

Synthesis, characterization and antimicrobial activity, and applications of new azo pyridone disperse dyes on polyester fabric
Alya Al-Etaibi (1,*)




(1) Natural Science Department, College of Health Science, Public Authority for Applied Education and Training, Fayha, 72853, Kuwait
(2) Dyeing, Printing and Textile Auxiliaries Department, Textile Research Division, National Research Centre, 12622, Dokki, Giza, Egypt
(3) Department of Biological Sciences, Faculty of Science, Kuwait University, Safat, 13060, Kuwait
(4) Department of Chemistry, Faculty of Science, Kuwait University, Safat, 13060, Kuwait
(*) Corresponding Author
Received: 12 Nov 2013 | Revised: 24 Dec 2013 | Accepted: 29 Dec 2013 | Published: 30 Jun 2014 | Issue Date: June 2014
Abstract
Three components; ethyl cyanoacetate, ethyl amines, and methyl propionylacetate were condensed using solid supports in microwave to give 1,4-diethyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile (9) that was then coupled with aromatic diazonium salts to give the corresponding arylhydrazono-1,4-diethyl-2,6-dioxo-1,2,5,6-tetrahydropyridine-3-carbonitrile disperse dyes, 10a-g. Structures of the afforded compounds were confirmed by (IR, NMR, EI/MS) and one of them was further confirmed by X-ray crystallography (10g). Fastness properties of the reported dyes were intensively examined against light, perspiration and washing fastness, exhibiting moderate, very good and excellent fastness levels, respectively. The antimicrobial activity of the dyes were tested against different bacterial strains of Gram positive and Gram negative characteristics, and yeast, at where most of them showed promising activities against such test organisms.
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European Journal of Chemistry
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DOI: 10.5155/eurjchem.5.2.321-327.969
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Natural Science Department, College of Health Science, Public Authority for Applied Education and Training, Fayha, Kuwait
Citations
[1]. Mamdouh A. Sofan, Tarek Abou Elmaaty, Neveen M. Hashem, Laijiu Zheng
One-Step Dyeing and Antimicrobial Finishing of PET Fabric with Novel 4-Arylazopyrazolone Disperse Dyes
Fibers and Polymers 21(12), 2817, 2020
DOI: 10.1007/s12221-020-9794-y

[2]. Mohamed Gomaa Badrey, Sobhi Mohamed Gomha, Hamada Moustafa Mashaly
Synthesis and studies on chromene based reactive azo dyes and their applications on different fabrics
European Journal of Chemistry 7(2), 146, 2016
DOI: 10.5155/eurjchem.7.2.146-151.1393

[3]. Alya M. Al-Etaibi, Morsy Ahmed El-Apasery
Nano TiO2 Imparting Multifunctional Performance on Dyed Polyester Fabrics with some Disperse Dyes Using High Temperature Dyeing as an Environmentally Benign Method
International Journal of Environmental Research and Public Health 17(4), 1377, 2020
DOI: 10.3390/ijerph17041377

[4]. Tarek Aysha, Mervat El‐Sedik, Hamada M. Mashaly, Morsy A. El‐Apasery, Oldřich Machalický, Radim Hrdina
Synthesis, characterisation, and applications of isoindigo/Pechmann dye heteroanalogue hybrid dyes on polyester fabric
Coloration Technology 131(4), 333, 2015
DOI: 10.1111/cote.12161

[5]. Ghada S. Masaret
Synthesis, Docking and Antihypertensive Activity of Pyridone Derivatives
ChemistrySelect 5(44), 13995, 2020
DOI: 10.1002/slct.202003959

[6]. Alya M. Al-Etaibi, Morsy Ahmed El-Apasery
Microwave-Assisted Synthesis of Azo Disperse Dyes for Dyeing Polyester Fabrics: Our Contributions over the Past Decade
Polymers 14(9), 1703, 2022
DOI: 10.3390/polym14091703

[7]. Alya M. Al-Etaibi, Morsy Ahmed El-Apasery
Facile Synthesis of Novel Disperse Dyes for Dyeing Polyester Fabrics: Demonstrating Their Potential Biological Activities
Polymers 14(19), 3966, 2022
DOI: 10.3390/polym14193966

[8]. Alya M. Al-Etaibi, Morsy Ahmed El-Apasery
Dyeing Performance of Disperse Dyes on Polyester Fabrics Using Eco-Friendly Carrier and Their Antioxidant and Anticancer Activities
International Journal of Environmental Research and Public Health 16(23), 4603, 2019
DOI: 10.3390/ijerph16234603

