European Journal of Chemistry

Synthesis of coumarin derivative using polymer supported reagents

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Published: Jun 30, 2018
DOI: https://doi.org/10.5155/eurjchem.9.2.89-91.1691
Keywords:
Iminocoumarin, Selective synthesis, Unsaturated nitrile, Knoevenagel condensation, 3-Methoxy salicylaldehyde, Polymer supported reagent
Section
Research Article
Issue
Vol. 9 No. 2 (2018): June 2018
Dates
Received 2018-03-01
Accepted 2018-03-31
Published 2018-06-30
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Chiheb Mhiri
Laboratory of Applied Chemistry and Natural Substances Resources and Environment, Faculty of Sciences, University of Carthage, Zarzouna‐Bizerta, 7021, Tunisia
http://orcid.org/0000-0001-6331-6393
Riadh Ternane
Laboratory of Applied Chemistry and Natural Substances Resources and Environment, Faculty of Sciences, University of Carthage, Zarzouna‐Bizerta, 7021, Tunisia
http://orcid.org/0000-0003-3557-7558
Naceur Hamdi
Chemistry Department, College of Science and Arts, Qassim University, Al-Rass, 51921, Kingdom of Saudi Arabia
http://orcid.org/0000-0003-0110-9588
Lassaad Baklouti
Laboratory of Applied Chemistry and Natural Substances Resources and Environment, Faculty of Sciences, University of Carthage, Zarzouna‐Bizerta, 7021, Tunisia
http://orcid.org/0000-0002-5142-7501

Abstract

Recently, there has been a surge in use of polymer-supported reagents and catalysts become common tools for organic synthesis in what is known as polymer-assisted synthesis since they can simplify product isolation and purification. In this context, coumarin derivative 3 was prepared in good yield and high purity, starting from 3-methoxy salicylaldehyde, using reagents supported on a macroporous ion exchange resin. For this purpose, iminocoumarin and unsaturated nitrile were used as starting materials. The synthesized compounds were characterized by IR, NMR and mass spectrometry.


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How to Cite
(1)
Mhiri, C.; Ternane, R.; Hamdi, N.; Baklouti, L. Synthesis of Coumarin Derivative Using Polymer Supported Reagents. Eur. J. Chem. 2018, 9, 89-91.

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