European Journal of Chemistry 2012, 3(2), 208-210. doi:10.5155/eurjchem.3.2.208-210.581

An efficient and facile ring closure of 2’-hydroxychalcones under irradiation of tungsten light


Sainath Zangade (1,*) , Avinash Shinde (2) , Arvind Patil (3) , Yeshwant Vibhute (4)

(1) Department of Chemistry, Madhavrao Patil Mahavidyalaya, Palam, Prabhani, Maharashtra, 431720, India
(2) Laboratory of Organic Synthesis, Department of Studies in Chemistry, Yeshwant Mahavidyalaya, Nanded, Maharashtra, 431602, India
(3) Laboratory of Organic Synthesis, Department of Studies in Chemistry, Yeshwant Mahavidyalaya, Nanded, Maharashtra, 431602, India
(4) Laboratory of Organic Synthesis, Department of Studies in Chemistry, Yeshwant Mahavidyalaya, Nanded, Maharashtra, 431602, India
(*) Corresponding Author

Received: 27 Dec 2011, Accepted: 20 Feb 2012, Published: 30 Jun 2012

Abstract


An efficient, green and facile reaction has been reported between 2’-hydroxychalcones and hydrazine hydrate in 2-methoxyethanol in presence of catalytic amount of acetic acid under irradiation of tungsten light to afford 2-pyrazolines. Present methodology presents several advantages including simple reaction procedure, no need of catalyst/special apparatus and short reaction time giving quantitative yields of product.

3_2_208_210_800


Keywords


2-Pyrazolines; Tungsten light; Photocyclisation; Green chemistry; 2-Methoxyethanol; 2’-Hydroxychalcones

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DOI: 10.5155/eurjchem.3.2.208-210.581

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Citations

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[1]. Sainath Zangade, Shyam Mokle, Avinash Shinde, Yeshwant Vibhute
Selective iodination of 2-acetyl-1-naphthol using iodine and iodic acid under solvent-free grinding technique
European Journal of Chemistry  3(3), 314, 2012
DOI: 10.5155/eurjchem.3.3.314-315.641
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[2]. Shivaji Chavan, Sainath Zangade, Archana Vibhute, Yeshwant Vibhute
Synthesis and antimicrobial activity of some novel 2-azetidinones and 4-thiazolidinones derivatives
European Journal of Chemistry  4(2), 98, 2013
DOI: 10.5155/eurjchem.4.2.98-101.714
/


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How to cite


Zangade, S.; Shinde, A.; Patil, A.; Vibhute, Y. Eur. J. Chem. 2012, 3(2), 208-210. doi:10.5155/eurjchem.3.2.208-210.581
Zangade, S.; Shinde, A.; Patil, A.; Vibhute, Y. An efficient and facile ring closure of 2’-hydroxychalcones under irradiation of tungsten light. Eur. J. Chem. 2012, 3(2), 208-210. doi:10.5155/eurjchem.3.2.208-210.581
Zangade, S., Shinde, A., Patil, A., & Vibhute, Y. (2012). An efficient and facile ring closure of 2’-hydroxychalcones under irradiation of tungsten light. European Journal of Chemistry, 3(2), 208-210. doi:10.5155/eurjchem.3.2.208-210.581
Zangade, Sainath, Avinash Shinde, Arvind Patil, & Yeshwant Vibhute. "An efficient and facile ring closure of 2’-hydroxychalcones under irradiation of tungsten light." European Journal of Chemistry [Online], 3.2 (2012): 208-210. Web. 19 Sep. 2019
Zangade, Sainath, Shinde, Avinash, Patil, Arvind, AND Vibhute, Yeshwant. "An efficient and facile ring closure of 2’-hydroxychalcones under irradiation of tungsten light" European Journal of Chemistry [Online], Volume 3 Number 2 (30 June 2012)

DOI Link: https://doi.org/10.5155/eurjchem.3.2.208-210.581

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