[9]. Alya M. Al-Etaibi, Morsy Ahmed El-Apasery
A Comprehensive Review on the Synthesis and Versatile Applications of Biologically Active Pyridone-Based Disperse Dyes
International Journal of Environmental Research and Public Health 17(13), 4714, 2020
DOI: 10.3390/ijerph17134714

[10]. Alya M. Al-Etaibi, Morsy Ahmed El-Apasery
Ultrasonic Dyeing of Polyester Fabric with Azo Disperse Dyes Clubbed with Pyridonones and Its UV Protection Performance
Chemistry 3(3), 889, 2021
DOI: 10.3390/chemistry3030065

References
[1]. Faustino, H.; Brannigan, C. R.; Reis, L. V.; Santos, P. F.; Almeida, P. Dyes Pigments 2009, 83, 88-94.
http://dx.doi.org/10.1016/j.dyepig.2009.03.018
[2]. Jia, R.; Zheng, C.; Yang, D.; Sun, J.; Wang, H. Color. Technol. 2012, 128(4), 290-294.
http://dx.doi.org/10.1111/j.1478-4408.2012.00377.x
[3]. Rangnekar, D. W.; Dhamnskar, S. V. Dyes Pigments 1990, 13(4), 241-250.
http://dx.doi.org/10.1016/0143-7208(90)85023-H
[4]. Nermin, E.; Fatih, E. Dyes Pigments 1995, 27(4), 313-320.
http://dx.doi.org/10.1016/0143-7208(94)00071-9
[5]. Bahatti, H. S.; Seshadri, S. Color. Technol. 2004, 120(4), 151-155.
http://dx.doi.org/10.1111/j.1478-4408.2004.tb00221.x
[6]. Yen, M. S.; Wang, I. J. Dyes Pigments 2004, 61(3), 243-250.
http://dx.doi.org/10.1016/j.dyepig.2003.10.015
[7]. Song, H. C. K.; Tian, H. Dyes Pigments 2002, 53(3), 257-262.
http://dx.doi.org/10.1016/S0143-7208(02)00021-9
[8]. Chien, C. C.; Wang, I. J. Dyes Pigments 1991, 15, 69-82.
http://dx.doi.org/10.1016/0143-7208(91)87008-B
[9]. Ertan, N.; Gurkan, P. Dyes Pigments 1997, 33, 137-147.
http://dx.doi.org/10.1016/S0143-7208(96)00044-7
[10]. Ashkar, S. M.; El-Apasery, M. A.; Touma, M. M.; Elnagdi, M. H. Molecules 2012, 17, 8822-8831.
http://dx.doi.org/10.3390/molecules17088822
[11]. Al-Etaibi, A.; El-Apasery, M. A.; Al-Awadi, N. Eur. J. Chem. 2013, 4(3), 240‐244.
http://dx.doi.org/10.5155/eurjchem.4.3.240-244.834
[12]. Al-Mousawi, S. M.; El-Apasery, M. A.; Mahmoud, H. M. Molecules 2013, 18, 7081-7092.
http://dx.doi.org/10.3390/molecules18067081
[13]. Chrysler, L. P. Methods of Test for Color Fastness of Textiles and Leather, 7th ed., Bradford, London 1990, pp. 89-94.
[14]. El-Apasery, M. A.; Al-Qalaf, F.; Almohammad, K.; Mahmoud, H. Eur. J. Chem. 2013, 4(3), 211-215.
http://dx.doi.org/10.5155/eurjchem.4.3.211-215.783
[15]. Isaacson, D. M.; Kirschbaum, J. Assays of antimicrobial substances In: Manual of Industrial Microbiology and Biotechnology (Demain, A. L.; Solomon, N. A.; Eds), ASM, 1986, 410-435.
[16]. Elguero, J.; Marzin, C.; Katritzky, A. R.; Linda, P. The Tautomerism of Heterocyles in Adv. Heterocycl. Chem., Academic Press, 1976, pp. 106-109.
[17]. Karci, F.; Karci, F. Dyes Pigments. 2008, 76(1), 147-157.
http://dx.doi.org/10.1016/j.dyepig.2006.07.029
[18]. Otutu, J. O.; Osabohien, E. Asian J. Mat. Sci. 2013, 5(1), 1-8.
[19]. Singh, K.; Singh, S.; Taylor, J. A. Dyes Pigments. 2002, 54, 189-200.
http://dx.doi.org/10.1016/S0143-7208(02)00053-0
[20]. Metwally, M. A.; Abdel-latif, E.; Amer, F. A.; Kaupp, G. Dyes Pigments 2004, 60, 249-264.
http://dx.doi.org/10.1016/S0143-7208(03)00153-0
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DOI Link: https://doi.org/10.5155/eurjchem.5.2.321-327.969

















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