 2020
DOI: 10.3389/fchem.2020.00095

References
[1]. Das, U.; Gul, H. I.; Alcorn, J.; Shrivastav, A.; George, T.; Sharma, R. K.; Nienaber, K. H.; Clercq, E. D.; Balzarini, J.; Kawase, M.; Kan, N.; Tanaka, T.; Tani, S.; Werbovetz, K. A.; Yakovich, A. J.; Manavathu, E. K.; Stables, J. P.; Dimmock, J. R. Eur. J. Med. Chem. 2006, 41, 577-585.
https://doi.org/10.1016/j.ejmech.2005.12.014
[2]. Yerdelen, K. O.; Gul, H. I.; Sakagami, H.; Umemura, N.; Sukuroglu, M. Lett. Drug Des. Discov. 2015, 12, 643-649.
https://doi.org/10.2174/1570180812666150213225134
[3]. Gul, H. I.; Cizmecioglu, M.; Zencir, S.; Gul, M.; Canturk, P.; Atalay M.; Topcu, Z. J. Enzyme Inh. Med. Chem. 2009, 24, 804-807.
[4]. Gul, H. I.; Yerdelen, K. O.; Gul, M.; Das, U.; Pandit, B.; Li, P-K.; Secen H.; Sahin, F. Arch. Der Pharm. 2007, 340, 195-201.
https://doi.org/10.1002/ardp.200600072
[5]. Bilginer, S.; Gul, H. I.; Mete, E.; Das, U.; Sakagami, H.; Umemura, N.; Dimmock, J. R. J. Enzyme Inh. Med. Chem. 2013, 28, 974-980.
[6]. Bilginer, S.; Unluer, E.; Gul, H. I.; Mete, E.; Isik, S.; Vullo, D.; Ozensoy-Guler, O.; Beyaztas, S.; Capasso, C.; Supuran, C. T. J. Enzyme Inh. Med. Chem. 2014, 29, 495-499.
[7]. Yamali, C.; Tugrak, M.; Gul, H. I.; Tanc, M.; Supuran, C. T. J. Enzyme Inh. Med. Chem. 2016, 31, 1678-1681.
[8]. Singh, P.; Anand, A.; Kumar, V. Eur. J. Med. Chem. 2014, 85, 758-777.
https://doi.org/10.1016/j.ejmech.2014.08.033
[9]. Yerdelen, K. O. Synthesis and evaluation of the cytotoxic activities of the compounds 3-aryl-1-(4-hydroxyphenyl)-2-propen-1 ones and 1,5-diaryl-penta-1,4-dien-3-ones and their aminomethyl derivatives. PhD thesis, Institute of Medical Sciences, Ataturk University, Erzurum, Turkey, 2009.
[10]. Dimmock, J. R.; Kandepu, N. M.; Hetherington, M.; Quail, J. W.; Pugazhenthi, U.; Sudom, A. M.; Chamankhah, M.; Rose, P.; Pass, E.; Allen, T. M.; Halleran, S.; Szydlowski, J.; Mutus, B.; Tannous, M.; Manavathu, E. K.; Myers, T. G.; Clercq, E. D.; Balzarini, J. J. Med. Chem. 1998, 41, 1014-1026.
https://doi.org/10.1021/jm970432t
[11]. Bruker. APEX2 and SAINT. Bruker AXS Inc., Madison, Wisconsin, USA, 2007.
[12]. Bruker. SADABS. Bruker AXS Inc., Madison, Wisconsin, USA, 2012.
[13]. Sheldrick, G. M. Acta Cryst. A 2008, 64, 112-122.
https://doi.org/10.1107/S0108767307043930
[14]. Farrugia, L. J. J. Appl. Cryst. 2012, 45, 849-854.
https://doi.org/10.1107/S0021889812029111
[15]. Spek, A. L. Acta Cryst. D 2009, 65, 148-155.
https://doi.org/10.1107/S090744490804362X
[16]. Sarojini, B. K.; Yathirajan, H. S.; Mustafa, K.; Sarfraz, H.; Bolte, M. Acta Cryst. E 2007, 63, o4477-o4477.
https://doi.org/10.1107/S1600536807052737
[17]. Sathya, S.; Reuben Jonathan, D.; Prathebha, K.; Jovita, J.; Usha, G. Acta Cryst. E 2014, 70, o1158-o1159.
https://doi.org/10.1107/S1600536814021953
[18]. Allen, F. H.; Kennard, O.; Watson, D. G.; Brammer, L.; Orpen, A. G.; Taylor, R. J. Chem. Soc. Perkin Trans. 1987, 2, S1-19.
https://doi.org/10.1039/p298700000s1
Supporting information
The Supplementary Material for this article can be found online at: Supplementary files
How to cite
The other citation formats (EndNote | Reference Manager | ProCite | BibTeX | RefWorks) for this article can be found online at: How to cite item
DOI Link: https://doi.org/10.5155/eurjchem.9.2.147-150.1733


















European Journal of Chemistry 2018, 9(2), 147-150 | doi: https://doi.org/10.5155/eurjchem.9.2.147-150.1733 | Get rights and content
Refbacks
- There are currently no refbacks.
Copyright (c) 2018 Authors

This work is published and licensed by Atlanta Publishing House LLC, Atlanta, GA, USA. The full terms of this license are available at http://www.eurjchem.com/index.php/eurjchem/pages/view/terms and incorporate the Creative Commons Attribution-Non Commercial (CC BY NC) (International, v4.0) License (http://creativecommons.org/licenses/by-nc/4.0). By accessing the work, you hereby accept the Terms. This is an open access article distributed under the terms and conditions of the CC BY NC License, which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited without any further permission from Atlanta Publishing House LLC (European Journal of Chemistry). No use, distribution or reproduction is permitted which does not comply with these terms. Permissions for commercial use of this work beyond the scope of the License (http://www.eurjchem.com/index.php/eurjchem/pages/view/terms) are administered by Atlanta Publishing House LLC (European Journal of Chemistry).
© Copyright 2010 - 2022 • Atlanta Publishing House LLC • All Right Reserved.
The opinions expressed in all articles published in European Journal of Chemistry are those of the specific author(s), and do not necessarily reflect the views of Atlanta Publishing House LLC, or European Journal of Chemistry, or any of its employees.
Copyright 2010-2022 Atlanta Publishing House LLC. All rights reserved. This site is owned and operated by Atlanta Publishing House LLC whose registered office is 2850 Smith Ridge Trce Peachtree Cor GA 30071-2636, USA. Registered in USA.