European Journal of Chemistry

Synthesis and crystal structure of 2-methoxy-4,6-bis(4-nitrophenoxy)-1,3,5-triazine



Main Article Content

Huang Yuanyuan
Bai Fang
Gao Guowei
Men Jian

Abstract

The novel compound, 2-methoxy-4,6-bis(4-nitrophenoxy)-1,3,5-triazine has been synthesized starting from 2,4,6-trichloro-1,3,5-triazine and characterized by 1H NMR, 13C NMR, IR, mass spectroscopy and elemental analysis. The single crystal of the title compound was obtained and subjected to X-ray diffraction analysis. The single crystal data illustrates that it belongs to the monoclinic system, space group C2/c with a = 13.818(3) Å, b = 7.8964(16) Å, c = 30.718(6) Å, β = 96.52(3) o, V = 3330.0(12) Å3, Z = 8, Dc = 1.537 g/cm3, C16H11N5O7, Mr = 385.30, µ (MoKα) = 0.124 mm−1, F(000) = 1584, the final R = 0.0489 and wR = 0.1821 for 2491 observed reflections with I>2σ(I).

3_1_17_20_800


icon graph This Abstract was viewed 1340 times | icon graph Article PDF downloaded 690 times icon graph Article CIF FILE downloaded 0 times

How to Cite
(1)
Yuanyuan, H.; Fang, B.; Guowei, G.; Jian, M. Synthesis and Crystal Structure of 2-Methoxy-4,6-bis(4-Nitrophenoxy)-1,3,5-Triazine. Eur. J. Chem. 2012, 3, 17-20.

Article Details

Share
Crossref - Scopus - Google - European PMC
References

[1]. Chandra, R.; Rajabi, L. J. Macromol. Sci. Rev. Macromol. Chem. Phys. 1997, 37, 61-96.
http://dx.doi.org/10.1080/15321799708014733

[2]. Lee, H. N.; Rield, F. R. Mater. Soc. 1989, 13, 301-318.

[3]. Owusu, A. O.; Martin, G. C.; Gotro, J. T. Polym. Eng. Sci. 1991, 31, 1604-1609.
http://dx.doi.org/10.1002/pen.760312208

[4]. Takao, I.; Hidehiko, S. J. Appl. Polym. Sci. 1997, 65, 1349-1357.
http://dx.doi.org/10.1002/(SICI)1097-4628(19970815)65:7<1349::AID-APP12>3.0.CO;2-Q

[5]. Liu, Y. L.; Chen, Y. J.; Wei, W. L. Polym. 2003, 44, 6465-6473.
http://dx.doi.org/10.1016/j.polymer.2003.08.006

[6]. Watanabe, M.; Yoshie, N. Polym. 2006, 47, 4946-4952.
http://dx.doi.org/10.1016/j.polymer.2006.05.036

[7]. Lin, R. H.; Liu, Y. H.; Chen, Y. H.; Lee, A. C.; Ho, T. H. Eur. Polym. J. 2007, 43, 4197-4209.
http://dx.doi.org/10.1016/j.eurpolymj.2007.08.004

[8]. Lin, R. H.; Lu, W. H.; Lin, C. W. Polym. 2004, 45, 4423-4435.
http://dx.doi.org/10.1016/j.polymer.2004.04.050

[9]. Hwang, H. L.; Li, C. H.; Wang, C. S. Polym. 2006, 47, 1291-1299.
http://dx.doi.org/10.1016/j.polymer.2005.12.040

[10]. Liu, Y. L.; Chen, Y. J. Polym. 2004, 45, 1797-1804.
http://dx.doi.org/10.1016/j.polymer.2004.01.001

[11]. Fang, Q.; Li, G. Z.; Zeng, X.; Jiang, L. X. J. Appl. Polym. 2004, 93, 475-480.
http://dx.doi.org/10.1002/app.20467

[12]. Fang, Q.; Ding, X. M.; Wu, X. Y.; Jiang, L. X. Polym. 2001, 47, 7595-7602.
http://dx.doi.org/10.1016/S0032-3861(01)00274-9

[13]. Hao, J.; Jiang, L.; Cai, X. Polym. 1996, 16, 3721-3727.
http://dx.doi.org/10.1016/0032-3861(96)00186-3

[14]. Lin, J.; Yuki, Y.; Kunisada, H.; Kondo, S. J. Appl. Polym. 1990, 40, 2113-2122.
http://dx.doi.org/10.1002/app.1990.070401124

[15]. Saida, K.; Sakai, M.; Narahara, T. Japan Patent (Jpn Kokai Tokkyo Koho) 52 136 298 and 52 136 189, 1977.

[16]. Sheldrick G. M., SHELXS97. Program for Crystal Structure Solution, University of Göttingen, Germany, 1997.

[17]. Jetti. R. K. R.; Thallapally, P. K.; Nangia, A. Chem. Comm. 2002, 952-953.

[18]. Ohkita, M.; Kawano, M.; Suzuki, T.; Tsuji, T. Chem. Comm. 2002, 3054-3055.

Supporting Agencies

Most read articles by the same author(s)
TrendMD

Dimensions - Altmetric - scite_ - PlumX

Downloads and views

Downloads

Download data is not yet available.

Metrics

Metrics Loading ...
License Terms

License Terms

by-nc

Copyright © 2024 by Authors. This work is published and licensed by Atlanta Publishing House LLC, Atlanta, GA, USA. The full terms of this license are available at https://www.eurjchem.com/index.php/eurjchem/terms and incorporate the Creative Commons Attribution-Non Commercial (CC BY NC) (International, v4.0) License (http://creativecommons.org/licenses/by-nc/4.0). By accessing the work, you hereby accept the Terms. This is an open access article distributed under the terms and conditions of the CC BY NC License, which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited without any further permission from Atlanta Publishing House LLC (European Journal of Chemistry). No use, distribution, or reproduction is permitted which does not comply with these terms. Permissions for commercial use of this work beyond the scope of the License (https://www.eurjchem.com/index.php/eurjchem/terms) are administered by Atlanta Publishing House LLC (European Journal of Chemistry).