European Journal of Chemistry 2013, 4(3), 245-249 | doi: https://doi.org/10.5155/eurjchem.4.3.245-249.820 | Get rights and content

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A facile synthesis of some biologically active disperse dyes derived from arylazonicotinates and their application on polyester fabrics


Morsy Ahmed El-Apasery (1,*) , Samar Mohamed Ashkar (2) , Marwan Touma (3) , Mohamed Hilmy Elnagdi (4)

(1) Dyeing, Printing and Textile Auxiliaries Department, Textile Research Division, National Research Centre, 12622 Dokki, Giza, Egypt
(2) Department of Chemistry, Faculty of Science, University of Aleppo, Aleppo, 10229, Syria
(3) Department of Chemistry, Faculty of Science, University of Aleppo, Aleppo, 10229, Syria
(4) Chemistry Department, Faculty of Science, Kuwait University, Safat 13060, Kuwait
(*) Corresponding Author

Received: 02 May 2013 | Revised: 08 Jun 2013 | Accepted: 09 Jun 2013 | Published: 30 Sep 2013 | Issue Date: September 2013

Abstract


A series of 2-hydroxy- and 2-amino-6-substituted-5-arylazonicotinates monoazo disperse dyes 6 and 8a-d were prepared via condensation of 3-oxo-3-substituted-2-arylhydrazonals 1a-d with active methylene nitriles 2a,b. A high temperature dyeing method was employed to apply these disperse dyes for polyester fabrics. Fastness properties of the dyed samples were measured. Most of the dyed fabrics tested displayed very good fastness level to washing, perspiration and light. Finally, the biological activities of the prepared dyes against gram positive and gram negative bacteria were evaluated.

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Keywords


Cinnolines; Disperse dyes; Polyester fabrics; Biological activity; Arylazonicotinates; Fastness properties

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DOI: 10.5155/eurjchem.4.3.245-249.820

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Citations

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[1]. Mohamed R. Eletmany, Marzough Aziz Albalawi, Reem A.K. Alharbi, Rokaia B. Elamary, Abd El-Fattah A. Harb, Moghraby A. Selim, Asmaa Sayed Abdelgeliel, Entesar A. Hassan, Islam M. Abdellah
Novel arylazo nicotinate derivatives as effective antibacterial agents: Green synthesis, molecular modeling, and structure-activity relationship studies
Journal of Saudi Chemical Society  27(3), 101647, 2023
DOI: 10.1016/j.jscs.2023.101647
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[2]. Saleh Mohammed Al-Mousawi, Morsy Ahmed El-Apasery, Mohamed Hilmy Elnagdi
Arylazoazines and arylazoazoles as interesting disperse dyes: Recent developments with emphasis on our contribution laboratory outcomes
European Journal of Chemistry  5(1), 192, 2014
DOI: 10.5155/eurjchem.5.1.192-200.883
/


[3]. K. M. Al Zaydi, M. A. Al-Johani, N. F. Alqahtani, S. M. Mousally, N. Hilmy Elnagdi
Reactions under Pressure: Synthesis of Functionally Substituted Arylhydrazonal Derivatives as Precursors of Novel Pyridazines and Nicotinates
Russian Journal of General Chemistry  90(4), 710, 2020
DOI: 10.1134/S1070363220040234
/


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How to cite


El-Apasery, M.; Ashkar, S.; Touma, M.; Elnagdi, M. Eur. J. Chem. 2013, 4(3), 245-249. doi:10.5155/eurjchem.4.3.245-249.820
El-Apasery, M.; Ashkar, S.; Touma, M.; Elnagdi, M. A facile synthesis of some biologically active disperse dyes derived from arylazonicotinates and their application on polyester fabrics. Eur. J. Chem. 2013, 4(3), 245-249. doi:10.5155/eurjchem.4.3.245-249.820
El-Apasery, M., Ashkar, S., Touma, M., & Elnagdi, M. (2013). A facile synthesis of some biologically active disperse dyes derived from arylazonicotinates and their application on polyester fabrics. European Journal of Chemistry, 4(3), 245-249. doi:10.5155/eurjchem.4.3.245-249.820
El-Apasery, Morsy, Samar Mohamed Ashkar, Marwan Touma, & Mohamed Hilmy Elnagdi. "A facile synthesis of some biologically active disperse dyes derived from arylazonicotinates and their application on polyester fabrics." European Journal of Chemistry [Online], 4.3 (2013): 245-249. Web. 4 Jun. 2023
El-Apasery, Morsy, Ashkar, Samar, Touma, Marwan, AND Elnagdi, Mohamed. "A facile synthesis of some biologically active disperse dyes derived from arylazonicotinates and their application on polyester fabrics" European Journal of Chemistry [Online], Volume 4 Number 3 (30 September 2013)

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DOI Link: https://doi.org/10.5155/eurjchem.4.3.245-249.820


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