European Journal of Chemistry 2015, 6(1), 57-62. doi:10.5155/eurjchem.6.1.57-62.1145

Pyridazine and its related compounds: Part 33. Synthesis of some disperse dyes derived from 3-hydrazinyl-4,5-diphenyl-1H-pyrazolo[3,4-c]pyridazine and their color assessment on polyester fabric


Ali AbdelHamid Deeb (1,*) , Mamdoh Bahgat El‐Hossami (2) , Ahmed Awad Mohammed Abdelgawad (3)

(1) Department of Chemistry, Faculty of Science, Zagazig University, Zagazig, 44519, Egypt
(2) Printing, Dyeing and Finishing Department, Faculty of Applied Arts, Helwan University, Giza, 12311, Egypt
(3) Medicinal and Aromatic Plants Department, Desert Research Center, Cairo, 11753, Egypt
(*) Corresponding Author

Received: 06 Sep 2014, Accepted: 18 Oct 2014, Published: 31 Mar 2015

Abstract


Active methylene compound such as ethyl acetoacetate was coupled with diazotized arylamines to give ethyl arylazoacetoacetates. When the obtained compounds refluxed with 3-hydrazinyl-4,5-diphenyl-1H-pyrazolo[3,4-c]pyridazine in the presence of ethanol yielded 1-(4, 5-Diphenyl-1H-pyrazolo[3, 4-c]pyridazin-3-yl)-3-methyl-4-(2-phenylhydrazono)-1H-pyrazol-5(4H)-one derivatives. The dyes were applied to polyester fabric, and their absorption spectral characteristics, fastness properties and color assessment measured.


Keywords


Pyridazine; Color assessment; Dyeing properties; Fastness properties; Heterarylazo disperse dyes; Absorption spectral characteristics

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DOI: 10.5155/eurjchem.6.1.57-62.1145

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Citations

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[1]. Ali Deeb, Ahmed A. M. Abdelgawad
Utility of 3-amino-1H-pyrazolo[3,4-c]pyridazine in heterocyclic synthesis
Chemistry of Heterocyclic Compounds  51(9), 785, 2015
DOI: 10.1007/s10593-015-1776-4
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[2]. Ali Deeb, Ahmed A. M. Abdelgawad
Heterocyclization of 5-aminothieno[2,3-c]pyridazine-6-carbonitriles
Phosphorus, Sulfur, and Silicon and the Related Elements  193(10), 637, 2018
DOI: 10.1080/10426507.2018.1487438
/


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How to cite


Deeb, A.; El‐Hossami, M.; Abdelgawad, A. Eur. J. Chem. 2015, 6(1), 57-62. doi:10.5155/eurjchem.6.1.57-62.1145
Deeb, A.; El‐Hossami, M.; Abdelgawad, A. Pyridazine and its related compounds: Part 33. Synthesis of some disperse dyes derived from 3-hydrazinyl-4,5-diphenyl-1H-pyrazolo[3,4-c]pyridazine and their color assessment on polyester fabric. Eur. J. Chem. 2015, 6(1), 57-62. doi:10.5155/eurjchem.6.1.57-62.1145
Deeb, A., El‐Hossami, M., & Abdelgawad, A. (2015). Pyridazine and its related compounds: Part 33. Synthesis of some disperse dyes derived from 3-hydrazinyl-4,5-diphenyl-1H-pyrazolo[3,4-c]pyridazine and their color assessment on polyester fabric. European Journal of Chemistry, 6(1), 57-62. doi:10.5155/eurjchem.6.1.57-62.1145
Deeb, Ali, Mamdoh Bahgat El‐Hossami, & Ahmed Awad Mohammed Abdelgawad. "Pyridazine and its related compounds: Part 33. Synthesis of some disperse dyes derived from 3-hydrazinyl-4,5-diphenyl-1H-pyrazolo[3,4-c]pyridazine and their color assessment on polyester fabric." European Journal of Chemistry [Online], 6.1 (2015): 57-62. Web. 22 Sep. 2019
Deeb, Ali, El‐Hossami, Mamdoh, AND Abdelgawad, Ahmed. "Pyridazine and its related compounds: Part 33. Synthesis of some disperse dyes derived from 3-hydrazinyl-4,5-diphenyl-1H-pyrazolo[3,4-c]pyridazine and their color assessment on polyester fabric" European Journal of Chemistry [Online], Volume 6 Number 1 (31 March 2015)

DOI Link: https://doi.org/10.5155/eurjchem.6.1.57-62.1145

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