European Journal of Chemistry 2014, 5(2), 321-327 | doi: https://doi.org/10.5155/eurjchem.5.2.321-327.969 | Get rights and content






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Synthesis, characterization and antimicrobial activity, and applications of new azo pyridone disperse dyes on polyester fabric


Alya Al-Etaibi (1,*) , Morsy Ahmed El-Apasery (2) , Huda Mahmoud (3) , Nouria Al-Awadi (4)

(1) Natural Science Department, College of Health Science, Public Authority for Applied Education and Training, Fayha, 72853, Kuwait
(2) Dyeing, Printing and Textile Auxiliaries Department, Textile Research Division, National Research Centre, 12622, Dokki, Giza, Egypt
(3) Department of Biological Sciences, Faculty of Science, Kuwait University, Safat, 13060, Kuwait
(4) Department of Chemistry, Faculty of Science, Kuwait University, Safat, 13060, Kuwait
(*) Corresponding Author

Received: 12 Nov 2013 | Revised: 24 Dec 2013 | Accepted: 29 Dec 2013 | Published: 30 Jun 2014 | Issue Date: June 2014

Abstract


Three components; ethyl cyanoacetate, ethyl amines, and methyl propionylacetate were condensed using solid supports in microwave to give 1,4-diethyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile (9) that was then coupled with aromatic diazonium salts to give the corresponding arylhydrazono-1,4-diethyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile disperse dyes, 10a-g. Structures of the afforded compounds were confirmed by (IR, NMR, EI/MS) and one of them was further confirmed by X-ray crystallography (10g). Fastness properties of the reported dyes were intensively examined against light, perspiration and washing fastness, exhibiting moderate, very good and excellent fastness levels, respectively. The antimicrobial activity of the dyes were tested against different bacterial strains of Gram positive and Gram negative characteristics, and yeast, at where most of them showed promising activities against such test organisms.


Keywords


Pyridones; Dyeing behavior; Polyester fabrics; Fastness properties; Antimicrobial activity; Microwave irradiation

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DOI: 10.5155/eurjchem.5.2.321-327.969

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Funding information


Natural Science Department, College of Health Science, Public Authority for Applied Education and Training, Fayha, Kuwait

Citations

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[1]. Mohamed Gomaa Badrey, Sobhi Mohamed Gomha, Hamada Moustafa Mashaly
Synthesis and studies on chromene based reactive azo dyes and their applications on different fabrics
European Journal of Chemistry  7(2), 146, 2016
DOI: 10.5155/eurjchem.7.2.146-151.1393
/


[2]. Alya M. Al-Etaibi, Morsy Ahmed El-Apasery
Nano TiO2 Imparting Multifunctional Performance on Dyed Polyester Fabrics with some Disperse Dyes Using High Temperature Dyeing as an Environmentally Benign Method
International Journal of Environmental Research and Public Health  17(4), 1377, 2020
DOI: 10.3390/ijerph17041377
/


[3]. Tarek Aysha, Mervat El-Sedik, Hamada M. Mashaly, Morsy A. El-Apasery, Oldřich Machalický, Radim Hrdina
Synthesis, characterisation, and applications of isoindigo/Pechmann dye heteroanalogue hybrid dyes on polyester fabric
Coloration Technology  131(4), 333, 2015
DOI: 10.1111/cote.12161
/


[4]. Alya M. Al-Etaibi, Morsy Ahmed El-Apasery
Dyeing Performance of Disperse Dyes on Polyester Fabrics Using Eco-Friendly Carrier and Their Antioxidant and Anticancer Activities
International Journal of Environmental Research and Public Health  16(23), 4603, 2019
DOI: 10.3390/ijerph16234603
/


[5]. Alya M. Al-Etaibi, Morsy Ahmed El-Apasery
A Comprehensive Review on the Synthesis and Versatile Applications of Biologically Active Pyridone-Based Disperse Dyes
International Journal of Environmental Research and Public Health  17(13), 4714, 2020
DOI: 10.3390/ijerph17134714
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Supporting information


The Supplementary Material for this article can be found online at: Supplementary files

How to cite


Al-Etaibi, A.; El-Apasery, M.; Mahmoud, H.; Al-Awadi, N. Eur. J. Chem. 2014, 5(2), 321-327. doi:10.5155/eurjchem.5.2.321-327.969
Al-Etaibi, A.; El-Apasery, M.; Mahmoud, H.; Al-Awadi, N. Synthesis, characterization and antimicrobial activity, and applications of new azo pyridone disperse dyes on polyester fabric. Eur. J. Chem. 2014, 5(2), 321-327. doi:10.5155/eurjchem.5.2.321-327.969
Al-Etaibi, A., El-Apasery, M., Mahmoud, H., & Al-Awadi, N. (2014). Synthesis, characterization and antimicrobial activity, and applications of new azo pyridone disperse dyes on polyester fabric. European Journal of Chemistry, 5(2), 321-327. doi:10.5155/eurjchem.5.2.321-327.969
Al-Etaibi, Alya, Morsy Ahmed El-Apasery, Huda Mahmoud, & Nouria Al-Awadi. "Synthesis, characterization and antimicrobial activity, and applications of new azo pyridone disperse dyes on polyester fabric." European Journal of Chemistry [Online], 5.2 (2014): 321-327. Web. 27 Oct. 2020
Al-Etaibi, Alya, El-Apasery, Morsy, Mahmoud, Huda, AND Al-Awadi, Nouria. "Synthesis, characterization and antimicrobial activity, and applications of new azo pyridone disperse dyes on polyester fabric" European Journal of Chemistry [Online], Volume 5 Number 2 (30 June 2014)

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DOI Link: https://doi.org/10.5155/eurjchem.5.2.321-327.969

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