

Determination of enantiomeric excess of leucine and valine by X-ray powder diffraction
Elżbieta Tadeusiak (1)





(1) Department of Structural Studies, Centre of Molecular and Macromolecular Studies, Polish Academy of Sciences, Sienkiewicza 112, Łódź, PL-90-363, Poland
(2) Department of X-ray Crystallography and Crystal Chemistry, Institute of General and Ecological Chemistry, Technical University of Łódź, Żeromskiego 116, Łódź, PL-90-924, Poland
(3) Department of X-ray Crystallography and Crystal Chemistry, Institute of General and Ecological Chemistry, Technical University of Łódź, Żeromskiego 116, Łódź, PL-90-924, Poland
(4) Department of X-ray Crystallography and Crystal Chemistry, Institute of General and Ecological Chemistry, Technical University of Łódź, Żeromskiego 116, Łódź, PL-90-924, Poland
(5) Department of X-ray Crystallography and Crystal Chemistry, Institute of General and Ecological Chemistry, Technical University of Łódź, Żeromskiego 116, Łódź, PL-90-924, Poland
(*) Corresponding Author
Received: 26 Jul 2010 | Accepted: 06 Aug 2010 | Published: 22 Dec 2010 | Issue Date: December 2010
Abstract
Two amino acids, leucine and valine, were studied by X-ray powder diffraction (XRPD). The linear correlations between intensity of racemate (decrease) or enantiomer (increase) and enantiomeric excesses were observed in each case.
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European Journal of Chemistry
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DOI: 10.5155/eurjchem.1.4.319-321.224
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Ministry of Science and Higher Education
Citations
[1]. María Mar Quesada-Moreno, Albert Virgili, Eva Monteagudo, Rosa M. Claramunt, Juan Ramón Avilés-Moreno, Juan Jesús López-González, Ibon Alkorta, José Elguero
A vibrational circular dichroism (VCD) methodology for the measurement of enantiomeric excess in chiral compounds in the solid phase and for the complementary use of NMR and VCD techniques in solution: the camphor case
The Analyst 143(6), 1406, 2018
DOI: 10.1039/C7AN01855J

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DOI Link: https://doi.org/10.5155/eurjchem.1.4.319-321.224

















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