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Solvent-free synthesis of 2H-indazolo[2,1-b] phthalazine-triones promoted by cavitational phenomenon using iodine as catalyst
Anitha Varghese (1,*)
, Aatika Nizam (2) , Rajani Kulkarni (3) , Louis George (4) (1) Department of Chemistry, Christ University, Bangalore, 560 029, India
(2) Department of Chemistry, Christ University, Bangalore, 560 029, India
(3) Department of Chemistry, Christ University, Bangalore, 560 029, India
(4) Department of Chemistry, Christ University, Bangalore, 560 029, India
(*) Corresponding Author
Received: 11 Feb 2013 | Revised: 27 Feb 2013 | Accepted: 13 Mar 2013 | Published: 30 Jun 2013 | Issue Date: June 2013
Abstract
An environmentally benign, simple and efficient protocol for the synthesis of 2H-indazolo[2,1-b] phthalazine-triones by condensation of phthalhydrazide, aromatic aldehydes and dimedone under solvent-free ultrasound assisted conditions employing a safe, readily available iodine as catalyst has been described. This process is a valuable addition as it devoids the use of any solvent and takes place in short duration of time giving good yield of the products.
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DOI: 10.5155/eurjchem.4.2.132-137.746
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Centre for Research, Christ University, Bangalore, India
Citations
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