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Synthesis and X-ray crystallography of (1R,3aR,7aR)-1-((S)-1-((2R,5S)-5-(3-hydroxypentan-3-yl)tetrahydrofuran-2-yl)ethyl)-7a-methyloctahydro-4H-inden-4-one
Modou Lo (1) , Andrea Martínez (2) , Hugo Santalla (3) , Fátima Garrido (4) , Aliou Hamady Barry (5) , Mohamed Gaye (6,*)
(1) Department of Chemistry, University Cheikh Anta Diop, Dakar, 10700, Senegal
(2) Dipartamento Química Orgínica, Facultade de Química, Universidade de Vigo, Vigo, 36310, Spain
(3) Dipartamento Química Orgínica, Facultade de Química, Universidade de Vigo, Vigo, 36310, Spain
(4) Dipartamento Química Orgínica, Facultade de Química, Universidade de Vigo, Vigo, 36310, Spain
(5) Department of Chemistry, University of Nouakchott, Nouakchott, 130301, Mauritania
(6) Department of Chemistry, University Cheikh Anta Diop, Dakar, 10700, Senegal
(*) Corresponding Author
Received: 21 Jun 2017 | Revised: 12 Jul 2017 | Accepted: 15 Jul 2017 | Published: 30 Sep 2017 | Issue Date: September 2017
The crystal of the title compound, C21H36O3 contains an oxolane ring, and six defined stereocenters which are unambigously established by the crystallography study. A three dimensional supramolecular architecture is ensured by hydrogen bonds from the hydroxy group which is both engaged in inter (O-H···O2) and intramolecular C-H···O-H) hydrogen bonds. Weak C-H···O=C hydrogen bonds are involved also into the consolidation of the network.
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The University of Vigo (Spain) and the Sonatel Fondation
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DOI Link: https://doi.org/10.5155/eurjchem.8.3.248-251.1602
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European Journal of Chemistry 2017, 8(3), 248-251 | doi: https://doi.org/10.5155/eurjchem.8.3.248-251.1602 | Get rights and content
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