European Journal of Chemistry

Synthesis, characterization and crystal structure of ethyl 4-(3-chloro benzamido)benzoate

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Published: Dec 22, 2010
DOI: https://doi.org/10.5155/eurjchem.1.4.289-290.207
Keywords:
Ethyl 4-(3-chlorobenzamido)benzoate, Crystal structure, Synthesis, Characterization
Section
Research Article
Issue
Vol. 1 No. 4 (2010): December 2010
Dates
Received 2010-07-16
Accepted 2010-08-07
Published 2010-12-22


Main Article Content

Aamer Saeed
Department of Chemistry, Quaid-I-Azam University, Islamabad, PK-45320, Pakistan
Hummera Rafique
Department of Chemistry, Quaid-I-Azam University, Islamabad, PK-45320, Pakistan
Ulrich Flörke
Department Chemie, Fakultät fur Naturwissenschaften, Universitat Paderborn, Warburgerstrasse 100, Paderborn, D-33098, Germany

Abstract

The title compound was efficiently synthesized in two steps starting from esterification of 4-aminobenzoic acid followed by amidation with 3-chlorobenzoyl chloride in dry tetrahydrofuran. The structure was confirmed by spectroscopic data and elemental analysis. The molecular structure was determined from single crystal X-ray diffraction data. It crystallizes in the triclinic space group P-1 with Z = 2 and unit cell dimensions a = 5.2941(15) Å, b = 8.157(2) Å, c = 16.238(4) Å, α = 82.682(6)°, β = 84.481(6)°, γ = 80.100(6)° and V = 683.2(3) Å3.

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How to Cite
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Saeed, A.; Rafique, H.; Flörke, U. Synthesis, Characterization and Crystal Structure of Ethyl 4-(3-Chloro benzamido)benzoate. Eur. J. Chem. 2010, 1, 289-290.

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